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Physical Sciences and Mathematics Commons

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Environmental Sciences

Theses

Theses/Dissertations

1989

Gas chromatography

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Full-Text Articles in Physical Sciences and Mathematics

Organics In Ambient Air By Collection On Tenax, Thermal Desorption,And Capillary Chromatography With Parallel Fid/Ecd Analysis, Chih-Hsiang Liao May 1989

Organics In Ambient Air By Collection On Tenax, Thermal Desorption,And Capillary Chromatography With Parallel Fid/Ecd Analysis, Chih-Hsiang Liao

Theses

Volatile organics in ambient air were regularly collected on Tenax cartridges at high (10 ml/min) and low (5 ml/min) intake flows. These Tenax samples were analyzed by using a Tekmar Automatic Thermal Desorber and capillary GC system with parallel flame ionization (FID) and electron capture detectors (ECD). A series of quality assurance procedures has been established to improve and assure the accuracy and precision of sample collector and analysis. These procedures relate to performance of the Tekmar thermal desorber, recovery efficiency from the Tenax, and include studies on breakthrough and co-elution. The results demonstrate (1) that from ambient air data …