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Determination Of Eight Kinds Of Insecticides In Dairy Products By Dispersed Solid Phase Extraction-Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry, Yan Wan-Ying, He Min-Heng, Wen Heng, Liu Zhi-Peng, Yu Zhi-Cong
Determination Of Eight Kinds Of Insecticides In Dairy Products By Dispersed Solid Phase Extraction-Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry, Yan Wan-Ying, He Min-Heng, Wen Heng, Liu Zhi-Peng, Yu Zhi-Cong
Food and Machinery
Objective: To detect eight kinds of insecticides in dairy products (pure milk, fermented milk, milk powder) rapidly. Methods: A high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) method based on dispersive solid phase extraction pre-treatment technology was established. The samples were extracted with acetonitrile-acetone solution (Vacetonitrile∶Vacetone=80∶20) in ultrasonic way, and the extraction solution was purified by Florisil, primary secondary amine and anhydrous MgSO4.After purification, the samples were analyzed by HPLC-MS/MS qualitatively and quantitatively in multi reaction monitoring (MRM) mode. Results: The correlation coefficient (r) of fenamiphos, imidacloprid, spinosad, dinotefuran, emamectin benzoate, methomyl, …