Engineering Commons^™

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

The research objectives of this project were as follows:

• To generate calibration curves of voltage versus oxygen concentration for the YSZ oxygen sensor system under various temperatures in liquid LBE.
• To determine the sensor characteristics of the YSZ sensor system.
• To determine oxygen dissolving rates in LBE under different temperatures in vitro.
• To study the effects of unwanted electrical conductivity, contributed by the mobility of the electrons at high temperatures, for more accurate oxygen measurement.
• To study alternative and promising oxygen measuring methods.

Modeling, Fabrication, And Optimization Of Niobium Cavities Final Phase: Final Report, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

This final report provides the activities and accomplishments of Modeling, Fabrication, and Optimization of Niobium Cavities – Final Phase. The fluid flow experiments for the etching of the superconducting cavity walls and baffle designs of phase II of the three phases has been completed leading to a MS thesis in December of 2003. Designing the experimental setup of secondary electron emission was well underway in early summer of 2003 when funding was made available for this portion of the study. By March 2004, many of the components of the experimental study reached UNLV with some assembly accomplished. The first secondary …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Iii Fourth Quarterly Report, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for niobium superconducting cavities. The surface preparation can significantly affect the secondary electron emission yields. Such yields are used in design codes. Current codes use values obtained from niobium samples cleaned by a different means at temperatures other than the operating temperature. Secondary electron emission studies on LANL surface-cleaned niobium are conducted with preliminary data presented in this report at room temperature. Soon studies will be …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Jan. 01 – March. 31, 2005), Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

We performed data analysis on the data collected from LANL test loop. One student was been hired to perform the data analysis. A new proposal is submitted to TRP program. We have one paper accepted for publication in International Journal of Heat and Mass Transfer, and another paper accepted for oral presentation by IEEE International Symposium of Circuits and Systems for the track Chemical Sensors. A manuscript regarding to the RGA analysis for the calibration of oxygen sensor is on the way.

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Iii, Third Quarterly Report, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

This quarterly report provides an update to the last phase of the Modeling, Fabrication, and Optimization of Niobium Cavities in the no-cost extension period. Designing the experimental setup of secondary electron emission was well underway in early summer of 2003 when funding was made available for this portion the study. By March 2004, many of the components of the experimental study reached UNLV with some assembly accomplished. The first secondary electron emission (SEE) measurement was made from the surface of a Faraday cup in September 2004. In December of 2005, the software for the particle positioning detector was finally up …

Modeling, Fabrication, And Optimization Of Niobium Cavities, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

One of the key technologies for the deployment of accelerator driven transmutation systems is the accelerator itself. Elliptical superconducting niobium cavities are used to increase the efficiency of the high-power accelerators needed to support the transmutation mission.

One of the major sources of energy loss from a superconducting accelerator cavity is a process known as multiple impacting (or “multipacting”) of electrons. This phenomenon limits the maximum amount of energy and power that the niobium cavity can store. As a result, the maximum power available for accelerating the desired charge, as well as the overall performance of the accelerator is reduced. …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

Although liquid lead-bismuth eutectic (LBE) is a good candidate for the coolant that can be employed in a subcritical transmutation blanket, it is known to be very corrosive to stainless steel, the material used in the containment structure. To mitigate this problem, trace levels of oxygen can be introduced into the system, causing the formation of a protective oxide layer at the interface between the LBE and steel. The proper formation of this oxide layer largely depends on the accurate measurement and subsequent control of the oxygen concentration in liquid LBE.

Yttria Stabilized Zirconia (YSZ) oxygen sensors, using molten bismuth …

Modeling, Fabrication, And Optimization Of Niobium Cavities Phase Iii: Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

This quarterly report provides an update to the last phase of the Modeling, Fabrication, and Optimization of Niobium Cavities. Designing the experimental setup of secondary electron emission was well underway in early summer of 2003 when funding was made available for this portion the study. By March 2004, many of the components of the experimental study reached UNLV with some assembly accomplished. The first secondary electron emission (SEE) measurement was made from the surface of a Faraday cup in September 2004. At a particular beam energy, the current measured with the Faraday cup and electrometer changed sign over a range …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (July 1 – Sept. 30, 2004), Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

Dr. Jiang Ma and Mr. Xiaolong Wu worked in LANL between July 1 and Sept. 15 to conduct the experiment. Test of the corrosion of different materials in LBE was performed. The influence of the process of gas introduction to the LBE was studied. Data analysis work was performed based on accumulated data. In the same time, progress has been made in the simulation for transport in oxygen mixing, and one paper was presented in a conference. Another paper was composed and submitted to IEEE International Symposium of Circuits and Systems for the track Chemical Sensors. Preparation of a paper …

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada Las Vegas (UNLV) and Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded, bent (three-point-bend), and cold-worked engineering materials using a new nondestructive technique based on positron annihilation spectroscopy (PAS). The proposed technique is to use γ-rays from a small MeV electron linear accelerator (Linac) to generate positrons inside the test sample via 2 pair production. This method can be used for materials characterization and investigation of defects in thick samples that usually cannot be accomplished by conventional positron technique or other …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Iii Third Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. The third phase concludes the experimental a fluid flow study and optimization study. The first quarter and second quarter of phase three also begins the experimental set-up of secondary emission studies from niobium in superconducting mode. This …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Iii Second Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. The third phase concludes the experimental a fluid flow study and optimization study. The first quarter and second quarter of phase three also begins the experimental set-up of secondary emission studies from niobium in superconducting mode. This …

Modeling, Fabrication, And Optimization Of Niobium Cavities, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

One of the key technologies for the deployment of acceleratordriven transmutation systems is the accelerator itself. Elliptical superconducting niobium cavities are used to increase the efficiency of the high-power accelerators needed to support the transmutation mission.

One of the major sources of energy loss from a superconducting accelerator cavity is a process known as multiple impacting (or “multipacting”) of electrons. This phenomenon limits the maximum amount of energy and power that the niobium cavity can store. As a result, the maximum power available for accelerating the desired charge, as well as the overall performance of the accelerator is reduced. Furthermore, …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

Lead-bismuth eutectic (LBE) is a candidate as a spallation target in sub-critical transmutation systems and as a coolant in nuclear programs. One of the primary concerns with LBE systems is the corrosion of stainless steel, the primary structural material used in nuclear systems. To mitigate this problem, trace levels of oxygen can be introduced into the system, causing the formation of a protective oxide layer at the interface between the LBE and steel. To protect the steel components, this oxide layer must be properly maintained. However, too much oxygen will produce unwanted oxide precipitation within the coolant and elsewhere in …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Aug. 01 – Oct. 31, 2003), Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

The experimental setup designed and manufactured in UNLV was shipped to LANL in early Aug. One student has been working in LANL to conduct the experiment since then. In the meantime, one new Ph. D. student has started to run the simulation for transport in oxygen mixing. In Oct., a professional has been hired to work in both experimental and the theoretical studies pertaining to the proposed work.

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements: Quarterly Progress Report (June 01 – August 31, 2003), Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada Las Vegas (UNLV), the Idaho State University (ISU), and the Los Alamos National Laboratory (LANL) is to evaluate the feasibility of determining residual stresses in cold-worked, plastically-deformed (bent), and welded materials using a nondestructive method based on positron annihilation spectroscopy (PAS). This technique uses γ-rays from a small MeV electron Linac to generate positrons inside the sample via pair production. This method is known to have capabilities of characterizing defects in thick specimens that could not be accomplished by conventional positron technique or other nondestructive methods. The generated …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Iii Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. The third phase concludes the experimental a fluid flow study and optimization study. The first quarter and second quarter of phase three also begins the experimental set-up of secondary emission studies from niobium in superconducting mode. This …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (May. 01 – July 31, 2003), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

The report for Y01 has been prepared and submitted. The final part of our apparatus, the N3Si4 stirrer, was received by the end of May. The assembly of the apparatus has almost been completed. The control plan for our apparatus has been revised. To run FLUENT, a high-end Unix-based Sun workstation has been acquired. Plan has been made to ship our apparatus to LANL.

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Ii Final Report, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. The second phase has resulted in an experimental setup of a fluid flow experiment with experimentation to be completed in the third year. Some of these results were presented at American Nuclear Society, Student Conference April 2-5, …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Feb. 01 – Apr. 30, 2003), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

We received most of the components, everything except the customized and outsourced stirrer, for the new apparatus for oxygen measurement/calibration. Thus far, most of the machining work has been completed. The LaveView module used for the data collection and the control of the apparatus has been tested. 2-D simulation work has been performed using FEMLAB.

Modeling, Fabrication, And Optimization Of Niobium Cavities Phase Ii: Third Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. The second phase has resulted in an experimental setup of a fluid flow experiment with experimentation to be completed in the third year. Other experimental activities include the evaluation of a vacuum system and various vacuum equipment …

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada, Las Vegas (UNLV) and the Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded, bent (three-point-bend), and cold-worked engineering materials using a new nondestructive technique based on positron annihilation spectroscopy. The proposed technique is to use x-rays from a small MeV electron Linac to generate positrons inside the sample via pair production. This method can be used for materials characterization and investigation of defects in thick samples that could not be accomplished by conventional positron technique or other nondestructive methods. The data …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Nov. 01 – Jan. 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

The design of the new apparatus for oxygen measurement/calibration has been completed. This new apparatus shall be of great importance for the UNLV researchers to conduct the research work in the campus.

Modeling, Fabrication, And Optimization Of Niobium Cavities: Final Phase, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. This is the third and final phase of the study.

The first phase has resulted in improving the basic understanding of multipacting and the process of chemical etching. The second phase has resulted in an experimental setup …

Modeling, Fabrication, And Optimization Of Niobium Cavities, Robert A. Schill Jr., Mohamed Trabia, William Culbreth

Transmutation Sciences Materials (TRP)

One of the key technologies for the deployment of accelerator driven transmutation systems is the accelerator itself. To increase the efficiency of the high-power accelerators needed to support the transmutation mission, the national and international accelerator teams have proposed using elliptical superconducting niobium cavities. This project is tasked with examining the impacts of the design and fabrication technologies for these elliptical niobium cavities on their performance. Niobium was selected primarily due to its behavior at low temperatures.

One of the major sources of energy loss from a superconducting accelerator cavity is a process known as multiple impacting (or “multipacting”) of …

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

Lead-bismuth eutectic (LBE) is a candidate as a spallation target in sub-critical transmutation systems and as a coolant in nuclear programs. One of the primary concerns with LBE systems is the corrosion of stainless steel, the primary structural material used in nuclear systems. To mitigate this problem, trace levels of oxygen can be introduced into the system, causing the formation of a protective oxide layer at the interface between the LBE and steel. To protect the steel components, this oxide layer must be properly maintained. However, too much oxygen will produce unwanted oxide precipitation within the coolant and elsewhere in …

Stress Corrosion Cracking Of Type 422 Stainless Steel, Ramprashad Prabhakaran

Transmutation Sciences Materials (TRP)

This paper presents the results of SCC tests of quenched and tempered martensitic Type 422 SS in neutral and acidic aqueous environments at ambient temperature and 90^oC.The susceptibility of smooth and notched tensile specimens to SCC was evaluated by using constant load (CL) and slow strain rate (SSR) test methods. During CL testing, a calibrated proof ring was used to apply a constant load to the test specimen. The magnitude of the applied stress was based on ambient temperature yield strength of the material. On the contrary, the test specimen during SSR testing was continuously strained in tension …

Effects Of Environmental Variables And Stress Concentration On Cracking Of Spallation Target Materials, Ajit K. Roy, Ramprashad Prabhakaran, Mohammad K. Hossain

Transmutation Sciences Materials (TRP)

This paper presents the results of stress corrosion cracking (SCC) studies of two martensitic target materials, namely Alloy EP-823 and Type 422 stainless steel. The susceptibility to SCC was evaluated by using constantload and slow-strain-rate (SSR) test techniques in neutral (pH: 6-7) and acidic (pH: 2-3) aqueous solutions at ambient temperature and 90^oC. A proof ring was used to apply tensile load to the smooth cylindrical specimen for 30 days in constant-load testing. For SSR testing, the specimen was strained in tension until fracture at a strain rate of 3.3 x 10^-6 sec^-1.

Effects Of Environmental Variables And Stress Concentration On Target Materials, Sudheer Sama

Transmutation Sciences Materials (TRP)

This paper presents a brief summary on stress corrosion cracking (SCC) behavior of alloy HT 9. The susceptibility of this alloy to SCC was evaluated by using constant load and slow strain rate test techniques in neutral and acidic solutions at ambient temperature and 90°C. A proof ring was used to apply tensile load to the smooth specimen for 30 days in constant load testing. In slow strain rate testing, the specimen was continuously strained in tension at a rate of 3.3 × 10^-6 sec^-1 until fracture.

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Aug. 01 – Oct. 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

After two month intensive work in LANL, some preliminary sensor calibration curves have been obtained. Further data analysis shall be performed to assess the theoretical and measured data. Also, a new experimental apparatus shall be designed and located in UNLV to continue the left work.

Technical Progress:

• A set of calibration curves of voltage vs. temperature ranging from 300⁰C to 500⁰C under various oxygen concentrations in liquid LBE for the YSZ oxygen sensor has been obtained and has been reported in one paper.

• A meeting with LBE committee and other faculty members in AAA …