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A Sustainable Approach For Tungsten Carbide Synthesis Using Renewable Biopolymers, Monsur Islam, Rodrigo Martinez-Duarte

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Here we present a sustainable, environment-friendly and energy-efficient approach for synthesis of porous tungsten carbide (WC). A biopolymer-metal oxide composite featuring iota-carrageenan, chitin and tungsten trioxide (WO3) was used as the precursor material. The reaction mechanism for the synthesis of WC was estimated using the results from X-ray diffraction characterization (XRD). A synthesis temperature of 1300 °C and dwell time of 3 h were found to be the optimum process parameters to obtain WC>98% pure. The grain size, porosity and Brunauer–Emmett–Teller (BET) surface area of the synthesized WC were characterized using field emission scanning electron microscopy, high resolution transmission …