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Synthesis And Stabilization Of Gold Nanoparticles From Chloride And Cyanide Systems, Kathryn Ariela Bozer
Synthesis And Stabilization Of Gold Nanoparticles From Chloride And Cyanide Systems, Kathryn Ariela Bozer
Graduate Theses & Non-Theses
Generating gold nanoparticles (AuNPs) from gold chloride solution by precipitating with compounds can be difficult due to the potentially required high temperatures. Tin chloride can be used to overcome this dilemma. The process that is known to make Purple of Cassius is a method where gold chloride and tin chloride solutions are mixed to form AuNPs and tin oxide precipitate. However, it is modified by adding hydrazine to resolubilize the tin oxide and provide a more stable solution for the AuNPs. A three-factor central composite experimentally designed model was created using Design Expert incorporating pH, temperature, and gold concentration as …