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Contamination Mitigation Strategies For Scanning Transmission Electron Microscopy, David R. G Mitchell Jan 2015

Contamination Mitigation Strategies For Scanning Transmission Electron Microscopy, David R. G Mitchell

Australian Institute for Innovative Materials - Papers

Modern scanning transmission electron microscopy (STEM) enables imaging and microanalysis at very high magnification. In the case of aberration-corrected STEM, atomic resolution is readily achieved. However, the electron fluxes used may be up to three orders of magnitude greater than those typically employed in conventional STEM. Since specimen contamination often increases with electron flux, specimen cleanliness is a critical factor in obtaining meaningful data when carrying out high magnification STEM. A range of different specimen cleaning methods have been applied to a variety of specimen types. The contamination rate has been measured quantitatively to assess the effectiveness of cleaning. The …