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Full-Text Articles in Life Sciences
Determination Of Eight Kinds Of Insecticides In Dairy Products By Dispersed Solid Phase Extraction-Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry, Yan Wan-Ying, He Min-Heng, Wen Heng, Liu Zhi-Peng, Yu Zhi-Cong
Determination Of Eight Kinds Of Insecticides In Dairy Products By Dispersed Solid Phase Extraction-Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry, Yan Wan-Ying, He Min-Heng, Wen Heng, Liu Zhi-Peng, Yu Zhi-Cong
Food and Machinery
Objective: To detect eight kinds of insecticides in dairy products (pure milk, fermented milk, milk powder) rapidly. Methods: A high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) method based on dispersive solid phase extraction pre-treatment technology was established. The samples were extracted with acetonitrile-acetone solution (Vacetonitrile∶Vacetone=80∶20) in ultrasonic way, and the extraction solution was purified by Florisil, primary secondary amine and anhydrous MgSO4.After purification, the samples were analyzed by HPLC-MS/MS qualitatively and quantitatively in multi reaction monitoring (MRM) mode. Results: The correlation coefficient (r) of fenamiphos, imidacloprid, spinosad, dinotefuran, emamectin benzoate, methomyl, …
Efficacy Of Insecticides Against Fall Armyworm, Spodoptera Frugiperda (Lepidoptera, Noctuidae) In Maize, Fawzan Masood Mian, Imtiaz Khan, Najeeb Ullah, Aqarab Husnain Gondal, Muhamad Saqib Ajmal, Muhammad Sajid Qureshi, Adnan Ihsan, Muhammad Raziq, Imran Qazi, Abdul Jabbar
Efficacy Of Insecticides Against Fall Armyworm, Spodoptera Frugiperda (Lepidoptera, Noctuidae) In Maize, Fawzan Masood Mian, Imtiaz Khan, Najeeb Ullah, Aqarab Husnain Gondal, Muhamad Saqib Ajmal, Muhammad Sajid Qureshi, Adnan Ihsan, Muhammad Raziq, Imran Qazi, Abdul Jabbar
Journal of Bioresource Management
Fall armyworm (FAW), Spodoptera frugiperda (Lepidoptera: Noctuidae) is most destructive specie of genus Spodoptera for several agricultural crops. In Pakistan's Sindh province, the invasive fall armyworm Spodoptera frugiperda was first documented causing serious maize damage in 2019. There is need to develop management strategies against this pest in the country. The current study was conducted to check the toxicity of different insecticides against FAW in maize field. The results showed among tested insecticides, deltamethrin was recorded most toxic insecticide followed by chlorantraniliprole and emamectin benzoate. At 1d days after first spray, least number of larvae were recorded with deltamethrin (0.07 …