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Articles 1 - 30 of 74
Full-Text Articles in Physical Sciences and Mathematics
Towards The Total Synthesis Of Thioviridamide: Thiyl Radical Approach To The Beta-Thioenamide Linkage Formation, Jung-Hoon Kang
Towards The Total Synthesis Of Thioviridamide: Thiyl Radical Approach To The Beta-Thioenamide Linkage Formation, Jung-Hoon Kang
Theses and Dissertations
We developed an approach to the β-thioenamide linkage contained in the S-(2-aminovinyl)cysteine (avCys) residue of thioviridamide.1,2 Kinetic and thermodynamic control of radical additions of thiols to ynamides were studied for the formation of β-thioenamide linkage. Thiyl radicals are electrophilic and ynamides are electron-rich alkynes. This complementary polarity of the radical and acceptor increases the likelihood of a successful radical addition reaction. Because little is known about these types of compounds (β-thioenamides), we were unsure what kinds of yields and stereoselectivities (cis vs. trans) to expect. The adduct stability is another issue to consider. Fortunately, under typical radical addition conditions, the …
Improving Library Searches Using Word-Correlation Factors And Folksonomies, Maria Soledad Pera
Improving Library Searches Using Word-Correlation Factors And Folksonomies, Maria Soledad Pera
Theses and Dissertations
Libraries, private and public, offer valuable resources to library patrons; however, formulating library queries to retrieve relevant results can be difficult. This occurs because when using a library catalog for library searches, patrons often do not know the exact keywords to be included in a query that match the rigid subject terms (chosen by the Library of Congress) or terms in other fields of a desired library catalog record. These improperly formulated queries often translate into a high percentage of failed searches that retrieve irrelevant results or no results at all. This explains why frustrated library patrons nowadays rely on …
Ontology Generation, Information Harvesting And Semantic Annotation For Machine-Generated Web Pages, Cui Tao
Ontology Generation, Information Harvesting And Semantic Annotation For Machine-Generated Web Pages, Cui Tao
Theses and Dissertations
The current World Wide Web is a web of pages. Users have to guess possible keywords that might lead through search engines to the pages that contain information of interest and browse hundreds or even thousands of the returned pages in order to obtain what they want. This frustrating problem motivates an approach to turn the web of pages into a web of knowledge, so that web users can query the information of interest directly. This dissertation provides a step in this direction and a way to partially overcome the challenges. Specifically, this dissertation shows how to turn machine-generated web …
Dynamic Load Balancing Of Virtual Machines Hosted On Xen, Terry Clyde Wilcox
Dynamic Load Balancing Of Virtual Machines Hosted On Xen, Terry Clyde Wilcox
Theses and Dissertations
Currently systems of virtual machines are load balanced statically which can create load imbalances for systems where the load changes dynamically over time. For throughput and response time of a system to be maximized it is necessary for load to be evenly distributed among each part of the system. We implement a prototype policy engine for the Xen virtual machine monitor which can dynamically load balance virtual machines. We compare the throughput and response time of our system using the cpu2000 and the WEB2005 benchmarks from SPEC. Under the loads we tested, dynamic load balancing had 5%-8% higher throughput than …
Using Geoscience Education Graduate Students To Help Faculty Transform Teaching Practice, Teagan L. Tomlin
Using Geoscience Education Graduate Students To Help Faculty Transform Teaching Practice, Teagan L. Tomlin
Theses and Dissertations
Universities make claims about student learning that graduates don't often achieve and are under pressure to show improvement in teaching and learning in their undergraduate programs. This has been the constant focus of university-level professional development programs, but most teachers are still not using the most effective teaching methods. Individual departments need to find ways to help their instructors overcome three main challenges associated with adopting more effective student-centered teaching methods. No matter what strategy is adopted, instructors need considerable support to 1) change their beliefs about what constitutes effective teaching and learning, 2) learn to effectively implement new strategies, …
Simulation And Analysis Of Cadmium Sulfide Nanoparticles, Chad Everett Junkermeier
Simulation And Analysis Of Cadmium Sulfide Nanoparticles, Chad Everett Junkermeier
Theses and Dissertations
I used ab initio molecular dynamics calculations to model cadmium sulfide nanoparticles. The nanoparticles were originaly spherical, bulk-like zinc-blende structures. Constant temperature molecular dynamics calculations reveals that CdS nanoparticles that are about 2 nm in diameter and have unpassivated surfaces are in an amorphous structure with short range order. The nearest neighbor distance on the surface of the nanoparticles being near the wurtzite nearest neighbor distance. I wrote the program xyzSTATS and used its results in justifying the amorphous nanoparticles claim. I also estimated the band gap of the CdS nanoparticles with unpassivated dangling bonds.
Real-Time Automatic Price Prediction For Ebay Online Trading, Ilya Igorevitch Raykhel
Real-Time Automatic Price Prediction For Ebay Online Trading, Ilya Igorevitch Raykhel
Theses and Dissertations
While Machine Learning is one of the most popular research areas in Computer Science, there are still only a few deployed applications intended for use by the general public. We have developed an exemplary application that can be directly applied to eBay trading. Our system predicts how much an item would sell for on eBay based on that item's attributes. We ran our experiments on the eBay laptop category, with prior trades used as training data. The system implements a feature-weighted k-Nearest Neighbor algorithm, using genetic algorithms to determine feature weights. Our results demonstrate an average prediction error of 16%; …
An Analysis Of Document Retrieval And Clustering Using An Effective Semantic Distance Measure, Nathan Scott Davis
An Analysis Of Document Retrieval And Clustering Using An Effective Semantic Distance Measure, Nathan Scott Davis
Theses and Dissertations
As large amounts of digital information become more and more accessible, the ability to effectively find relevant information is increasingly important. Search engines have historically performed well at finding relevant information by relying primarily on lexical and word based measures. Similarly, standard approaches to organizing and categorizing large amounts of textual information have previously relied on lexical and word based measures to perform grouping or classification tasks. Quite often, however, these processes take place without respect to semantics, or word meanings. This is perhaps due to the fact that the idea of meaningful similarity is naturally qualitative, and thus difficult …
A See-Ability Metric To Improve Mini Unmanned Aerial Vehicle Operator Awareness Using Video Georegistered To Terrain Models, Cameron Howard Engh
A See-Ability Metric To Improve Mini Unmanned Aerial Vehicle Operator Awareness Using Video Georegistered To Terrain Models, Cameron Howard Engh
Theses and Dissertations
Search and rescue operations conducted in wilderness environments can be greatly aided by the use of video filmed from mini-UAVs. While lightweight, inexpensive and easily transportable, these small aircraft suffer from wind buffeting and may produce video that is difficult to search. To aid in the video search process, we have created a system to project video frames into a 3D representation of the search region. This projection allows us to tie each frame of video to a real-world location, enabling a myriad of novel views, mosaics and metrics that can be used to guide the search including a new …
Parameter Estimation For The Beta Distribution, Claire Elayne Bangerter Owen
Parameter Estimation For The Beta Distribution, Claire Elayne Bangerter Owen
Theses and Dissertations
The beta distribution is useful in modeling continuous random variables that lie between 0 and 1, such as proportions and percentages. The beta distribution takes on many different shapes and may be described by two shape parameters, alpha and beta, that can be difficult to estimate. Maximum likelihood and method of moments estimation are possible, though method of moments is much more straightforward. We examine both of these methods here, and compare them to three more proposed methods of parameter estimation: 1) a method used in the Program Evaluation and Review Technique (PERT), 2) a modification of the two-sided power …
The Hybrid Game Architecture: Distributing Bandwidth For Mmogs While Maintaining Central Control, Jared L. Jardine
The Hybrid Game Architecture: Distributing Bandwidth For Mmogs While Maintaining Central Control, Jared L. Jardine
Theses and Dissertations
Current Massively Multi-player Online Games (MMOGs) have enormous server-side bandwidth requirements. The costs of providing this bandwidth is in turn passed on to the consumer in the form of high monthly subscription fees. Prior work has primarily focused on distributing this bandwidth using peer-to-peer architectures, but these architectures have difficulty preventing cheating, overwhelming low resource peers, and maintaining consistent game state. We have developed a hybrid game architecture that combines client-server and peer-to-peer technologies to prevent cheating, maintain centralized and consistent game state, significantly reduce central server bandwidth, and prevent lower capacity players from being overwhelmed. By dramatically reducing the …
Investigating The Margins Of Pleistocene Lake Deposits With High-Resolution Seismic Reflection In Pilot Valley, Utah, John V. South
Investigating The Margins Of Pleistocene Lake Deposits With High-Resolution Seismic Reflection In Pilot Valley, Utah, John V. South
Theses and Dissertations
A vast area of the northeastern Great Basin of the western USA was inundated by a succession of Plio-Pleistocene lakes, including Lake Bonneville (28 ka to 12 ka). The Pilot Valley playa, located just east of the Utah-Nevada border near Wendover, Utah, within the eastern Basin and Range Province, represents an 8 to 16 km wide and ~50 km long remnant of these lakes. The playa corresponds to the upper surface of a closed basin that is delimited by two mountain ranges, which are mantled by recent alluvial fans over which the playa sediments have prograded. In order to investigate …
Photocycloaddition Of Allenes, Crystal Ward
Photocycloaddition Of Allenes, Crystal Ward
Theses and Dissertations
For the past ten years the Fleming research group has been involved in the research of allene compounds. We have explored the synthesis of allenes as well as several reactions involving allenes, such as oxidation and nitrene addition. Recently, we have explored the synthesis and photochemistry of allenic alcohols tethered to silicon. There are literature examples using allenes in synthesis, but very few examples exist using allenes in photochemical cycloaddition reactions. We have found that a diisopropylallenyloxy(cinnamyloxy)silane derivative undergoes [2+2] photochemical cycloaddition to produce a cyclobutylsilane product when irradiated for 60-75 minutes.
Wolfcampian Development Of The Nose Of The Eastern Shelf Of The Midland Basin, Glasscock, Sterling, And Reagan Counties, Texas, Douglas S. Flamm
Wolfcampian Development Of The Nose Of The Eastern Shelf Of The Midland Basin, Glasscock, Sterling, And Reagan Counties, Texas, Douglas S. Flamm
Theses and Dissertations
The nose of the Eastern shelf of the Midland Basin is a prominent structural and depositional feature present in Glasscock, Sterling, and Howard counties, Texas. This feature has been expressed in many regional maps and mentioned in some literature, but has not otherwise been studied significantly. This study looks at the viability of using an acoustic impedance seismic inversion to interpret the 2nd and 3rd order sequence stratigraphy of the southern portion of the nose of the Eastern shelf along with its shelf to basin transition in Glasscock, Sterling, and Reagan counties during the Wolfcampian (Asselian-Sakmarian) time (Early Permian). The …
Biologically Relevant Multiple Sequence Alignment, Hyrum D. Carroll
Biologically Relevant Multiple Sequence Alignment, Hyrum D. Carroll
Theses and Dissertations
Researchers use multiple sequence alignment algorithms to detect conserved regions in genetic sequences and to identify drug docking sites for drug development. In this dissertation, a novel algorithm is presented for using physicochemical properties to increase the accuracy of multiple sequence alignments. Secondary structures are also incorporated in the evaluation function. Additionally, the location of the secondary structures is assimilated into the function. Multiple properties are combined with weights, determined from prediction accuracies of protein secondary structures using artificial neural networks. A new metric, the PPD Score is developed, that captures the average change in physicochemical properties. Using the physicochemical …
Testing Direct Simulation Monte Carlo Methods Against The Fluid Equations In The Inductively Coupled Plasma Mass Spectrometer, William R. Somers
Testing Direct Simulation Monte Carlo Methods Against The Fluid Equations In The Inductively Coupled Plasma Mass Spectrometer, William R. Somers
Theses and Dissertations
A Direct Simulation Monte Carlo fluid dynamics code named FENIX has been employed to study gas flow-through properties of the inductively coupled plasma mass spectrometer (ICP-MS). Simulation data have been tested against the Navier-Stokes and heat equations in order to see if FENIX functions properly. The Navier-Stokes and heat equations have been constructed from simulation data and are compared term by term. This comparison shows that FENIX is able to correctly reproduce fluid dynamics throughout the ICP-MS simulation, with an exception immediately behind the ICP-MS sampler cone, where the continuum criterion for the Navier-Stokes equation is not met. Testing the …
Implementation Of Optical Spectra Calculations In Fireball: A Local-Orbital Density Functional Theory Approach, Ivan Grigoryevich Okhrimenko
Implementation Of Optical Spectra Calculations In Fireball: A Local-Orbital Density Functional Theory Approach, Ivan Grigoryevich Okhrimenko
Theses and Dissertations
We have expanded the capabilities of the ab initio tight-binding molecular dynamics package FIREBALL to include calculations of optical properties. Basic zero order approximation is based on transitions between Kohn-Sham states. Corrections for electron-electron interactions are based on time dependant density functional theory (TDDFT). Consistent with the FIREBALL approach, we use precalculated integrals and approximations to make the program faster.
An Infrastructure For Performance Measurement And Comparison Of Information Retrieval Solutions, Gary Saunders
An Infrastructure For Performance Measurement And Comparison Of Information Retrieval Solutions, Gary Saunders
Theses and Dissertations
The amount of information available on both public and private networks continues to grow at a phenomenal rate. This information is contained within a wide variety of objects, including documents, e-mail archives, medical records, manuals, pictures and music. To be of any value, this data must be easily searchable and accessible. Information Retrieval (IR) is concerned with the ability to find and gain access to relevant information. As electronic data repositories continue to proliferate, so too, grows the variety of methods used to locate and access the information contained therein. Similarly, the introduction of innovative retrieval strategies—and the optimization of …
Autonomous And Intelligent Radio Switching, Quiyi Duan
Autonomous And Intelligent Radio Switching, Quiyi Duan
Theses and Dissertations
With the proliferation of mobile applications and the abundance of wireless devices, it is increasingly common for devices to support multiple radios. When two devices are communicating they should choose the best available radio based on user preference and application requirements. This type of “radio switching” should happen automatically, so that the system optimizes performance dynamically. To achieve this objective, we design an Autonomous and Intelligent Radio Switching (AIRS) system to leverage the radio heterogeneity common in today's wireless devices. The AIRS system consists of three key components. First, we design a radio preference evaluation module to dynamically select the …
Generalized Random Walks, Their Trees, And The Transformation Method Of Option Pricing, Thomas Gordon Stewart
Generalized Random Walks, Their Trees, And The Transformation Method Of Option Pricing, Thomas Gordon Stewart
Theses and Dissertations
The random walk is a powerful model. Chemistry, Physics, and Finance are just a few of the disciplines that model with the random walk. It is clear from its varied uses that despite its simplicity, the simple random walk it very flexible. There is one major drawback, however, to the simple random walk and the geometric random walk. The limiting distribution is either normal, lognormal, or a levy process with infinite variance. This thesis introduces an new random walk aimed at overcoming this drawback. Because the simple random walk and the geometric random walk are special cases of the proposed …
I. Thermodynamics And Magnetism Of Cu2ocl2 Ii. Repairs To Microcalorimeter The "2"S Are Subscripts, And The Second 2 Is Preceded By A Lower Case L, Not A One, Thomas J. Parry
Theses and Dissertations
Adiabatic calorimetry provides accurate and precise specific heat (Cp) data. From this data, thermodynamic functions may be calculated. Cu2OCl2, melanothallite, became of interest as part of a study of a particular thermochemical cycle. The experimental specific heat data and the calculated thermodynamic functions are reported here. Free energies of formation, calculated from the thermodynamic functions, suggest the particular cycle of interest with this compound as an intermediate is not feasible; uncertainty as to the accuracy of CuO and CuCl2 data used in the calculations indicate further study may be necessary. Upon collection of the specific heat data, an antiferromagnetic transition …
A Radical Conjugate Addition Approach To The Total Synthesis Of Celogentin C, Steven G. Capps
A Radical Conjugate Addition Approach To The Total Synthesis Of Celogentin C, Steven G. Capps
Theses and Dissertations
The synthesis of five chiral DBFOX (dibenzofuran-oxazoline) ligands with either aryl or benzyl substituents will be presented. The requisite amino alcohols were obtained with high enantioselectivity either commercially (DBFOX/Bn), via Sharpless asymmetric aminohydroxylation (DBFOX/Nap, DBFOX/t-BuPh, DBFOX/Pip), or via phase-transfer catalyzed asymmetric alkylation (DBFOX/MeNap). These ligands, complexed with Mg(NTf2)2, were used as Lewis acid promoters of enantioselective radical conjugate additions to α/β-unsaturated nitro-amides/esters. A summary of these results is presented and discussed. These findings led us to believe that our initial binding model between metal, ligand, and substrate was flawed. Thus, we figured that if we started with a functionality known …
A Microanalytical Approach To Understanding The Origin Of Cumulate Xenoliths From Mauna Kea, Hawaii, Megan Pickard
A Microanalytical Approach To Understanding The Origin Of Cumulate Xenoliths From Mauna Kea, Hawaii, Megan Pickard
Theses and Dissertations
Cumulate xenoliths erupted with alkalic hawaiite lavas from a postshield cinder cone on Mauna Kea, Hawaii include a variety of mafic and ultramafic rock types. Previous studies of major and trace element compositions of minerals in the xenoliths are interpreted to show transitional to alkalic magma parentages from the postshield stage, although any orthopyroxene-bearing xenoliths are considered to have tholeiitic parents. Major element compositions minerals were analyzed using the electron microprobe and trace element compositions of clinopyroxene grains were analyzed by laser ablation inductively coupled plasma mass spectrometry. In this study, major element compositions of clinopyroxene, olivine and plagioclase grains …
On Autonomous Multi-Agent Control In Wilderness Search And Rescue: A Mixed Initiative Approach, Benjamin C. Hardin
On Autonomous Multi-Agent Control In Wilderness Search And Rescue: A Mixed Initiative Approach, Benjamin C. Hardin
Theses and Dissertations
Searching for lost people in a Wilderness Search and Rescue (WiSAR) scenario is a task that can benefit from large numbers of agents, some of whom may be robotic. These agents may have differing levels of autonomy, determined by the set of tasks they are performing. In addition, the level of autonomy that results in the best performance may change due to varying workload or other factors. Allowing a supervisor and a searcher to jointly decide the correct level of autonomy for a given situation (“mixed initiative”) results in better overall performance than giving an agent absolute control over their …
Magmatic Sulfur And Chlorine Abundances At Stromboli, Italy And Their Role In The Formation Of Vesicle-Hosted Metal Alloys, Nichelle Lynn Baxter
Magmatic Sulfur And Chlorine Abundances At Stromboli, Italy And Their Role In The Formation Of Vesicle-Hosted Metal Alloys, Nichelle Lynn Baxter
Theses and Dissertations
Strand et al. (2002) discovered small metal alloy grains rich in Cu, Co, and Sn (maximum size 150 µm) in vesicles of lava from Kilauea Volcano. These alloys are also found in basaltic rocks of several Italian volcanoes. To better understand the origin of these metal-rich grains, bombs from Stromboli Volcano were examined. Two bomb types were collected from Stromboli: pumiceous bombs and scoriaceous bombs. Bulk rock trace element geochemistry indicates that there are no significant differences in Cu, Co, or Sn (the three major components of the metal alloys) between the pumiceous and scoriaceous bombs. Comparison of olivine melt …
Regulators Of G-Protein Signaling, Rgs13 And Rgs16, Are Associated With Cxcl12-Mediated Cd4+ T Cell Migration, Lijin Xia
Theses and Dissertations
Chemokines are important chemical signals that guide lymphocyte movement within the immune system and promote the organization and functions of germinal centers (GCs) in the secondary lymphoid tissues. Previous studies have shown that GC T cells exhibit high expression of chemokine receptor 4, CXCR4, but that these cells are unable to migrate to the ligand for this receptor, the chemokine CXCL12. This “migratory paralysis” to CXCL12 was found to be correlated with the expression of two Regulators of G-protein Signaling, RGS13 and RGS16 in the GC T cells. The objective of my research was to determine whether RGS13 and RGS16 …
Pre-Eruptive Conditions Of The Oligocene Wah Wah Springs Tuff, Southeastern Great Basin Ignimbrite Province, Kurtus Steven Woolf
Pre-Eruptive Conditions Of The Oligocene Wah Wah Springs Tuff, Southeastern Great Basin Ignimbrite Province, Kurtus Steven Woolf
Theses and Dissertations
The Wah Wah Springs Tuff (30.0 Ma) is one of several very large volume ash-flow tuffs (>3200 km³ of erupted magma) that were emplaced near the peak of the flare-up of activity in the Great Basin ignimbrite province of western North America. It can be characterized as a "monotonous intermediate" ignimbrite because of its intermediate concentrations of silica (~63 to ~70 wt. %), apparent uniform chemical and mineralogical characteristics, and crystal-rich nature (32 ± 10 % phenocrysts on a dense rock basis). The major phase assemblage found throughout deposit is similar to other monotonous intermediates with a few exceptions …
Spectroscopic Study Of Compressible Mobile Phase And Stationary Phase Behavior In Chromatography, Lawrence R. Baker
Spectroscopic Study Of Compressible Mobile Phase And Stationary Phase Behavior In Chromatography, Lawrence R. Baker
Theses and Dissertations
Raman spectroscopy, laser-induced fluorescence, and sum-frequency generation (SFG) spectroscopy are used to investigate the behavior of compressible mobile phases and stationary phases under a variety of chromatographic conditions. Efforts to understand and optimize separations employing compressible mobile phases have been limited by a lack of understanding of the mobile phase density gradient. Mobile phase compressibility leads to gradients in linear velocity and solute retention and affects separation speed and efficiency, especially in packed columns. This work describes on-column density measurement of CO2, a common carrier fluid for SFC and SGC, in packed capillary columns using Raman microspectroscopy. On-column detection by …
Assessing Multivariate Heritability Through Nonparametric Methods, Benjamin Alan Carper
Assessing Multivariate Heritability Through Nonparametric Methods, Benjamin Alan Carper
Theses and Dissertations
The similarities between generations of living subjects are often quantified by heritability. By distinguishing genotypic variation, or variation due to parental pairings, from phenotypic variation, or normal intraspecies variation, the heritability of traits can be estimated. Due to the multivariate nature of many traits, such as size and shape, computation of heritability can be difficult. Also, assessment of the variation of the heritability estimate is extremely difficult. This study uses nonparametric methods, namely the randomization test and the bootstrap, to obtain both a measure of the extremity of the observed heritability and an assessment of the uncertainty.
Theory And Estimation Of Acoustic Intensity And Energy Density, Derek C. Thomas
Theory And Estimation Of Acoustic Intensity And Energy Density, Derek C. Thomas
Theses and Dissertations
In order to facilitate the acquisition and accurate interpretation of intensity and energy density data in high-amplitude pressure fields, the expressions for intensity and energy density are examined to ascertain the impact of nonlinear processes on the standard expressions. Measurement techniques for estimating acoustic particle velocity are presented. The finite-difference method is developed in an alternate manner and presented along with bias and confidence estimates. Additionally, two new methods for estimating the local particle velocity are presented. These methods appears to eliminate the errors and bias associated with the finite-difference technique for certain cases.