Open Access. Powered by Scholars. Published by Universities.®
Articles 1 - 1 of 1
Full-Text Articles in Other Engineering
Microwave-Assisted Synthesis Of Zno Micro-Javelins, Suresh Pillai, Declan Mccormack, John M. Kelly, Sibu C. Padmanabhan
Microwave-Assisted Synthesis Of Zno Micro-Javelins, Suresh Pillai, Declan Mccormack, John M. Kelly, Sibu C. Padmanabhan
Articles
The microwave (MW)-assisted formation of ZnO micro-javelins from zinc nitrate and urea in aqueous solution is described. The particles (named as ‘micro-javelins’ because of their high aspect ratio and needle-like tips) grow hexagonally with well-defined facets in the h0110i direction and pointed tips in (0001) direction. Powder X-ray diffraction patterns show the appearance of a strikingly dominant (1000) orientation. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) investigations reveal the morphological evolution of these hexagonal ZnO particles with time. The effect of precursor concentrations, counterion type andMWirradiation power and their consequent influence on pH and Zn2+ ion concentration are …