Engineering Commons^™

Effect Of Process Parameter On Temperature Distribution, Microstructure, And Mechanical Properties Of Self-Reacting Friction Stir Welded Aluminum Alloy 6061-T651, Monica Adriana Torres

Open Access Theses & Dissertations

Self-reacting friction stir welding is the latest FSW tool configuration developed, it employs two shoulders--one on top and one on the bottom of the workpiece-- this tool configuration offers many advantages over conventional welding techniques. However, the current lack of information and specifications limits its understanding and application. This investigation analyzed the effect of process parameters on temperature distribution, microstructure evolution, and final mechanical properties of 6061-T651 SR-FS welds. A factorial experiment was carried out, in which three-process parameters were analyzed--rotational speed, travel speed, and tool plunge force-- three levels were analyzed for each parameter, except for a tool plunge …

Fabrication And Characterization Of Nanocrystalline Yttrium Oxide Thin Films For Electronic Device Applications, Mudavakkat Vikas Haridas

Open Access Theses & Dissertations

This thesis presents the optimization of growth conditions for fabricating nanocrystalline Yttrium Oxide (Y2O3) thin films on silicon and optical grade, high quality quartz substrates in order to study its structural, optical and electrical properties for electronic device applications.

Commercially Y2O3 has proven to be difficult to fabricate at high quality due to its high temperature growth requirements and the need to alter established fabrication methods for electronic devices. A high temperature requirement for high quality poses a problem for research and analysis. This calls upon for an optimization of the growth conditions to facilitate fabrication of thin films for …

Fundamental Studies Of Co-Base Superalloy Biomedical Prototypes Fabricated By Electron Beam Melting: Microstructures And Microstructural Architecture, Sara M. Gaytan

Open Access Theses & Dissertations

Rapid prototyping, especially electron beam melting (EBM) technology by ARCAM have proven to provide outstanding microstructural and mechanical properties on different alloys fabricated by this technology. Being a computer designed driven technology, complex components, that are hard or even impossible to fabricate by traditional manufacturing techniques, can be fabricated by layer-by-layer EBM technology.

Microstructural and mechanical properties are compared for an EBM femoral knee component prototype with a traditionally-fabricated and body-removed femoral knee implant. Block and cylindrical shape components fabricated by EBM were also analyzed for this project. The alloy utilized for these components is Co-26Cr-6Mo-0.2C characterized by the standards …

Ballistic Projectile Metallurgical Issues And Fundamentals: Aerosol Production In Rod Penetration Erosion And Erosion Phenomena Associated With Railgun Development, Brenda Ivette Machado

Open Access Theses & Dissertations

The issue is derived from ballistic erosion as it relates to nanoparticle production and respiration of these particles as a health concern ballistic erosion and ballistic erosion as it relates to railgun performance. A common thread between these two issues is dynamic recrystallization (DRX). DRX has been demonstrated to be the dominant mechanism for solid-state flow associated with ballistic projectile/target penetration and interaction, friction-stir welding phenomena, and other high-strain rate deformation phenomena.

Aerosol particulates collected on filters from ballistic penetration and erosion events for W-Ni-Co and W-Ni-Fe kinetic energy rod projectiles penetrating steel target plates were observed to be highly …

Development And Characterization Of The Oxidation Behavior Of Various High Temperature Niobium Based Alloys, Benedict Isabel Portillo

Open Access Theses & Dissertations

The oxidation response of various niobium based refractory alloys from the Nb-Mo-Si-B-X alloy system has been examined at temperatures between 700 and 1400°C in air. The development of these alloys was part of an ongoing effort to develop and discover a new materials system capable of replacing nickel based super alloys. Additions of titanium were found to provide limited oxidation resistance. A discontinuous layer of TiO2 was observed to from at temperatures above 1100°C. Alloys containing titanium additions were observed to suffer from pest oxidation at low and intermediate temperatures due to the development of Nb2O5. Poor oxidation resistance at …

The Effect Of Cr, Si And B On The Oxidation Behavior On Three Nb-Based Alloys, David Alvarez

Open Access Theses & Dissertations

Nb-based alloys are of particular interest to replace the current Ni-based superalloys for high-temperature structural applications. One important limitation to improve the efficiency of gas-turbine engines is the temperature limit of current materials being used. By allowing the temperature to increase, the efficiency will increase. Nb-based alloys have high melting points and adequate mechanical properties but the oxidation resistance is still inadequate.

This research focuses on the oxidation behavior of three Nb-based alloys to study the effect of Cr and Si variation and look at the effect of Boron. Boron can form a glassy borosilicate which is viscous at high …

Preparation And Characterization Of Iron Oxide And Hydroxide Based Nanomaterials, Guillermo Carbajal Franco

Open Access Theses & Dissertations

Iron (Fe) oxides and hydroxides are common and abundant materials. They exhibit diverse crystal structures, properties and phenomena by virtue of which they find a wide range of scientific and technological applications. Controlled growth and manipulation of the specific structure and electronic behavior to meet the requirements of a given application is a challenging problem in view of many possible phases and composition of the resulting materials. The preparation method and experimental conditions will, therefore, significantly affect the properties and performance of Fe oxides and hydroxides. The goal of the project is to obtain Fe-based oxide/hydroxide catalytic materials and to …

Microstructural Architecture Developed In The Fabrication Of Solid And Open-Cellular Copper Components By Additive Manufacturing Using Electron Beam Melting, Diana Alejandra Ramirez

Open Access Theses & Dissertations

The fabrication of Cu components were first built by additive manufacturing using electron beam melting (EBM) from low-purity, atomized Cu powder containing a high density of Cu2O precipitates leading to a novel example of precipitate-dislocation architecture. These microstructures exhibit cell-like arrays (1-3µm) in the horizontal reference plane perpendicular to the build direction with columnar-like arrays extending from ~12 to >60 µm in length and corresponding spatial dimensions of 1-3 µm. These observations were observed by the use of optical metallography, and scanning and transmission electron microscopy. The hardness measurements were taken both on the atomized powder and the Cu components. …