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Supercritical Fluid Extraction (Sfe) And High Performance Liquid Chromotography (Hplc) Analysis Of Polycyclic Aromatic Hydrocarbon (Pah) Contaminated Soil, Marie Renee Gargas
Supercritical Fluid Extraction (Sfe) And High Performance Liquid Chromotography (Hplc) Analysis Of Polycyclic Aromatic Hydrocarbon (Pah) Contaminated Soil, Marie Renee Gargas
Theses
Methods for the extraction and analysis of polycyclic aromatic hydrocarbons (PAHs) from contaminated soil were evaluated for use in a treatability study. Candidate procedures were selected from EPA SW-846 (Third Edition) methods. Soxhlet extraction (3540B) was selected to determine initial PAH concentrations. Supercritical fluid extraction with carbon dioxide (SFE: 3561) and high performance liquid chromatography (HPLC: 8310) were evaluated for use as the extraction and analysis methods. Experimental soil was obtained from a petroleum product refinery site; a Certified Reference Material (CRM) was also studied.
Experiments focused on determining concentrations of anthracene, chrysene, fluoranthene, phenanthrene, and pyrene in untreated experimental …