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Fabrication And Superconducting Properties Of Highly Dense Mgb2 Bulk Using A Two-Step Sintering Method, Minoru Maeda, Yue Zhao, Yoshifumi Watanabe, Hiroaki Matsuoka, Y Kubota

Australian Institute for Innovative Materials - Papers

We investigated on microstructure and superconducting properties of high-density MgB₂superconductors synthesized by a heat-treatment method combining a short period of sintering at 1100^°C with a following annealing at a low temperature. The two-step sintering method was found to achieve a coexistence of a high density and broadened XRD full width at half maximum (FWHM) of MgB₂ peak in the samples. The onset of diamagnetism at 5 T was approximately 2 K higher than those of the samples heat-treated by single-step sintering at high or low temperatures. Different second-step annealing temperatures were examined in this work. …