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Chemistry

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Single-crystal X-ray study

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Full-Text Articles in Physical Sciences and Mathematics

6-[(4-Hydroxyphenyl)Diazenyl]- 1,10-Phenanthrolin-1-Ium Chloride Monohydrate, Akram Hazeen, Yan Zhang, Minchong Mao, Kraig A. Wheeler, Mark E. Mcguire Oct 2011

6-[(4-Hydroxyphenyl)Diazenyl]- 1,10-Phenanthrolin-1-Ium Chloride Monohydrate, Akram Hazeen, Yan Zhang, Minchong Mao, Kraig A. Wheeler, Mark E. Mcguire

Kraig A. Wheeler

In the cation of the title molecular salt, C18H13N4O+_Cl__H2O, the dihedral angle between the mean planes of the 1,10- phenanthroline system and the phenol ring is 14.40 (19)_. The crystal packing is stabilized by O—H_ _ _O hydrogen bonds, weak N—H_ _ _Cl and O—H_ _ _Cl intermolecular interactions and _—_ stacking interactions [centroid–centroid distance = 3.6944 (13) and 3.9702 (12) [A °]

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10,12-Dimethylpteridino[6,7-F][1,10]- Phenanthroline-11,13(10h,12h)-Dione– Chloroform (1/1), Waynie Olaprath, Jennifer Rodin, Kraig A. Wheeler, Mark E. Mcguire Jan 2010

10,12-Dimethylpteridino[6,7-F][1,10]- Phenanthroline-11,13(10h,12h)-Dione– Chloroform (1/1), Waynie Olaprath, Jennifer Rodin, Kraig A. Wheeler, Mark E. Mcguire

Kraig A. Wheeler

In the title co-crystal, C18H12N6O2_CHCl3, intramolecular Cl3C—H_ _ _N hydrogen-bonding interactions occur between a single CHCl3 and both N atoms at the 1,10-positions on the phenanthroline portion of the molecule. The interplanar distance between inversion-related molecules is 3.241 (2) A ° .

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(+-)-3-Carboxy-2-(Imidazol-3-Ium-1-Yl)- Propanoate, Sara A. Reeb, Marlesa C. Shields, Kraig A. Wheeler Jan 2009

(+-)-3-Carboxy-2-(Imidazol-3-Ium-1-Yl)- Propanoate, Sara A. Reeb, Marlesa C. Shields, Kraig A. Wheeler

Kraig A. Wheeler

The title compound, C7H8N2O4, crystallizes as a zwitterion, with molecules organized into molecular sheets via carboxyl– carboxylate and N+—H_ _ _carboxylate contacts. These sheets are constructed from translationally related molecules that further link to neighboring motifs via _-stacking [centroid– centroid distance 3.504 (3) A ° ] and weak C—H_ _ _O contacts.

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