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Full-Text Articles in Engineering

Utilizing Waste Latex Paint Toward Improving The Performance Of Concrete, Mohamed Leithy, Eslam Gomaa, Ahmed A. Gheni, Mohamed Elgawady Aug 2023

Utilizing Waste Latex Paint Toward Improving The Performance Of Concrete, Mohamed Leithy, Eslam Gomaa, Ahmed A. Gheni, Mohamed Elgawady

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

In this paper, incorporating the waste latex paint (WLP) into the conventional concrete as a partial replacement of sand to improve its durability was investigated. The fresh and hardened characterizations, in addition to the durability of concrete, were examined. The slump test was used to evaluate the fresh properties, while the hardened properties were evaluated through the volume of voids and absorption rate, in addition to the compressive, splitting tensile, and flexural strengths tests. The durability performance was evaluated by the surface resistivity, bulk electrical resistivity, as well as freeze and thaw resistance tests. The results showed a reduction in …


Development And Characterization Of Coal-Based Thermoplastic Composite Material For Sustainable Construction, Haibin Zhang, Wenyu Liao, Genda Chen, Hongyan Ma Aug 2023

Development And Characterization Of Coal-Based Thermoplastic Composite Material For Sustainable Construction, Haibin Zhang, Wenyu Liao, Genda Chen, Hongyan Ma

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

The exploitation of coal and the disposal of waste plastic present significant environmental and economic challenges that require sustainable and profitable solutions. In response, we propose a renewable construction composite material of coal-based thermoplastic composite (CTC) that can be made from low-grade coal and plastic waste. We developed and tested the hot-press fabrication method for this CTC, using coal with a maximum particle size of 4.75 mm and recycled high-density polyethylene (HDPE). The effects of the coal fraction (50–80 wt.%) on compressive properties, thermal properties, microstructure, and ecological and economic efficiencies of the CTC were investigated. Test results revealed that …


A Strong And Ductile Cobalt-Free Solid-Solution Fe30ni30mn30cr10 Multi-Principal Element Alloy From Hot Rolling, Hans Pommerenke, Jiaqi Duan, Nathan Curtis, Victor Delibera, Adam Bratten, Andrew Hoffman, Mario F. Buchely, Ronald J. O'Malley, Haiming Wen Jul 2023

A Strong And Ductile Cobalt-Free Solid-Solution Fe30ni30mn30cr10 Multi-Principal Element Alloy From Hot Rolling, Hans Pommerenke, Jiaqi Duan, Nathan Curtis, Victor Delibera, Adam Bratten, Andrew Hoffman, Mario F. Buchely, Ronald J. O'Malley, Haiming Wen

Materials Science and Engineering Faculty Research & Creative Works

Most of the Face-Centered Cubic (FCC) Multi-Principal Element Alloys (MPEAs) Developed Thus Far Contain Cobalt. for Many Applications, it is Either required or Beneficial to Avoid Cobalt, Since Cobalt Has Long-Term Activation Issue (For Nuclear Applications), is Expensive, and is Considered a Critical Material. in Addition, FCC Structured Solid-Solution MPEAs Tend to Have Relatively Low Strength. a FCC Solid-Solution Fe30Ni30Mn30Cr10 (At %) MPEA Was Fabricated Via Arc Melting, Followed by Homogenization at 1100 °C for 12 H. the Alloy Was Hot Rolled at 1100 °C with a Total Reduction of Up to 97 %. the Microstructure Was Characterized and Mechanical …


Mechanical Properties Of Zrb2 Ceramics Determined By Two Laboratories, Jeffrey J. Swab, Jecee Jarman, William Fahrenholtz, Jeremy Lee Watts Jan 2023

Mechanical Properties Of Zrb2 Ceramics Determined By Two Laboratories, Jeffrey J. Swab, Jecee Jarman, William Fahrenholtz, Jeremy Lee Watts

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties for zirconium diboride (ZrB2) were measured at two laboratories and compared. Two billets of ZrB2 were prepared by hot-pressing commercial powder. The relative densities of the billets were >99% and with an average grain size of 5.9 ± 4.5 µm. Both laboratories prepared American Society for Testing and Materials (ASTM) C1161 B-bars for strength and ASTM C1421 bars with notch configuration A for fracture toughness. Specimens were machined by diamond grinding at the Army Research Laboratory (ARL) and electrical discharge machining (EDM) at Missouri S&T. Strength bars tested at Missouri S&T were polished to a.25 μm finish …


Effect Of Mechanical Activation On Carbothermal Synthesis And Densification Of Zrc, Nina Obradović, Lun Feng, Suzana Filipović, Miljana Mirković, Darko Kosanović, Jelena Rogan, William Fahrenholtz Jan 2023

Effect Of Mechanical Activation On Carbothermal Synthesis And Densification Of Zrc, Nina Obradović, Lun Feng, Suzana Filipović, Miljana Mirković, Darko Kosanović, Jelena Rogan, William Fahrenholtz

Materials Science and Engineering Faculty Research & Creative Works

Zirconium carbide ceramics were prepared by carbothermal reduction of ZrO2 and C that were mixed by high-energy ball milling. Powders were milled for times from 0 to 120 min in air. As milling time increased, the surface area of the powders increased, indicating significant particle size reduction. Milled powders were reacted at 1600 °C and then densified by spark plasma sintering at 2000 °C, which was sufficient to convert the starting powders to zirconium carbide. Unmilled powders did not reach full density. Milled powders reached full density, but ZrO2 impurities were found for specimens prepared from powders milled …


Strength Retention Of Single-Phase High-Entropy Diboride Ceramics Up To 2000°C, Lun Feng, William Fahrenholtz, Gregory E. Hilmas, Yue Zhou, Jincheng Bai Jan 2023

Strength Retention Of Single-Phase High-Entropy Diboride Ceramics Up To 2000°C, Lun Feng, William Fahrenholtz, Gregory E. Hilmas, Yue Zhou, Jincheng Bai

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties of single-phase (Hf0.2,Nb0.2,Ta0.2,Ti0.2,Zr0.2)B2 ceramics with high purity were investigated. The resulting ceramics had relative density greater than 99%, and an average grain size of 4.3 ± 1.6 μm. At room temperature (RT), the Vickers hardness was 25.2 ± 0.6 GPa at a load of 0.49 N, Young's modulus was 551 ± 7 GPa, fracture toughness was 4.5 ± 0.4 MPa m1/2, and flexural strength was 507 ± 10 MPa. Flexural strength increased by more than 50% from 507 ± 10 MPa at RT to 776 ± …


Processing And Mechanical Properties Of Hot-Pressed Zirconium Diboride – Zirconium Carbide Ceramics, Eric W. Neuman, William Fahrenholtz, Gregory E. Hilmas Sep 2022

Processing And Mechanical Properties Of Hot-Pressed Zirconium Diboride – Zirconium Carbide Ceramics, Eric W. Neuman, William Fahrenholtz, Gregory E. Hilmas

Materials Science and Engineering Faculty Research & Creative Works

ZrB2 was mixed with 0.5 wt% carbon and up to 10 vol% ZrC and densified by hot-pressing at 2000 °C. All compositions were > 99.8% dense following hot-pressing. The dense ceramics contained 1–1.5 vol% less ZrC than the nominal ZrC addition and had between 0.5 and 1 vol% residual carbon. Grain sizes for the ZrB2 phase decreased from 10.1 µm for 2.5 vol% ZrC to 4.2 µm for 10 vol% ZrC, while the ZrC cluster size increased from 1.3 µm to 2.2 µm over the same composition range. Elastic modulus was ~505 GPa and toughness was ~2.6 MPa·m½ for all compositions. …


Anti-Washout Concrete: An Overview, Hao Lu, Xiao Sun, Hongyan Ma Aug 2022

Anti-Washout Concrete: An Overview, Hao Lu, Xiao Sun, Hongyan Ma

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

Anti-washout concrete (AWC) is a special cement-based material that can be directly employed in underwater environments without dispersion. It was developed around 50 years ago, and more than 150 journal articles and technical reports have been published. This paper provides a holistic review about the basic fresh-state and hardened-state properties of the AWC, such as water (washout) resistance, consistency, bleeding and segregation resistance, mechanical properties, and durability, as well as relevant testing methods. The discrepancies between AWC's characteristics and those of conventional concrete are clearly presented. The mixture compositions, supplementary cementitious materials (SCMs), and other conditions that affect AWC's performance …


Effect Of Boron In Cast Iron, Suyash Durendra Pawaskar Aug 2022

Effect Of Boron In Cast Iron, Suyash Durendra Pawaskar

Masters Theses

"Boron, mostly considered a residual element, has started to cause issues in the cast iron foundries by causing a decrease in the strength of pearlitic gray and ductile iron castings. Because of the increase in the use of boron-added steel scrap from automotive steel and a lack of agreement on the critical levels of boron in cast iron, foundries are facing difficulties in controlling the microstructure of gray iron castings when boron is present. The current investigation was designed to analyze the effects of boron in cast irons and predict a mechanism to understand its effects with a vision of …


Room-Temperature Mechanical Properties Of A High-Entropy Diboride, Alec C. Murchie, Jeremy Lee Watts, William Fahrenholtz, Gregory E. Hilmas Jul 2022

Room-Temperature Mechanical Properties Of A High-Entropy Diboride, Alec C. Murchie, Jeremy Lee Watts, William Fahrenholtz, Gregory E. Hilmas

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties of a (Hf,Mo,Nb,Ta,W,Zr)B2 high-entropy ceramic were measured at room temperature. A two-step synthesis process was utilized to produce the (Hf,Mo,Nb,Ta,W,Zr)B2 ceramics. The process consisted of a boro/carbothermal reduction reaction followed by solid solution formation and densification through spark plasma sintering. Nominally, phase pure (Hf,Mo,Nb,Ta,W,Zr)B2 was sintered to near full density (8.98 g/cm3) at 2000°C. The mean grain size was 6 ± 2 µm with a maximum grain size of 17 µm. Flexural strength was 528 ± 53 MPa, Young's modulus was 520 ± 12 GPa, fracture toughness was 3.9 ± 1.2 MPa·m1/2, and hardness (HV0.2) was 33.1 …


Use Of Saturated Lightweight Sand To Improve The Mechanical And Microstructural Properties Of Uhpc With Fiber Alignment, Huanghuang Huang, Le Teng, Xiaojian Gao, Kamal Khayat, Fazhou Wang, Zhichao Liu May 2022

Use Of Saturated Lightweight Sand To Improve The Mechanical And Microstructural Properties Of Uhpc With Fiber Alignment, Huanghuang Huang, Le Teng, Xiaojian Gao, Kamal Khayat, Fazhou Wang, Zhichao Liu

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

This paper studied the influence of pre-saturated lightweight sand (LWS) on the mechanical and microstructural properties of UHPC cast with steel fiber alignment. The changes in hydration kinetics, porosity, nano-mechanical, and mechanical properties were studied. The LWS was used at 0–50% replacement volumes of total sand. Predominant fiber alignment was favored through a flow-induced casting method during casting of flexural prisms. Experiment results showed that the 28-d autogenous shrinkage was decreased from 450 to 275 μm/m with the LWS content increasing from 0 to 50%. The addition of 20% LWS led to maximum increases of 15%, 15%, and 20% in …


Development And Characterization Of Magnesium Phosphate Cement Based Ultra-High Performance Concrete, Jihui Qin, Fumin Dai, Hongyan Ma, Xiaobing Dai, Zhen Li, Xingwen Jia, Jueshi Qian Apr 2022

Development And Characterization Of Magnesium Phosphate Cement Based Ultra-High Performance Concrete, Jihui Qin, Fumin Dai, Hongyan Ma, Xiaobing Dai, Zhen Li, Xingwen Jia, Jueshi Qian

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

This study aims at the development of magnesium phosphate cement-based ultra-high performance concrete (MPC-UHPC). To this end, MPC paste phase was designed by using high magnesia-to-phosphate (M/P, 3.5) and low water-to-cement (W/C, 0.10–0.16) mass ratios, and certain amounts of ultra-fine fly ash (UFA, 5%–15%). Fresh and hardened properties, and microstructure of the developed MPC-UHPC were evaluated, and compared with those of conventional UHPC as well. Test results showed that lower W/C resulted in higher mechanical strengths and lower drying shrinkage, but the sharp decrease of workability and increase of autogenous shrinkage. At a constant W/C, the addition of UFA effectively …


The Effect Of Nanostructures In Aluminum Alloys Processed Using Additive Manufacturing On Microstructural Evolution And Mechanical Performance Behavior, Rachel Boillat, Sriram Praneeth Isanaka, Frank W. Liou May 2021

The Effect Of Nanostructures In Aluminum Alloys Processed Using Additive Manufacturing On Microstructural Evolution And Mechanical Performance Behavior, Rachel Boillat, Sriram Praneeth Isanaka, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

This paper reviews the status of nanoparticle technology as it relates to the additive manufacturing (AM) of aluminum-based alloys. A broad overview of common AM processes is given. Additive manufacturing is a promising field for the advancement of manufacturing due to its ability to yield near-net-shaped components that require minimal post-processing prior to end-use. AM also allows for the fabrication of prototypes as well as economical small batch production. Aluminum alloys processed via AM would be very beneficial to the manufacturing industry due to their high strength to weight ratio; however, many of the conventional alloy compositions have been shown …


Effects Of Zirconia Doping On Additively Manufactured Alumina Ceramics By Laser Direct Deposition, John M. Pappas, Aditya R. Thakur, Xiangyang Dong Jul 2020

Effects Of Zirconia Doping On Additively Manufactured Alumina Ceramics By Laser Direct Deposition, John M. Pappas, Aditya R. Thakur, Xiangyang Dong

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The ability to additively manufacture functional alumina ceramics has the potential to lower manufacturing costs and development time for complex components. In this study, the doping effects of zirconia on laser direct deposited alumina ceramics were investigated. The microstructure of the printed samples was analyzed in terms of grain size and composition distribution. The addition of zirconia was found to accumulate along alumina grain boundaries and resulted in significant grain refinement. The zirconia doping largely reduced crack formation during processing compared to that of pure alumina samples. In the case of 10 wt% zirconia, cracking during deposition was nearly completely …


Development Of Stage-I Tempered High Strength Cast Steel For Ground Engaging Tools, Viraj Ashok Athavale Jan 2019

Development Of Stage-I Tempered High Strength Cast Steel For Ground Engaging Tools, Viraj Ashok Athavale

Doctoral Dissertations

"Ground Engaging Tools (GET) are the expendable replacement parts used in heavy machinery used with mining or construction equipment. GET’s protect the expensive machine components from the wear and tear found common in high-impact or high-abrasion environments. The goal of this project is to develop advanced next-generation alloy choices that outperforms the existing GET materials. A method of predicting tempered hardness of mixed microstructures was formulated. Using this model, two alloy series viz. Cr-Ni-Mo and Mn-Si-Mo-V were proposed and experimented with the goal of obtaining a high strength and impact resistant cast steel. Cast iterations of Cr-Ni-Mo alloy series were …


Mechanical Properties Of Zr-Based Bulk Metallic Glass Parts Fabricated By Laser-Foil-Printing Additive Manufacturing, Yingqi Li, Ming-Chuan Leu, Hai-Lung Tsai Aug 2018

Mechanical Properties Of Zr-Based Bulk Metallic Glass Parts Fabricated By Laser-Foil-Printing Additive Manufacturing, Yingqi Li, Ming-Chuan Leu, Hai-Lung Tsai

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The application of bulk metallic glasses (BMGs) has been traditionally limited to parts with small dimensions and simple geometries, due to the requirement of fast cooling during the conventional process of casting. This research exemplifies a promising additive manufacturing method, i.e., laser-foil-printing (LFP), to fabricate high-quality BMG parts with large dimensions and complex geometries. In this study, Zr52.5Ti5Al10Ni14.6Cu17.9 BMG parts were fabricated by LFP technology in which MG foils are laser welded layer-by- layer upon a substrate. The mechanical properties of the fabricated BMG parts were measured using micro-indentation, tensile test …


Time Effect Of Water Injection On The Mechanical Properties Of Coal And Its Application In Rockburst Prevention In Mining, Xiaofei Liu, Guang Xu, Chong Zhang, Biao Kong, Jifa Qian, Dong Zhu, Mingyao Wei Nov 2017

Time Effect Of Water Injection On The Mechanical Properties Of Coal And Its Application In Rockburst Prevention In Mining, Xiaofei Liu, Guang Xu, Chong Zhang, Biao Kong, Jifa Qian, Dong Zhu, Mingyao Wei

Mining Engineering Faculty Research & Creative Works

Coal seam water injection is widely used to prevent rockbursts in coal mines, and the duration of water injection is an important parameter related to the effectiveness of rockburst prevention, making it of practical importance to optimize the effective water injection duration. This paper presents the test results of the mechanical properties and pore structure of samples with different soaking time, obtained from a working face where rockburst occurred. Soaking time changes the mechanical properties of samples, and this time effect differs with the coal size (from centimeter to nanometer size). Results of numerical simulation and on-site tests in the …


Factorial Design Approach In Proportioning Prestressed Self-Compacting Concrete, Wu-Jian Long, Kamal Khayat, Guillaume Lemieux, Feng Xing, Wei-Lun Wang Mar 2015

Factorial Design Approach In Proportioning Prestressed Self-Compacting Concrete, Wu-Jian Long, Kamal Khayat, Guillaume Lemieux, Feng Xing, Wei-Lun Wang

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

In order to model the effect of mixture parameters and material properties on the hardened properties of, prestressed self-compacting concrete (SCC), and also to investigate the extensions of the statistical models, a factorial design was employed to identify the relative significance of these primary parameters and their interactions in terms of the mechanical and visco-elastic properties of SCC. In addition to the 16 fractional factorial mixtures evaluated in the modeled region of -1 to +1, eight axial mixtures were prepared at extreme values of -2 and +2 with the other variables maintained at the central points. Four replicate central mixtures …


An Investigation Of The Effect Of Direct Metal Deposition Parameters On The Characteristics Of The Deposited Layers, Tarak A. Amine, Joseph William Newkirk, Frank W. Liou Jul 2014

An Investigation Of The Effect Of Direct Metal Deposition Parameters On The Characteristics Of The Deposited Layers, Tarak A. Amine, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

Multilayer direct laser deposition (DLD) is a fabrication process through which parts are fabricated by creating a molten pool into which metal powder is injected as particles. During fabrication, complex thermal activity occurs in different regions of the build; for example, newly deposited layers will reheat previously deposited layers. The objective of this study was to provide insight into the thermal activity that occurs during the DLD process. This work focused on the effect of the laser parameters of newly deposited layers on the microstructure and mechanical properties of the previously deposited layers in order to characterize these effects to …


Thermophysical And Mechanical Properties Of Hardened Cement Paste With Microencapsulated Phase Change Materials For Energy Storage, Hongzhi Cui, Wenyu Liao, Shazim Ali Memon, Biqin Dong, Waiching Tang Jan 2014

Thermophysical And Mechanical Properties Of Hardened Cement Paste With Microencapsulated Phase Change Materials For Energy Storage, Hongzhi Cui, Wenyu Liao, Shazim Ali Memon, Biqin Dong, Waiching Tang

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

In this research, structural-functional integrated cement-based materials were prepared by employing cement paste and a microencapsulated phase change material (MPCM) manufactured using urea-formaldehyde resin as the shell and paraffin as the core material. The encapsulation ratio of the MPCM could reach up to 91.21 wt%. Thermal energy storage cement pastes (TESCPs) incorporated with different MPCM contents (5%, 10%, 15%, 20% and 25% by weight of cement) were developed, and their thermal and mechanical properties were studied. The results showed that the total energy storage capacity of the hardened cement specimens with MPCM increased by up to 3.9-times compared with that …


Effect Of Architecture And Porosity On Mechanical Properties Of Borate Glass Scaffolds Made By Selective Laser Sintering, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Taylor Comte Aug 2013

Effect Of Architecture And Porosity On Mechanical Properties Of Borate Glass Scaffolds Made By Selective Laser Sintering, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Taylor Comte

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The porosity and architecture of bone scaffolds, intended for use in bone repair or replacement, are two of the most important parameters in the field of bone tissue engineering. The two parameters not only affect the mechanical properties of the scaffolds but also aid in determining the amount of bone regeneration after implantation. Scaffolds with five different architectures and four porosity levels were fabricated using borate bioactive glass (13-93B3) using the selective laser sintering (SLS) process. The pore size of the scaffolds varied from 400 to 1300 μm. The compressive strength of the scaffolds varied from 1.7 to 15.5 MPa …


Freeze-Form Extrusion Fabrication Of Functionally Graded Material Composites Using Zirconium Carbide And Tungsten, Ang Li, Aaron S. Thornton, Bradley K. Deuser, Jeremy Lee Watts, Ming-Chuan Leu, Greg Hilmas, Robert G. Landers Aug 2012

Freeze-Form Extrusion Fabrication Of Functionally Graded Material Composites Using Zirconium Carbide And Tungsten, Ang Li, Aaron S. Thornton, Bradley K. Deuser, Jeremy Lee Watts, Ming-Chuan Leu, Greg Hilmas, Robert G. Landers

Materials Science and Engineering Faculty Research & Creative Works

Ultra-high-temperature ceramics are being investigated for future use in aerospace applications due to their superior thermo-mechanical properties, as well as their oxidation resistance, at temperatures above 2000⁰C. However, their brittleness makes them susceptible to thermal shock failure. As graded composites, components fabricated as functionally-graded materials (FGMs) can combine the superior properties of ceramics with the toughness of an underlying refractory metal. This paper discusses the grading of two materials through the use of a Freeze-form Extrusion Fabrication (FEF) system to build FGM parts consisting of zirconium carbide (ZrC) and tungsten (W). Aqueous-based colloidal suspensions of ZrC and W were developed …


Effect Of Particle Size, Binder Content And Heat Treatment On Mechanical Properties Of 13-93 Bioactive Glass Scaffolds, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez Aug 2011

Effect Of Particle Size, Binder Content And Heat Treatment On Mechanical Properties Of 13-93 Bioactive Glass Scaffolds, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Particle size, binder content and the post-processing schedule are important parameters that affect the microstructure, and, hence, the mechanical properties of parts produced using the indirect selective laser sintering process. 13-93 bioactive glass, with mean particle sizes ranging from 10 μm to 44 μm, is mixed with different amounts of stearic acid binder to fabricate green scaffolds. Through the design of the post-processing schedule, the time required for postprocessing the green scaffolds is reduced from the initial 80 hrs to 12 hrs. The compressive strength varies from 41 MPa for a part with~60% porosity to 157 MPa for a part …


Freeze Extrusion Fabrication Of 13-93 Bioactive Glass Scaffolds For Bone Repair, Tieshu Huang, Nikhil D. Doiphode, M. N. Rahaman, Ming-Chuan Leu, B. Sonny Bal, D. E. Day Aug 2010

Freeze Extrusion Fabrication Of 13-93 Bioactive Glass Scaffolds For Bone Repair, Tieshu Huang, Nikhil D. Doiphode, M. N. Rahaman, Ming-Chuan Leu, B. Sonny Bal, D. E. Day

Materials Science and Engineering Faculty Research & Creative Works

There is an increasing demand for synthetic scaffolds with the requisite biocompatibility, internal architecture, and mechanical properties for the bone repair and regeneration. In this work, scaffolds of a silicate bioactive glass (13-93) were prepared by a freeze extrusion fabrication (FEF) method and evaluated in vitro for potential applications in bone repair and regeneration. The process parameters for FEF production of scaffolds with the requisite microstructural characteristics, as well as the mechanical and cell culture response of the scaffolds were evaluated. After binder burnout and sintering (60 min at 700°C), the scaffolds consisted of a dense glass network with interpenetrating …


Freeform Fabrication Of Zirconium Diboride Parts Using Selective Laser Sintering, Ming-Chuan Leu, Erik B. Adamek, Tieshu Huang, Greg Hilmas, Fatih Dogan Aug 2008

Freeform Fabrication Of Zirconium Diboride Parts Using Selective Laser Sintering, Ming-Chuan Leu, Erik B. Adamek, Tieshu Huang, Greg Hilmas, Fatih Dogan

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Using the Selective Laser Sintering (SLS) process, both flexural test bars and 3D fuel injector components have been fabricated with zirconium diboride (ZrB2) powder. Stearic acid was selected as the binder. Values of SLS process parameters were chosen such that the green parts could be built with sharp geometrical features and that the sintered parts could have good mechanical properties. After binder burnout and sintering, the SLS fabricated ZrB2 test bars achieved 80% theoretical density, and the average flexural strength of the sintered samples was 195 MPa. These values demonstrate the feasibility of the SLS process for …