Physical Sciences and Mathematics Commons^™

Mass Spectra Correlations And The Appearance Potentials Of The Major Tobacco Alkaloids, William Frederick Kuhn

Master's Theses

The main objectives of this investigation were three­ fold: (1) to design and fabricate a heated inlet system for the mass spectrometer; (2) to obtain the mass spectra of the major tobacco alkaloids under normal operating conditions; and ( 3) to determine the ionization potentials of the alkaloids as well as the appearance potentials of some of the major fragment ions derived from the alkaloids.

The mass spectrometer is designed to analyze only materials in the vapor state . Since some materials do not exert sufficient vapor pressure at room temperature under reduced pressure to be analyzed directly, it is …

An Investigation Of The Analysis Of Turpentine By Gas Chromatography, John R. Wagner

Master's Theses

The development of gas chromatography and the publication of data on terpene analysis by this method has lead to this attempt to analyze turpentine by gas chromatography. The work has been limited to Gum Spirits of Turpentine and Steam Distilled Wood Turpentine since these are of chief importance and are the only types commonly retailed in small packages.

There have been three objectives:

1. To develop a method based on gas chromatography for distinguishing between Steam Distilled Wood Turpentine and Gum Spirits of Turpentine, and detection of mixtures and adulteration.

2. To identify as many components of the two turpentines …

A Chromatographic Study Of The Polyphenols In Cured Tobacco, Marvin Dennis Edmonds

Master's Theses

The object of this project was to isolate, separate, and identify the polyphenols in tobacco. Following this, the aim was to develop a method for the quantitative determination of the major polyphenols in tobacco.

Existing methods for the determination of polyphenols in tobacco involve lengthy procedures which are concerned with one or two of the polyphenols rather than the· complete class of compounds. The methods consist of exhaustive extraction procedures, lengthy chromatographic procedures and numerous methods of identification.

Extensive research on the determination of polyphenols by chromatography has been carried out in the field of tobacco and in other fields. …