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12th Annual Rocky Mountain Spectroscopy Conference

Rocky Mountain Conference on Magnetic Resonance

Program and abstracts from the 12th annual meeting of the Rocky Mountain Spectroscopy Conference, sponsored by the Rocky Mountain Section of the Society for Applied Spectroscopy. Held in Denver, Colorado, August 3-4, 1970.

An Experimental Study Of Lateral Soil Pressures And Moments On Flexible Sheet Piles, James H. Donahue

Civil & Environmental Engineering Theses & Dissertations

In order to study the effect compaction has on lateral earth pressures exerted on and bending moments in steel sheet pile bulkheads, an experimental study was undertaken which employed the placement of a non-cohesive soil at two specific densities against three model piles of varying thicknesses. The soil was placed both in a loose and a dense state and the bending strains and deflections of the sheet piles were measured at various stages of backfill. Surface loadings were then placed after completion of the backfilling to observe the effects these loads had on the bending moments. The results of the …

The Microstructure Of Hardened Gypsum Pastes, Raafat Ishak Abdel Malek

Archived Theses and Dissertations

No abstract provided.

A Comparative Study Of The Inorganic Composition In Body Fluids Of Four Egyptian Tick Species, Samir Fouad Araman

Archived Theses and Dissertations

No abstract provided.

Traps And Trap Distribution In Commercial Zinc Sulphides Phosphors Silver Activated And Poisoned With Cobalt, Zohra Safinaz El Calamawy

Archived Theses and Dissertations

No abstract provided.

Switching Characteristics Of Calcium Borate Glasses Containing Iron, Mahmoud Aly El Hamamsy

Archived Theses and Dissertations

No abstract provided.

Wood Flour Molding, Charles Reed Snyder

Graduate Research Papers

The purposes of this research are briefly stated in the following:

1. Develop an understanding of the values of an industrial process through the use of raw materials and laboratory equipment.

2. Investigate wood flour molding and its relation to industry.

3. Experiment with materials, laboratory equipment, and wood flour mixtures to produce a molded article.

4. Develop an instructional unit for use in an industrial arts curriculum.

Jigs And Fixtures In Wood Industries, Arno K. Grabe

Graduate Research Papers

As an integral part of most woodworking industries, jigs and fixtures are worthy of some study. There is very little evidence of written material covering the topic even though the use of many of these devices is widespread throughout industry. The fact that these devices normally result in a substantial saving in production costs can often make them an important facet of a firm's business.

This saving can be accomplished in a number of different ways: use of unskilled workers, standardization of parts, interchangeability of pieces, reduction of safety hazards, and lowering of production time. Not all points will apply …

Electron Emitter Tips And Method, P. D. Ownby

Materials Science and Engineering Faculty Research & Creative Works

Boron is deposited on the (110) plane facet at the center of a tungsten electron emitter tip by chemical vapor deposition of boron triiodide. The emission current density is greatest in the center of the emitting area (FIG. 2).

Diffusion And Internal Friction In Sodium-Rubidium Silicate Glasses, Gary L. Mcvay

Doctoral Dissertations

"The internal friction and self diffusion coefficients of sodium and rubidium ions for (1 - X) Na₂O·X Rb₂O·3 SiO₂ glasses have been measured. The diffusion measurements employed radioactive isotopes and a thin sectioning technique and extended from 350 to 500°C. Internal friction measurements were made from -150 to 500°C and at frequencies of 0.05 to 6000 Hz. The maximum height for the mixed alkali internal friction peak occurs at the composition where the sodium and rubidium diffusion coefficients are equal. It is concluded that the mechanism responsible for the mixed alkali peak is a cooperative rearrangement of sodium-rubidium ions and …

Voids In Neutron Irradiated Aluminum, Nicholas H. Packan

Doctoral Dissertations

"Void formation in high purity aluminum resulting from irradiation to fluences between 1.5 x 10¹⁹ and 1.6 x 10²² neutrons/cm² (E > 0 .1 MeV) at a temperature of 55 ± 5ºC was studied, primarily by means of transmission electron microscopy. In particular the effects of neutron fluence and flux were examined, as well as the possible influences of both preexisting and transmutation-produced impurities. A very low concentration of voids (about 10¹²/cm³) resulted from irradiation to 1.5 x 10¹⁹ neutrons/cm²; they averaged about 150 Å in diameter. Void concentrations and sizes increased with fluence, reaching values of 6 x 10¹⁴ voids/cm³ …

Temperature Variation In Distribution Of Relaxation Times In Aluminosilicate Glasses, David Wayne Moore

Doctoral Dissertations

"The distribution of relaxation times for the alkali peak in a Li₂ O·A1₂O₃ ·2.0SiO₂ glass and for the mixed alkali peak in a 0.5Li₂O·0.5Na₂O·A1₂O₃·2.OSiO₂ glass was studied using the internal friction technique. A lognormal distribution of relaxation times provided the best agreement with the experimental data. The ß parameter of the lognormal distribution function, which is related to the half-height peak width, varied with temperature, indicating that the distribution of relaxation times is dependent upon the activation energy and the activation entropy of the relaxation mechanism. The major contributor to the distribution of relaxation times is a wide distribution in …

The Deformation Mechanisms In Sublimed Magnesium Under Cyclic Loading, Babu Narian Thakur

Doctoral Dissertations

"A detailed study of the deformation processes in sublimed magnesium under reverse bending fatigue in air at room temperature has been undertaken utilizing the light, scanning and transmission electron microscopy. The Principal deformation modes are the basal slip and {10Ī2} twinning. The proportion of twinning increases markedly with the increasing stress level and the number of cycles. The evidence for cross slip is seen on the basal slip bands. The extrusions are seen not only along the basal slip lines but also along the {10Ī2} twin boundaries. In the later stages of fatigue, the extrusions chip off producing a notch …

Electrode Reactions In Zinc Electrolysis, Ernest R. Cole

Doctoral Dissertations

"The effects of temperatures from 0°C to 50°C and current densities from 10 asf to 200 asf on the current efficiency in the electrolysis of pure zinc sulfate solutions (65 gpl Zn⁺⁺ - 200 gpl H₂SO₄) were determined. Pure platinum and platinum coated titanium anodes were used with an aluminum cathode. Platinum anodes were not inert at certain combinations of temperature and current density, and platinum acted as a low overvoltage impurity causing resolution of the cathode deposit. Orientation of the zinc deposits was found to vary with temperature and to have a distinct relationship to current efficiency. Preconditioning of …

The Oxidation Kinetics Of Liquid Lead And Lead Alloys, Thomas Edward Weyand

Doctoral Dissertations

"Liquid lead and lead-silver alloys were investigated to determine the rates and products of oxidation in pure oxygen at temperatures of 350 to 600°C. The kinetic data were determined using a Cahn electro-balance. Liquid lead was found to follow a cubic rate of oxidation between 350 and 400°C. A parabolic rate was found at temperatures above 400°C. 0.496% silver and 2.258% silver alloys followed a cubic rate of oxidation from 350 to 550°C and tended to approach a parabolic rate of oxidation above this temperature. Silver additions were found to increase the rate of oxidation as compared to the pure …

Thermal Expansion Of Tetragonal Pbo, Charles A. Sorrell

Materials Science and Engineering Faculty Research & Creative Works

Thermal expansion of tetragonal PbO, investigated by high‐temperature X‐ray diffraction in vacuum, is nearly isotropic, with the coefficient in the c0 direction only slightly greater than that in the a0 direction. Volume thermal expansion is only slightly greater than in massicot. Retardation of the litharge‐massicot transformation is tentatively interpreted as the result of very low oxygen partial pressures caused by catastrophic oxidation of the stainless‐steel sample holder and resulting oxygen scavenging by lead vapor. Copyright © 1970, Wiley Blackwell. All rights reserved

Fracture Surface Energy Determinations Of High Density Polycrystalline Ceramics, Gene Arthur Pahlmann

Masters Theses

"Values of fracture surface energy were measured for steatite, zircon, mullite and four densities of alumina. Rods of these high density materials were cut into thin rectangular specimens which were notched and broken in three-point loading. The resulting load necessary for fracture of the specimens was used to calculate the fracture surface energy of the materials. The value for the steatite was around 20,000 ergs/cm². The values for the zircon and mullite were on the order of 13,000 ergs/cm², and the values for the aluminas ranged from 17,000 to 24,000 ergs/cm²"--Abstract, page ii.

Imperfections In The Ag-In System (Alpha-Phase) And Lattice Parameters Of Cadmium Oxide, Prafulla Maganlal Vora

Masters Theses

"This thesis has been divided into two parts, namely, "Imperfections in the Ag-In System (Alpha-Phase)" and "Lattice Parameters of Cadmium Oxide." Imperfections in the Ag-In System (Alpha-Phase): It can be shown -- as in the case of the Cu-In α solid solutions -- that during quenching from the liquid state, strains are produced by the quenching process and, in addition, vacancies are quenched-in, in the Ag-In α-solid solutions. The number of vacancies present, measured by the decreased density of the alloys, is proportional to the indium content up to the solid-solubility limit. Upon heat treatment of the alloys, the thermal …

Cathodic Behavior Of Co, Co-Fe Alloys And Some Other Metals In Acids In A Cathodic Protection Arrangement, Ram Bajaj

Masters Theses

"During cathodic protection of a corroding metal, electrons are forced into the metal by a sacrificial anode, a battery or a rectifier. These electrons, which constitute the suppressing or external current, are discharged (by H⁺ of the corrosive liquid) on the local cathode of the corroding metal decreasing the emf of the local cells, and, thus, reducing the cell current or the rate of corrosion of the metal. This process was studied in detail by finding out the relationship existing between the cell and suppressing currents. The study was made using two circuits: the cell circuit (representing the local current) …

Etch Patterns On Zone-Refined Fe, M. E. Straumonis, Chang-Soo Kim

Electrical and Computer Engineering Faculty Research & Creative Works

Upon dissolution of zone-refined Fe in strong acids, mainly three kinds of corrosion patterns were observed in the crystallites of the sections. Regardless of the acids, the {110} plane always appeared on the three patterns in the form of smooth and even steps, ledges, or facets. The {112}, {122}, and {123} planes were also developed but to a much lesser degree. The {100} and {111} planes were not observed because grains of the respective orientation were missing on the sections. Attempts were made to explain the formation of the planes by taking into consideration the reticular density of the planes …

Carburization Of Type 316l Stainless Steel In Static Sodium, F. B. Litton, Arthur E. Morris

Materials Science and Engineering Faculty Research & Creative Works

The transport of carbon from an iron-87 wt.% carbon alloy through static sodium to Type 316L stainless steel was investigated at temperatures of interest to the liquid-metal fast-breeder reactor (LMFBR) program. The rate-controlling step for the experimental geometry employed was the diffusion of carbon in the source. © 1970.

Exact Solution For A Model Of Dislocation Pipe Diffusion, J. Mimkes, Manfred Wuttig

Materials Science and Engineering Faculty Research & Creative Works

The dislocations are treated as an ideal array of parallel pipes of radius and diffusivity Dp embedded in the bulk material of the diffusivity Db. The exact solution of this problem of diffusion along semi-infinite edge dislocations is presented for cubic, tetragonal, and hexagonal crystals. The solution makes it possible to evaluate the dislocation pipe radius a and the ratio of diffusivities from one experiment. It is applied to experimental data for self-diffusion in tellurium available in the literature. The results of the calculations are a dislocation pipe radius a=(1.5 0.5)x10-4 cm and an activation energy for the pipe diffusion …

The Smelting Of Lead Drosses, Humberto Adolfo Arzabe

Masters Theses

"The constitution of the matte and bullion obtained by the smelting of lead drosses coming from the cooling of lead blast furnace bullion was investigated by metallographic, chemical, electron-microprobe, and X-ray means. At smelting temperatures (1200°C to 1300°C) two liquid phases are in equilibrium. A liquid lead phase with low concentrations of copper and sulfur, and a lighter liquid matte phase containing a high concentration of copper and sulfur with some dissolved lead. On cooling to room temperature the matte precipitates cuprous sulfide, a eutectic mixture of cuprous sulfide and lead sulfide with a deficiency of sulfur, and metallic lead …

Spheroidization In Tool Steels, Sharad Gajanan Bankar

Masters Theses

"A carbon steel, W1, and four other alloy tool steels, namely, A2, H13, D3, and M2, were spheroidized by five different procedures. Any modification made in the treatments for an individual steel were suggested by the results obtained with these five procedures. The hardnesses and microstructures obtained were compared with steel samples annealed at a tool steel mill. The response given by different steels to various methods of spheroidization was studied. It was found that A2, W1, and D3 steels responded the best to the cycling method whereas the best response to the isothermal annealing was given by H13 and …

Investigation Of The System Al₂O₃-Teo₂-O₂, Vera Zelenkova Sestak

Masters Theses

"The system Al₂O₃-TeO₂-O₂ has been investigated by X-ray diffraction and differential thermal analysis in air and in sealed silica ampoules. The tellurate, Al₂TeO₆, with tellurium in the +6 valence state, forms in air but not in vacuum at 1 mm pressure. A second phase, a tellurite, possibly Al₂Te₂O₇, forms in air or vacuum by devitrification. The glass-forming region is wider than previously stated and is more extensive in vacuum--from 50% to 98% TeO₂. Tentative phase boundaries have been placed for the system in air and vacuum"--Abstract, page ii.

A Systematic Study Of Instrument Variables Upon The Accuracy Of Microprobe Analysis, R. A. Parr

Masters Theses

"The purpose of this investigation was to study the effect of instrument parameter changes upon X-ray intensity measurements of the copper-manganese system. The parameters utilized in this study included: (1) polished, contaminated, and 600 grit surfaces ; (2) constant sample current and constant beam current modes; and (3) 15 KV, 20 KV, and 25 KV accelerating potentials. Inspection of the data disclosed three interesting points: (1) copper and manganese X-ray intensity measurements appear to be a linear function of composition in the 15 KV through 25 KV accelerating potential range; (2) electron backscatter measurements consistently show in a limited range …

Metallographic Study Of Phase Changes In Heat Treated Ductile Iron, Mahendra Vadilal Desai

Masters Theses

"Continuous cast ductile iron samples were hardened. It was found that carbide dissolved in the austenite faster than graphite and that this material requires higher austenitizing temperatures and longer austenitizing time than steels. Tempered microstructures were affected by the prior austenitizing treatment and it appeared that the amount of carbon dissolved in the austenite determined the tempered microstructure. Several attempts to determine the austenite grain size indicated that it is not as easy to determine in ductile iron as in steels. Two techniques, heat etching and an isothermal transformation method, were found to reveal prior austenite grain size. It was …

Investigations Of Several Variables In The Dwight-Lloyd Mcwane Ironmaking Process, James Orlan Hood Jr.

Masters Theses

"The Dwight- Lloyd McWane Ironmaking Process (D-LM) is the first commercial process of its particular type and one of the few commercial processes involving prereduction of iron ore in existence today. This presentation reviews some promising ironmaking processes which involve iron ore prereduction, with special attention being given the D-LM process. Although the D-LM process is continuous from iron ore to high quality molten cast iron, the research and discussion herein is limited to principal variables involved in the production of high quality carbonized pellets in the prereduction phase of the operation. The variables of process temperature and pellet carbon …

Thermal Expansion Of Orthorhombic Pbo, Charles A. Sorrell

Materials Science and Engineering Faculty Research & Creative Works

Thermal expansion of orthorhombic PbO was investigated by high‐temperature X‐ray diffraction. The coefficients in the a0, and c0 directions are equal and Pb–O chains extended in the a0 direction and bonded into layers in the b0 direction; appreciable Pb–Pb bonding is indicated. Coordination and bond distances observed in PbSiO3 and lead silicate glasses, which are similar to those of massicot, and PbnOn polymeric units reported in PbO vapor are interpreted as additional evidence of the importance of PbO chains as structural entities. Copyright © 1970, Wiley Blackwell. All rights reserved

Some Effects Of Oh Groups On Sodium Silicate Glasses, Mokhtar Sayed Maklad

Doctoral Dissertations

"Glasses of various compositions in the Na₂O-SiO₂ system were prepared with different levels of OH concentration. Phase separation kinetics, thermal expansion, radiation induced optical absorption, and internal friction of these glasses were studied. The increase in OH content in these glasses was found to (a) enhance the rate of phase separation; (b) increase thermal expansion above the glass temperature and change the dilatometric softening temperature in a way that depends on microstructure; (c) increase the radiation induced optical absorption bands associated with positive hole centers and decrease those associated with electron trap centers; and, (d) decrease the low temperature alkali …