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2008

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Development Of A Fish-Based Index Of Biotic Integrity For Oxbow Lakes Of The Yazoo River Basin, Mississippi, Nathan Aycock Dec 2008

Development Of A Fish-Based Index Of Biotic Integrity For Oxbow Lakes Of The Yazoo River Basin, Mississippi, Nathan Aycock

Theses and Dissertations

Fish community data were used to develop an index of biotic integrity (IBI) to quantify habitat degradation in oxbow lakes of the Delta region of the Yazoo River Basin. Daytime boat electrofishing was used to sample the fish assemblage of 30 oxbow lakes during 2006-2007. We evaluated 70 candidate metrics based on their responses to measures of anthropogenic disturbance. Six metrics were retained for inclusion in the IBI: species richness, Shannon’s diversity (H’), average tolerance, and catch rates of buffalo, orangespotted sunfish, and litho-psammophilic spawners. The six IBI metrics showed strong multivariate relationships with measures of habitat degradation in a …


Development Of A Sensory Descriptive Lexicon For Calamondins (Citrus Mitis Blanco) And Consumer Acceptance Of Calamondin Yogurt, Ye Tian Dec 2008

Development Of A Sensory Descriptive Lexicon For Calamondins (Citrus Mitis Blanco) And Consumer Acceptance Of Calamondin Yogurt, Ye Tian

Theses and Dissertations

The objectives of this research were to establish a semi-descriptive sensory language that describes the attributes of calamondin fruit and develop yogurt products flavored with calamondin and test consumers’ acceptance of the products. A total of 89 sensory terms were established by trained panelists to describe calamondins. Yogurt products were developed with 0%, 5%, 10%, and 15% calamondin pulp. Results demonstrated that no significant difference (P>0.05) occurred for consumers’ acceptance of yogurt appearance and texture, and significant differences (P<0.05) occurred for consumers’ acceptance of yogurt flavor and overall liking. Generally, the yogurt with 10% honey and the yogurt with 10% honey and 5% calamondin pulp were well accepted by consumers. The consumers were grouped into 6 clusters based on their prefences. The majority (60%) of the consumers liked moderately yogurts with 10% honey, and 0% and 5% calamondin pulp respectively.


Development Of Corrective Actions For Higher Order Contingencies, Bharath Kumar Ravulapati Dec 2008

Development Of Corrective Actions For Higher Order Contingencies, Bharath Kumar Ravulapati

Theses and Dissertations

The importance of the electric power infrastructure has been exposed by several blackouts throughout the world in the last decade. These blackouts were caused mainly by physical vulnerabilities, human errors and natural disasters. The power grid is becoming more and more prone to outages which affect not only the power system network, but also other infrastructures and the society in several ways. Utilities generally operate with an (N-1) security level (no violations for single outage), and blackouts are generally caused by higher order contingencies. There is lack of effective methods and analysis tools to deal with higher order contingencies. Higher …


Educational Video Impact On College Student Knowledge, Opinions, And Referral Attitudes Regarding Attention-Deficit/Hyperactivity Disorder, Nichol Frances Pritchard Dec 2008

Educational Video Impact On College Student Knowledge, Opinions, And Referral Attitudes Regarding Attention-Deficit/Hyperactivity Disorder, Nichol Frances Pritchard

Theses and Dissertations

The interaction of osteoclasts and osteoblasts regulates bone density and the maintenance of osseointegration of implants. To investigate osteoblastic response to strain, rat osteosarcoma cells were cultured on titanium plates and subjected to one of three treatments: a neutral control (0 microstrain), tension (1000 microstrain), and compression (1000 microstrain). Treatments were applied via 4 point bending for fifteen minutes each day to a strain of 1mm/m at a sinusoidal frequency of 1Hz. Cells were measured for DNA as indicator of proliferation, alkaline phosphatase as indicator of phenotype and total protein and calcium deposition as indicators of matrix formation. Results indicated …


Effects Of Culture Methods And Simulated Microgravity Conditions On Development Of Bovine Embryos Produced In Vitro, Songi Jung Dec 2008

Effects Of Culture Methods And Simulated Microgravity Conditions On Development Of Bovine Embryos Produced In Vitro, Songi Jung

Theses and Dissertations

The objectives of this study were (1) to determine the optimum in vitro culture conditions for in vitro fertilized bovine embryos among culture methods and (2) to investigate whether bovine fertilization and embryo development would occur in simulated microgravity conditions in vitro. In the first part of this study, the result showed that the microdrop method was the optimum culture method among groups; however, FBS supplementation did not significantly affect the bovine preimplantation embryo development in vitro. In the second part of this study, the result showed that bovine in vitro fertilization did not occur in simulated microgravity conditions. Moreover, …


Fabrication Of Aluminum Matrix Particulate Composites By Compaction And Sintering, Wei Li Dec 2008

Fabrication Of Aluminum Matrix Particulate Composites By Compaction And Sintering, Wei Li

Theses and Dissertations

With the possession of extremely broad unique properties, particulate reinforced aluminum composites are very attractive in diverse applications. Aluminum matrix particulate composites are challenging to work with. A single pressing and sintering process was used to fabricate the reinforced aluminum composites in this study. The key advantage of this method is its comparative low expense. However, abrasive reinforcement powders can lead to shorter tool life. To study the fundamental wear mechanisms during the die compaction process, a new method was developed and combined with experiments to quantify tool wear. Automatic die compaction experiments and tribological experiments are employed in this …


The Effect Of Policy And Land Use Change On Water Quality In A Coastal Watershed City: An Analysis Of Covington, Louisiana, Kenneth Tyler Langley Dec 2008

The Effect Of Policy And Land Use Change On Water Quality In A Coastal Watershed City: An Analysis Of Covington, Louisiana, Kenneth Tyler Langley

Theses and Dissertations

There is currently a great need to expand the understanding of land use policy’s impact on water quality. The purpose of this thesis is to examine local policy in place in Covington, Louisiana in order to find out if it is having an impact on land use, which then has an impact on water quality. Methods used included reclassification of land use categories within a Geographical Information System and analysis of changes in the city over a four year period. Policy was assessed using a pre-existing evaluation method from The Center for Watershed Protection as well as by a more …


The Effects Of Low Atmosphere Stunning And Deboning Time On Broiler Breast Meat Quality, Vamsidhar Battula Dec 2008

The Effects Of Low Atmosphere Stunning And Deboning Time On Broiler Breast Meat Quality, Vamsidhar Battula

Theses and Dissertations

A randomized complete block design with three replications (n=432, 72 broilers per treatment) was utilized to evaluate the effects of electrical (ES) and low atmosphere pressure stunning (LAPS) on the quality of broiler breast meat deboned at 0.75, 2, and 4h postmortem. The L* values were lower (P<0.05) for LAPS than ES at 4 h and 2 h deboning times. Shear force did not differ (P>0.05) between stun methods but decreased (P<0.05) as deboning time increased. Consumers were clustered into 8 groups based on preference and liking of samples. Sixtyive percent of consumers (3 clusters) liked all broiler breast treatments. Within these three clusters, some consumers preferred (P<0.05) 4 h deboned samples over those deboned at 2 h (Cluster 7), and other consumers preferred (P<0.05) those deboned at 2 h over 4 h samples (Cluster 6). Data reveals that both stunning methods provide high quality breast meat with minimal product differences.


Use Of Empirically-Based Reading Interventions To Address The Academic Skills Deficits And Escape-Maintained Target Behaviors Exhibited By Elementary School Students, Melissa S. Anderson Dec 2008

Use Of Empirically-Based Reading Interventions To Address The Academic Skills Deficits And Escape-Maintained Target Behaviors Exhibited By Elementary School Students, Melissa S. Anderson

Theses and Dissertations

The participants in this study were referred by the teacher or the teacher support team for a functional behavioral assessment (FBA) and development of a positive behavior support plan to address disruptive behavior and academic skills deficits. Therefore, the purpose of Experiment I was to examine the ability of FBA procedures to identify students with reading difficulty who demonstrated problem behavior potentially maintained by escape from academic demands. Each environmental variable introduced during the brief functional analysis was manipulated via a multiple element design (Cooper, Wacker, Sasso, Reimers, & Donn, 1990; Derby et al., 1992; Northup et al., 1991). Experiment …


Epidemiologic And Economic Study Of Hyperelastosis Cutis/Herda In The Quarter Horse Cutting Industry, Sally Grant Tipton Dec 2008

Epidemiologic And Economic Study Of Hyperelastosis Cutis/Herda In The Quarter Horse Cutting Industry, Sally Grant Tipton

Theses and Dissertations

Hyperelastosis Cutis (HC) is an autosomal recessive disorder in Quarter Horses. Homozygous (Hr/Hr) horses are affected with fragile, hyperextensible skin that sloughs and scars easily following minor trauma. Heterozygous (N/Hr) horses appear normal, but carry one copy of the gene. Objectives were to determine inbreeding coefficients of affected (Hr/Hr), carrier (N/Hr), and normal (N/N) Quarter Horses, compared to Thoroughbreds, and evaluate economic effects of HC within the cutting horse industry. Of the top cutting horses from 1985 through 2006, 35 were confirmed carriers by either DNA analysis or production of affected offspring. Although 23% of the earnings from the leading …


Evaluation Of Erosional Forcings Of A Beach/Berm/Wetland System And Applicable Restoration Technologies, Jared Kyle Mckee Dec 2008

Evaluation Of Erosional Forcings Of A Beach/Berm/Wetland System And Applicable Restoration Technologies, Jared Kyle Mckee

Theses and Dissertations

The purpose of this study was to evaluate the local and regional processes causing the shoreline recession of an eroding beach/berm/wetland system on the eastern shore of Mobile Bay. The analysis was then used to evaluate different technologies which could meld to create a holistic shoreline protection design to fortify the entire spectrum of the shoreline. Wind waves are the major erosional force causing a bi-directional, but southerly dominated, longshore transport and an erosional cross-shore transport during large wave events. Erosion mitigation technologies which promote ecological integrity are presented and include: oyster shell breakwaters, SAV establishment, intertidal grass plantings, and …


Evaluation Of Propane Fueled Chp Systems For Small Commercial Applications, Justin Byron Ramsay Dec 2008

Evaluation Of Propane Fueled Chp Systems For Small Commercial Applications, Justin Byron Ramsay

Theses and Dissertations

This thesis evaluates the effects of Combined Heating and Power (CHP) systems with a Propane fueled spark ignited engine as prime mover used in a small commercial building. The system was evaluated in five different U.S. cities. The most common operating modes, thermal load following (FTL) and electric load following (FEL) were evaluated, and an optimized operating mode was developed and investigated. The optimized operating mode is a hybrid (FHL) of FEL and FTL operation. Methodology for the derivation and application of these models is presented. Also, the economic effects of Diesel and Natural Gas were investigated. The results for …


Exploration Of The Genomes Of Two Diverse Conifers, Supaphan Thummasuwan Dec 2008

Exploration Of The Genomes Of Two Diverse Conifers, Supaphan Thummasuwan

Theses and Dissertations

My research is focused on advancing understanding of the genomes of two important distantly related conifer species, loblolly pine (Pinus taeda L.) and bald cypress (Taxodium distichum (L.) Rich. var. distichum). Loblolly pine is the most commercially important tree crop in the United States, the major source of pulpwood for paper manufacturing, a source of quality lumber, a prime bioenergy feedstock, and an important part of the ecosystem of the southeastern U.S. Bald cypress is the dominant tree species in the aptly named ¡°cypress swamps¡± of the South.Its ecological importance to the wetlands of the southern U.S. is immeasurable. Moreover, …


Nmr Backbone Chemical Shift Assignments Of The Hvdhfr1:Nadph Binary Complex, Karthikeshwar Vangala Dec 2008

Nmr Backbone Chemical Shift Assignments Of The Hvdhfr1:Nadph Binary Complex, Karthikeshwar Vangala

Theses and Dissertations

Extremophiles are the organisms that survive in environments which are inhospitable to other creatures. This thesis made an attempt to understand the enviromental effects, in particular saline, on enzyme structure by using three dimensional NMR. The enzyme DHFR1 from halophile Haloferaxi volcanii is complexed with its coactor NADPH, and the saline effects on the complex are studied by comparison with its apoenzyme, hvDHFR1. Backbone chemical shift assignments of the hvDHFR1:NADPH complex were attained which can be functional (along with future work) in understanding the effect of salts on enzyme structure, function, and flexibility. A total of 27 amino acids were …


Nutrient Digestibility And Utilization By Cattle Consuming Cotton Gin Mote As A Replacement For Forage, Cassie Marie Welch Dec 2008

Nutrient Digestibility And Utilization By Cattle Consuming Cotton Gin Mote As A Replacement For Forage, Cassie Marie Welch

Theses and Dissertations

Two studies were conducted to evaluate cotton gin mote as a forage replacement by determining nutrient digestibility and nitrogen and energy retention. Three diets were used: 0%, 50%, and 100% mote. Dry matter intake was greatest for steers consuming 100% mote. Digestibility of DM, OM, CP, and energy was least for steers consuming 50% mote and greatest for those consuming 0% mote. Digestibility of NDF and ADF was greatest for steers consuming 0% mote. Fat digestibility was greatest by steers consuming 0% mote and least by steers consuming 100% mote, with those consuming 50% mote being intermediate. Steers consuming 0 …


Population Characteristics Of Interior Double-Crested Cormorants Breeding Across The Southern Border Of Ontario, Jennifer Erin Chastant Dec 2008

Population Characteristics Of Interior Double-Crested Cormorants Breeding Across The Southern Border Of Ontario, Jennifer Erin Chastant

Theses and Dissertations

Interior Double-crested cormorant reproduction was examined on a large geographical scale to evaluate management actions. Three distinct breeding areas across Ontario were selected. Beginning in 2002, over 11,000 preledged cormorants have been marked. During 2006 and 2007, re-observation of banded birds, colony data such as nest, egg, and chick measurements, and island morphology, were collected. Data revealed no significant regional differences in adult size. However, eggs in eastern Lake Ontario (ELO) were larger than North Channel of Lake Huron (NChan) and Lake of the Woods (LOW). Chicks in ELO throughout development were smaller than NChan and LOW. Number of gulls …


Predicting Compliance With Prescribed Organizational Information Security Protocols, Jordan Douglas Shropshire Dec 2008

Predicting Compliance With Prescribed Organizational Information Security Protocols, Jordan Douglas Shropshire

Theses and Dissertations

Why do some employees go out of their way to follow prescribed information security protocols, while others all but ignore organizational information security measures? A body of research known as organizational citizenship behavior provides insight into this issue. Theories of organizational citizenship behavior draw mainly from the psychological and sociological disciplines. They are used to explain the behaviors of employees who act in the best interest of the company, even when they don’t have to. Examples of citizenship behaviors include information sharing, voluntary reduction of compensation, and relinquishment of power for the benefit of the organization (Nathanson & Becker 1973). …


Product Formulation And Consumer Acceptability Of Processed Cheese Made With Different Types Of Cocoas And Chocolates & Product Formulation And Quantitative Descriptive Analysis Of Aged Cheddar Cheese With Different Types Of Chocolate Inclusions, Vishal Kumar Royyala Dec 2008

Product Formulation And Consumer Acceptability Of Processed Cheese Made With Different Types Of Cocoas And Chocolates & Product Formulation And Quantitative Descriptive Analysis Of Aged Cheddar Cheese With Different Types Of Chocolate Inclusions, Vishal Kumar Royyala

Theses and Dissertations

The objectives of this research were to compare different types of cocoa and chocolates in the formulation of processed chocolate cheese and aged Cheddar cheese, and to evaluate sensory, physical, chemical and quality parameters of each. Four different varieties of chocolates were utilized along with other ingredients to prepare processed chocolate cheeses and were tested for consumer acceptability for their basic and critical attributes. Chocolate chips of four different types and proportions were incorporated into Cheddar cheese curd, ripened for 105 days, and a trained panel evaluated the sensory parameters. Results indicated that processed chocolate cheese made with Bordeaux chocolate …


Marital Instability In East Asian Societies: A Comparative Study Of China, Taiwan, And South Korea, Susan Lynne Rich Dec 2008

Marital Instability In East Asian Societies: A Comparative Study Of China, Taiwan, And South Korea, Susan Lynne Rich

Theses and Dissertations

The rising trend in marital instability and divorce is a topic of discussion nearly world-wide. While divorce affects considerably fewer people in non-Western societies, its rising trend and impact are quite alarming. Given the well established findings in the West, it is useful to study divorce and marital instability in non-Western societies so that prior findings from the West can be scrutinized and validated cross-culturally. This study is necessary because the theories developed in the West may not be entirely applicable to non-Western societies and cultural factors may in some cases be more important than socio-economic factors. By using the …


Molecular And Biochemical Analysis Of Water Stress Induced Responses In Grape, Ramesh Katam Dec 2008

Molecular And Biochemical Analysis Of Water Stress Induced Responses In Grape, Ramesh Katam

Theses and Dissertations

Water stress affects vine productivity, disease tolerance, and enological characteristics of grape. Florida Hybrid Bunch grape are developed through hybridization of local grape spp with Vitis vinifera. These cultivars are mostly grown in southeast region of United States. Water deficit conditions resulted due to failure of rains in the region has developed concern among Florida grape growers to increase water use efficiency of grape. The goal of this research is to identify genes and proteins differentially expressed in response to water stress and to correlate these changes with enological characteristics. Investigating transcripts and proteins will allow us to correlate them …


Molecular Dynamics Simulations Of Metals, Bohumir Jelinek Dec 2008

Molecular Dynamics Simulations Of Metals, Bohumir Jelinek

Theses and Dissertations

This dissertation describes the development and testing of modified embedded atom method (MEAM) interatomic potentials for Al, Si, Mg, Cu, Fe, and their alloys, with primary concentration on Mg-Al system. We performed the density functional theory (DFT) based ab initio calculations to determine the structural and elastic properties of element pairs that are impractical to obtain from experimental measurements. Specifically, we estimated the cohesive energy, equilibrium atomic volume, bulk modulus, and elastic moduli of every element pair in the NaCl reference structure. Based on the results of DFT calculations, MEAM parameters for each element pair were constructed. We extensively tested …


Morphological And Physiological Changes In Laying Hens In Various Stages Of Non-Feed Withdrawal Molt, Ann Laster Mcdonald Dec 2008

Morphological And Physiological Changes In Laying Hens In Various Stages Of Non-Feed Withdrawal Molt, Ann Laster Mcdonald

Theses and Dissertations

Molting is a natural occurrence in the Avian species that can include a period of fasting. Animal rights groups view the longepted standard industry practice as inhumane. Based on influences from these groups and the recommendation of its scientific committee, United Egg Producers (UEP) requires members of its Animal Care Certified Program use a noneed withdrawal molting program, even though the morphological and physiological effects of this method have not been studied in depth and the existing literature provides contradictory results. Research regarding how to induce a noneed withdrawal molt has been performed using feed that is nutrient deficient or …


Nitrogen Doping In Low Temperature Halo-Carbon Homoepitaxial Growth Of 4h-Silicon Carbide, Kritsa Chindanon Dec 2008

Nitrogen Doping In Low Temperature Halo-Carbon Homoepitaxial Growth Of 4h-Silicon Carbide, Kritsa Chindanon

Theses and Dissertations

With the low-temperature halo-carbon epitaxial growth technique developed at MSU prior to this work, use of a halo-carbon growth precursor enabled low-temperature homoepitaxial process for 4H-SiC at temperatures below 1300 °C with good quality. Investigations of the nitrogen doping dependence are reported. It has been demonstrated that the efficiency of the nitrogen incorporation may be different for different substrate orientations, with the Cace showing the higher value of doping. The Si/C ratio is known to influence the doping during the epitaxial growth due to the site-competition mechanism. The doping on the Cace showed weak dependence on the Si/C ratio. On …


Responsiveness Of Elementary-Aged Students, With And Without Specific Learning Disabilities, To Interventions For Mathematics Calculation, Masanori Ota Dec 2008

Responsiveness Of Elementary-Aged Students, With And Without Specific Learning Disabilities, To Interventions For Mathematics Calculation, Masanori Ota

Theses and Dissertations

The Response to Intervention (RtI) model is an identification model for Specific Learning Disability (SLD), one of the 13 disability categories identified under the Individual with Disabilities Education Act (IDEA) of 2004. The RtI model has been proposed as an alternative model to the discrepancy model (e.g., intelligence quotient-achievement discrepancy model). In the RtI model, students’ responsiveness (e.g., levels of performance and slopes of progress) yields their eligibility for special education. However, to date, research that examined the validity of the RtI model (e.g., examination of intervention responsiveness with students with academic deficits) has been limited in the area of …


Restoring Blackland Prairies In Mississippi: Remnant-Restored Prairie Comparisons And Techniques For Augmenting Forbs, Andrew Clifford Dailey Dec 2008

Restoring Blackland Prairies In Mississippi: Remnant-Restored Prairie Comparisons And Techniques For Augmenting Forbs, Andrew Clifford Dailey

Theses and Dissertations

One knowledge gap hindering prairie restoration is uncertainty about when a restored prairie communities sufficiently resemble remnant prairie. I surveyed plant communities in remnant prairies, prairies > 5 years post-restoration, and prairies ≤ 5 years post-restoration in Mississippi. Remnants had the greater species richness. Restored prairies had less cover of woody plants and forbs but greatest non-natives. Restored prairies were not similar to remnant prairies (similarity index = 28.9 - 25.9%), primarily because restored prairies had fewer prairie forbs. Thus, restoration may take decades. Transplanting locallyapted prairie forbs into restored prairies may accelerate restoration, but this has not been evaluated adequately. …


Stability Of Catfish Methyl Esters Under Normal Versus Accelerated Storage Conditions, Saowalee Jongrattananon Dec 2008

Stability Of Catfish Methyl Esters Under Normal Versus Accelerated Storage Conditions, Saowalee Jongrattananon

Theses and Dissertations

Oxidative storage stability was conducted to determine the optimum antioxidant for the production of catfish methyl esters (CFME) for use as biodiesel. Peroxide value, anisidine value, 2-thiobarbituric reaction substances, acid value, iodine value, UV absorbance, and induction period were measured. Antioxidant, stability parameters changed over a storage time of one year when stored at 25°C. The CFME were not stable to oxidation without the addition of TBHQ. When stored at 25°C, oxidative parameters indicated that CFME was a stable product that met oxidative stability standards when TBHQ was added. When held at 80°C for 28 days, the samples with TBHQ …


Study Of The Dielectric Degradation Of Xlpe And Epr Power Cables By Switching Impulses, Prakash Shrestha Dec 2008

Study Of The Dielectric Degradation Of Xlpe And Epr Power Cables By Switching Impulses, Prakash Shrestha

Theses and Dissertations

The insulation of the high voltage power cable will be placed under higher electrical stress by switching surges during the power system operation. The switching surge weakens the power cable insulation and it leads to failure of cables. It has a significant effect on the aging of the insulation material that affects the lifetime of the power cables. This research studies the electrical degradation of 15 kV XLPE and EPR power cables insulation by applying 100, 500, 1000 and 5000 switching impulses of 100 kV. The status of the polymer cable insulation aging is evaluated by the measurement of partial …


Teacher Perceptions Of The Centers For Ocean Sciences Education Excellence: Central Gulf Of Mexico Program, Tracie Tingle Sempier Dec 2008

Teacher Perceptions Of The Centers For Ocean Sciences Education Excellence: Central Gulf Of Mexico Program, Tracie Tingle Sempier

Theses and Dissertations

The 12 Centers for Ocean Sciences Education Excellence (COSEE) are funded by the National Science Foundation and are designed to promote creative ways of disseminating marine science research and its importance to the public. The focus of this study is the COSEE Central Gulf of Mexico program which encourages active partnerships between research scientists and teachers. In these collaborative partnerships, teachers and scientists work together to create educational products and disseminate best practices in ocean sciences education. The purpose of this study was to determine whether the lesson plans and curricula created through the Centers for Ocean Sciences Education Excellence: …


Formulation Of A Fruit Slush Using Evaporated Sweet Whey, Reginald Carl Sean Johnson Dec 2008

Formulation Of A Fruit Slush Using Evaporated Sweet Whey, Reginald Carl Sean Johnson

Theses and Dissertations

Wheyruit slush formulas were evaluated prior to consumer testing of pre-selected formulated beverages. Varying ingredients were prepared in accordance to a factorial design of maximum use of whey and minimum use of additional ingredients. Whey was obtained from the Mississippi State University Dairy Processing Plant and evaporated. The evaporated sweet whey was combined with blueberries, cherry concentrate, Splenda®, water and ice. Sensory tests were conducted to evaluate appearance, flavor and overall acceptability of formulations. Panelists were asked to participate in a survey to elaborate personal perceptions of the products. Formulation of 125mL whey and 30g blueberries had the higher acceptability …


Guest Intercalation Into Metal Halide Inorganic-Organic Layered Perovskite Hybrid Solids And Hydrothermal Synthesis Of Tin Oxide Spheres, Nilantha Bandara Dec 2008

Guest Intercalation Into Metal Halide Inorganic-Organic Layered Perovskite Hybrid Solids And Hydrothermal Synthesis Of Tin Oxide Spheres, Nilantha Bandara

Theses and Dissertations

The work presented in this thesis is divided into two research areas. In part I, the synthesis and guest intercalation of inorganic-organic metal halide ammonium layered perovskites is discussed. Comparisons are made between the solid matrix before and after the intercalations, and all solids are characterized using thermogravimetric analysis (TGA) and powder X-ray diffraction (XRD). In part II, “templateree” hydrothermal synthesis of tin oxide spheres in the presence of different ortho-substituted anilines is discussed. The aim is to determine whether there are differences in the structures, shapes and surface morphology of the tin oxide spheres that correspond to the identity/shape …