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Surface Interactions Between Nickel Ions And Sodium Dodecyl Sulfate, Ralph Edward Coleman

Masters Theses

"In this research the interaction of nickel ions with the surfactant sodium dodecyl sulfate at the liquid-air interface was studied. Surface tension measurements were performed on pure sodium dodecyl sulfate solutions, with and without the addition of nickel ions. Results of these measurements showed that the addition of nickel ions lowered the equilibrium surface tension values of pure sodium dodecyl sulfate solutions and shifted the critical micelle concentration to lower concentrations. The foam fractionation technique was used to determine if the nickel ions could be removed from surfactant solutions. It was found that the removal of nickel ions was influenced …

Engineering Properties Of Bloomington-Normal Subsoils, Rohn Dunseth Abbott

Masters Theses

"The glacial subsoils of the Bloomington-Normal, Illinois area have been analyzed with regard to their engineering properties. Several boring logs are included to illustrate the horizontal and vertical variability in soil units encountered and in the engineering properties of these soil units. The engineering properties of the two most common foundation soils, the Bloomington and Normal tills are compared and special consideration is given to evaluating the compressibility of these materials. Evidence is presented that indicates that the circumferential trimming of a highly preconsolidated soil containing stones can cause significant sample disturbance. Special sampling techniques which eliminate circumferential trimming yield …

Analytical And Experimental Methods For Determining The Properties Of Materials At Very High Rates Of Loading, A. G. Behring

Masters Theses

"In the following report, some of the properties of ALCOA 7075 T651 aluminum, when subjected to high rates of loading, are experimentally investigated by impacting two rods of the material longitudinally. One rod is accelerated to a uniform velocity with an air gun launcher. The stationary second rod is instrumented with strain gages on its lateral surface in order to determine the strain-time history following impact. A detailed description of the experimental equipment is included. Simple, one-dimensional theory is used to determine the dynamic, elastic modulus of the test material under the impact condition. Several observations regarding the behavior of …

The Design Of A Hybrid Computer System, James Joseph Becker

Masters Theses

"Three typical hybrid computers in industry and educational institutions are presented. The hybrid computer designed and built at the University of Missouri at Rolla consists of an SCC-650 digital computer, a TR-48 analog computer, and a hybrid interface. The interface permits the digital computer to control the modes of operation on the analog computer. There are also 9 multiple-pole relays on the interface that can be controlled by the digital computer. A 320 hold removable patchboard is included in the interface. There are 40 trunks lines from the analog computer that are present on the patchboard. The 4 digital-to-analog channels …

The Design Of A Tape Deck Controller, Frederick Harold Keeve

Masters Theses

"A controller was built to interface the SCC-650 general purpose digital computer and the Kennedy Model 1400R incremental write/continuous read tape unit. All logic design information, signal lists, and tape deck instructions are included"--Abstract, page ii.

The Design Of A Molten Fueled, Vortex Reactor, For Use As A Rocket Propulsion Device, Robert Philip Schmitt

Masters Theses

"The purpose of this investigation is to design a nuclear reactor which can be used as a rocket propulsion device. The reactor investigated is fueled with a molten uranium-bismuth alloy and utilizes a two phase vortex flow principle. Hydrogen is employed as a coolant and rocket propellant. The hydrogen is heated directly by the fuel thus eliminating the need for heat exchangers. The major part of the investigation consists of a two group neutron diffusion study to show the operational feasibility of this type of reactor and to obtain an optimum design. the study shows that this type of reactor …

Construction Time And Cost Control Using The Ibm Project Management System/360, James Donald Bailey

Masters Theses

"The object of this investigation was to determine the advantages or disadvantages involved in the use of the IBM Project Management system/360 as a time and cost control tool as compared to the methods presently used by construction contractors in the small to medium size range.

The methods used by three construction contractors were investigated in order to acquire a sample of methods presently used.

It was determined from the investigation that a number of advantages could be obtained which would provide better control of a construction project.

It was also decided that a detailed investigation concerning the cost of …

A Numerical (Matrix) Solution For The Vibration Frequencies And Modes Of A Nonuniform Rectangular Plate With Arbitrary Edge Conditions, F. David Utterback

Masters Theses

"The material presented in this thesis is designed to provide the practicing engineer with a practical, approximate method of solution for the increasingly important problem of plate vibrations. The technique presented herein is basically an application of the use of generalized coordinates to describe the elastic and inertial properties of a finite element representation of a nonuniform rectangular plate. The plate will be idealized by utilizing a modification of the grid work technique developed by Hrennifkoff as a lattice work of interconnecting beams. By employing the elastic displacements as generalized coordinates, the only required compatibility conditions are that the displacements …

The Numerical Solution Of Two-Dimensional Fluid Flow Problems, E. David Spong

Masters Theses

"A numerical solution method is developed for the solution of two-dimensional, irrotational and compressible fluid flow problems. The partial differential equation, in terms of the velocity potential, describing the flow is replaced by finite difference equations and the resulting matrix is solved by Gaussian elimination. The method is successfully applied to two subsonic flow problems: a 7.5⁰ wedge and a 6⁰ wedge inlet. The method becomes invalid, as expected, with the appearance of sonic velocity in the flow field. An investigation of the definition of the singularities is made. This indicates that the best agreement with the experimental results for …

Sufficiency Conditions For Constrained Optima, Cheng-Chun Huang

Masters Theses

"The sufficiency conditions for constrained optimization problems are derived through the use of Lagrangian functions and through the introduction of the new concept of "constrained total derivatives." The relations can be used with equality and/or inequality constraints. The sufficiency conditions derived earlier by Phipps were corrected in this work--Abstract, page ii.

Endogenous Metabolism Of Polyporus Sulfureus. : Utilization Of Exogenous Carbohydrates And Fatty Acids, Shu-Mei Wang

Masters Theses

"A strain of Polyporus sulfureus from the collection at the University of Missouri at Rolla was used in this investigation. Organisms of this genus have been reported to produce eburicoic acid in good yield and this was confirmed for the organism used in this study by the isolation and identification of eburicoic acid from the mycelium. Growth studies of this organism showed that 4% malt extract is a better medium than synthetic media containing asparagine, nitrate or nitrate plus 0.5% yeast extract as nitrogen sources. An examination of the pH of the culture medium led to the conclusion that regardless …

Distillation Column Simulation And Control, Hsian T. Chao

Masters Theses

"A 5-component, 10-stage distillation column was simulated by PACTOLUS by use of the hybrid technique. It was found that the digital-analog simulator is completely satisfactory for solving unsteady-state multicomponent distillation problems. A feedforward controller for a distillation column was designed and tested. The effects of feedforward and feedback control on binary system distillation columns were compared by PACTOLUS. It was found that the liquid flow rates, the holdups as well as the number of stages are important factors in the design of a feedforward controller"--Abstract, page ii.

A Study Of Swirling Air Flow In A Converging Nozzle, Charles William Lineberry

Masters Theses

"A study was conducted to determine the behavior of swirling air flow in a converging nozzle. Special instrumentation was constructed to obtain radial traverses of the flow at four axial positions. the data collected consisted of velocity, static pressure, and stagnation temperature. The flow pattern demonstrated the Ranque-Hilsh effect and reversed axial flow in the core region. As the flow entered the nozzle, it had the characteristics of a free vortex. At the exit plane the characteristics were those of a forced vortex. The converging nozzle caused an increase in the magnitude of the axial velocity component"--Abstract, page ii.

An Experimental Method Of Determining The Thermal Accommodation Coefficients Of Metallic Surfaces, Raymond John Dethorne

Masters Theses

"In the free molecule regime, Knudsen number greater than 10, heat is transferred from a solid by radiation and conduction. The ability of a surface to emit radiant energy is governed by a surface property called emittance while the surface property which apparently regulates the amount of heat transferred by conduction is called the thermal accommodation coefficient. This thesis presents the results of an experimental investigation to determine a relationship between these two properties, emittance and thermal accommodation coefficient. A test apparatus was constructed to measure both the radiation and conduction contributions between two concentric cylinders. cylinders of aluminum and …

Compressive Creep Of Basic Refractories, Maurice E. Green

Masters Theses

"The microstructure and mineralogical composition of direct bonded, 50 wt.% magnesia - 50 wt.% chrome ore refractory compositions containing controlled additions of silica were correlated with their compressive creep behavior in the temperature range 1450⁰ to 1550⁰C under stresses of 100 to 175 psi. Steady state creep rates were determined from the linear regression of the steady state regions of deformation on time. Apparent activation energies and deformation flow characteristics were determined from the temperature and stress dependence of the steady state creep rates. Silica contents up to 3.5 wt.% increased the amount of direct intergranular bonding which decreased the …

Kinetics Of The Formation Of Strontium Zirconate, W. H. Parker

Masters Theses

"The decomposition rate of strontium carbonate (SrC0₃) was measured using a TGA apparatus. It was found to deviate slightly from zero order classical reaction. The rate of formation of strontium zirconate (SrZr0₃) from zirconium oxide (ZrO₂) and strontium oxide (SrO) in the form of the decomposition product of SrCO₃ was measured using quantitative x-ray diffraction for mineralogical analysis. It was found to most nearly follow the Zhuravlev-Lesokhin-Tempel' man rate equation. The rate of decomposition of strontium carbonate was found to be more rapid than the rate of formation of strontium zirconate such that for the most part strontium oxide is …

Spacing Of Explosive Charges, Calvin J. Konya

Masters Theses

"It is generally believed that the spacing of simultaneously initiated collar primed multiple charges is not dependent on the charge length. The stresses generated by explosive charges have been assumed to propagate through a material in a cylindrical manner. this assumption implied that the stress generated in any plane along the charge diameter would have been uniform in magnitude and direction. A finite explosive velocity along with a conical stress wave causes the stresses near the collar to differ from those farther down the column. for this reason, the spacing of charges would be dependent on charge length. An experimental …

Thermal Runaway In Power Transistors, Jerry H. Lee

Masters Theses

"Considerable work has been done on the theory of thermal runaway and the relationship between transistor junction temperature and collector power dissipation. The first part of this thesis is a review of literature. An equation for the normalized junction temperature and its peak value is developed. From this equation, the junction temperature at the thermal runaway point for a given maximum power dissipation could be determined. The second part of this thesis is experimental. The author examined the thermal runaway points for eight different transistors in the basic common emitter class A circuit which operated under no signal DC conditions"--Abstract, …

Radiation And Annealing Characteristics In Neutron Bombarded Transistors Operated In The Inverse Configuration, Lo-Soun Su

Masters Theses

"When operating a silicon planar epitaxial transistor in the inverse configuration (i.e., with the emitter functioning as a collector and the collector functioning an emitter) the bulk space-charge volume of the new "emitter-base" junction is increased by a factor of 26.5 times that of the normal emitter-base junction. The carrier concentration in the new "emitter" is decreased by five orders of magnitude from that of the normal emitter, thus making it easier to investigate the effects of neutron radiation on the space-charge region and at the surface. Experiments using biasing of the new "emitter-base" junction during neutron radiation to change …

An Intragastric Ph And Motility Monitoring And Automatic Titration System, Barry Foster Maycock

Masters Theses

"Knowledge of the effects of prolonged states of weightlessness on the physiological activities of gastric motility and acid secretion will aid in the planning of future space flights, since aberrations in these activities could affect the performance of astronauts. Investigation of these activities requires monitoring of the pressure and pH in the stomach and titration of the gastric contents. Since previous methods and equipment used for performing these functions are inadequate for this investigation, the equipment whose design and operation are discussed in this thesis was developed. This equipment includes an ingestible sensor capsule which is tethered in the stomach, …

The Downhole Suspension And Testing Of An Electrodynamic Shear Wave Exciter, Robert Franklin Kehrman

Masters Theses

"The work in this research project was aimed at designing a Downhole Electromagnetic Shear Wave Generator capable of delivering a wide frequency band, random, continuous signal. This Exciter was built using a compressed-air driven piston assembly for downhole application. The device was tested in the laboratory in a concrete test facility. It proved to be capable of transmitting a continuous, measurable stress into the concrete in a 100 to 5,000 hertz frequency band"--Abstract, page ii.

A Study Of Porous Membrane Evaporation For Desalination In A Flow System, Jing Ming Lee

Masters Theses

"The purpose of this investigation was to study the simultaneous mass and heat transfer mechanism in evaporation through a porous membrane with a non-wettable surface. Such water repellent membranes permit the passage of water vapor, but not liquid water. The investigation concerned the mass transfer rate through the membrane pores with flow on one or both sides of the membrane. The water-repellent membrane separated a hot salt solution from the fresh water, and a copper sheet separated the fresh water from a cold salt solution. A three-channel evaporator-condenser was used, and the membrane consisted of glass fiber paper treated with …

The Decomposition Of 5-Hydroxymethyl-2-Furaldehyde Under Gamma Irradiation, William George Bowles

Masters Theses

"An investigation into the effects of gamma irradiation decomposition of 5-hydroxymethyl-2-furaldehyde (HMF) revealed HMF to be resistant to radiation catalyzed decomposition. A 1.0 normal solution of HMF was irradiated at a dose rate of 4.1 x 10⁵ Rads/hr to a total dose of 8.2 x 10⁶ Rads from a 5000 Curie ⁶⁰Co source. a total of 31 per cent of the HMF decomposed in a zero order reaction, although it was found the HMF decomposed completely under cadmium shielded irradiation in a nuclear reactor with some neutrons present. The reaction rate constant was found to be 4.8 x 10⁻³ moles …

Fast Neutron Induced Resistivity Changes In Order-Disorder Fe₃Al, Bruce A. Betts

Masters Theses

"Resistivity measurements were made of ordered, disordered and intermediate states of order-disordered specimens of Fe₃Al while being irradiated by neutrons. All the specimens were irradiated at ambient temperature, approximately 35°C in a modified Bulk Shielding Swimming Pool type reactor. The ordered and near ordered specimens increased in resistivity indicating disordering whereas the disordered and near disordered specimens decreased in resistivity indicating an ordering process was occuring [sic]. By extrapolation, an equilibrium condition was determined and estimated at 130-135 micro-ohms-cm resistivity that would remain constant during irradiation because the ordering and disordering affects of neutron irradiation would be in equilibrium"--Abstract, page …

A Study Of Bismuth Ferrate And Bismuth Manganate In Solid Solution With Lead Titanate, Harris C. Jones

Masters Theses

"A new sample holder for measuring the high frequency dielectric constant of ferroelectrics at high temperature was constructed. The new sample holder eliminated discontinuities in the slotted line and improved the electrical contact between the ceramic and brass components. Measurements of the high frequency dielectric constant of an aged sample of 90% BiFeO₃ - 10% PbTiO₃ were made as a function of temperature using the slotted line technique. The dissipation function for the aged sample was found to have a more normal behavior near the Curie point than the virgin samples previously measured. Resistivity measurements were made as a function …

Investigation Of Thermal Resistance At The Interface Of Dissimilar And Similar Metals, Ching-Liang Lin

Masters Theses

"Experiments have been conducted to investigate the resistance and the effect of the directional heat flow at the interface of metals in contact. The test specimens were cylinders, axially aligned and dead weight loaded. Specimen materials were aluminum, bronze, and steel. The tests were conducted at environment pressures of 5x10⁻⁵ Torr. or less. The dead weight load was kept at 10 lbs. for all tests and the surface roughness for all specimens was from 6 to 8x10⁻⁶ inch. The results of the investigation reveal that the resistance to heat flow at the interface of metals decreases as the interface temperature …

Instrumentation Of A Shock Tube Facility, James Everett West

Masters Theses

"The theory of schlieren and interferometer systems was described and related to studies of shock waves in a shock tube. An interferometer was procured and a schlieren system was modified for use with the UMR shock tube facility. The design and construction of a base for the systems and window assemblies for the shock tube comprised the major portion of the work on this project. A short series of tests were run to ascertain the compatibility of the instrumentation to the UMR shock tube facility. While no schlieren photograph of the shock wave was obtained, the system was shown to …

Constant Horizontal Force Machining Through Flash Welded Steel Bars Of Varying Hardness, Donald Naeger

Masters Theses

"The purpose of this experiment was to determine the effect of a constant horizontal force applied to the carriage of a lathe as it turned a piece of stock which consisted of two steel bars, of different hardness, flash welded together. This experiment was performed on a lathe to which a pulley system with a mechanical advantage of six was attached to the carriage. The strain on the tool was measured both in the horizontal and vertical directions by a tool dynamometer on which eight strain gages were mounted. The strain gages were calibrated on a Tinius-Olsen testing machine. The …

An Intensity Regulation System For A Monochromator, David A. Wayne

Masters Theses

"In the investigation of phenomena involving both optical intensity and wavelength, an instrument is often desired which allows one of the quantities to be held constant while the other is varied. A relatively inexpensive system is described which utilizes a commercial grating monochromator and external feedback electronics to regulate the output intensity as the wavelength is varied. In this system, a sample of the output intensity is taken by a photosensor with known spectral response. The output of the photosensor is then compared electronically with that of a pre-programmed function generator which cancels nonlinearities in the photo-sensor. The resulting signal …

The Effect Of Prior Cold Work On The Pressure Welding Of Ferritic Nodular Iron, Ronald Morris Ledbetter

Masters Theses

"The purpose of this investigation was to determine the effect of prior cold work by swaging on the pressure welding of ferritic nodular iron. Test pressure welds were produced from continuously cast ferritic nodular iron in the as cast condition and with prior cold work of 20, 30, 40, and 50 per cent reductions in area. Welding pressures of 23,500 psi, 35,300 psi, and 47,100 psi were employed. All welds were made at interface temperatures of 2000°F. Welds made with the as cast material at high welding pressures possessed relatively low tensile strengths due to the creation of planes of …