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Geology

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Augustana College

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Raman

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Effects Of Heat Treatment Of Spinels As Determined By Vis/Nir And Raman Spectroscopy And Xrd, Jill Reale, Dr. Michael B. Wolf Jun 2019

Effects Of Heat Treatment Of Spinels As Determined By Vis/Nir And Raman Spectroscopy And Xrd, Jill Reale, Dr. Michael B. Wolf

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Heat treatment is done to improve the color and clarity and, therefore, the value of gemstones. The objectives of this study include observing color and inclusion changes in pink spinels after heat treatment, and analyzing structural changes within differently colored spinels using Raman Spectroscopy and X-ray diffraction with a Paris Edinburgh Press. We expected the heat treatment to yield color changes and fading of small inclusions. Cut and polished spinels were heated to 1400C for 2 days or 850C for 3 days. Future experiments involve 800C, 750C, and 700C all for 1 week, 1500C for 4 days, and 1600C for …