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Changsha University of Science and Technology
4-dichlorophenoxyacetic acid; synthesis; antibacterial activity
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Full-Text Articles in Life Sciences
Preparation, Characterization And Antibacterial Activity Of O-2,4-Dichlorophenoxyacetic-Oligochitosan, Yuan Xiaoxian, Yue Lin, Jiang Qixing, Liu Xiaoli, Chen Wanwen, Xia Wenshui, Ping Yuan
Preparation, Characterization And Antibacterial Activity Of O-2,4-Dichlorophenoxyacetic-Oligochitosan, Yuan Xiaoxian, Yue Lin, Jiang Qixing, Liu Xiaoli, Chen Wanwen, Xia Wenshui, Ping Yuan
Food and Machinery
The O-2,4-dichlorophenoxyacetic-oligochitosan (Dcpo-O-COS) was synthesized by chitosan oligosaccharide (COS) and 2,4-dichlorophenoxyacetic acid. The steps were as followed: amino protecting of chitosan oligosaccharide, carboxyl acyl chlorination of 2,4-dichlorophenoxyacetic acid, hydroxyl of COS reacted with acyl chlorination 2,4-dichlorophenoxyacetic acid, amino deprotection. Fourier transform infrared (FTIR), UV-Vis absorption and 1H nuclear magnetic resonance (NMR) were used to characterize the structure of the final product. The results exhibited that Dcpo-O-COS was successfully synthesized. Moreover, both stability, tested by X-ray diffraction (XRD) and Thermogravimetric Analysis (TGA), and antibacterial activity, toresistance to Escherichia coli and Staphylococcus aureus, of Dcpo-O-COS were higher than COS.