Physical Sciences and Mathematics Commons^™

The Effects Of Rapid Heating And Cooling On The Composition, Structure, And Superconducting Properties Of Bi-Sr-Ca-Cu-O Compounds, Qing Duan

Dissertations and Theses

Bulk and thin film samples of Bi₂₋[subscript x]Pb[subscript x]Sr₂Ca₂Cu₃O[subscript y] compounds were prepared by suitable methods. The thin film and bulk samples were exposed to argon gas at temperatures of about 2000 °C and pressures of about 300 atm. in a ballistic compressor (BC) and then cooled at a rate of about 10⁵ °C/sec. The samples before and after this treatment were examined and compared using a transmission electron microscope (TEM), a scanning electron microscope (SEM), an energy dispersive spectrometer (EDS) , and an x-ray diffractometer (XRD). Resistance and magnetic susceptibility measurements were made to determine changes in superconducting temperature …