Engineering Commons^™

Hierarchical Microstructures To Overcome The Conflict Between Strength And Toughness Of Hard Coatings: Tin/Ni As A Model System, Ignacio Lopez Cabanas

Material Science and Engineering Dissertations

In the recent times, industry's production speed has been increasing and thus, the production of parts needs to adapt and so do the materials used to manufacture them. Hence, tools exposed to more extreme conditions using hard coatings need them to be more reliable. In this work an improvement of the toughness of TiN/Ni coatings is achieved through the combination of different microstructures at different levels. This first part consisted on finding the optimum TiN/Ni composition by using a high throughput methodology for a faster analysis and the second on the combination of that composition with a multilayer structure to …

Analysis Of Novel Corrosion Resistant Maraging Steels For Use In Additive Manufacturing, Bradley Michael Samuel, James Knowlton Smith

Materials Engineering

Stainless maraging steel has been proven to be an industry standard material for plastic injection molds. Its high hardness and corrosion resistance extend the lifetime of the tool. This alloy system is also well-suited to additive manufacturing, which can be utilized to form internal cooling channels, further increasing tool life. Using Rapid Alloy Development (RAD) Oerilkon METCO is developing a new composition of stainless maraging tool steel that has high hardness/strength, is corrosion resistant, and has additive-capable melting and solidification properties. This study tests the hardness and corrosion resistance of the new RAD alloys against the current market competitor Corrax …

Experimental Investigation Of Laser Scan Strategy On The Microstructure, Mechanical Properties And Residual Stress Of Inconel 718 Parts Fabricated By Selective Laser Melting, Kiriti Mamidi

Mechanical and Aerospace Engineering Theses

Inconel 718 (IN718) is a nickel-based superalloy which exhibits excellent tensile and impact resistant properties along with good corrosion resistance at high temperatures. However, due to the high toughness and work hardening, the machinability of this superalloy is low. Therefore, the selective laser melting (SLM) process has been adopted as an efficient technique to fabricate IN718 parts as it overcomes the problems associated with conventional manufacturing of superalloys. SLM is a widely used additive manufacturing technique which offers the possibility to induce multi-functionality into a single component, and thus reduce the number of components that are needed. In the SLM …

Predicting Hardness Of Friction Stir Processed 304l Stainless Steel Using A Finite Element Model And A Random Forest Algorithm, Tyler Alan Mathis

Theses and Dissertations

Friction stir welding is an advanced welding process that is being investigated for use in many different industries. One area that has been investigated for its application is in healing critical nuclear reactor components that are developing cracks. However, friction stir welding is a complicated process and it is difficult to predict what the final properties of a set of welding parameters will be. This thesis sets forth a method using finite element analysis and a random forest model to accurately predict hardness in the welding nugget after processing. The finite element analysis code used and ALE formulation that enabled …

Custom Foot Prosthetic: Diabetic Care, Chandler Streuli

All Undergraduate Projects

Across the United States there are people every day who lose their toes to diabetes or to loss of circulation within their legs. The problem becomes building a more cost effective and efficient prosthetic for these individuals. The prosthetics that are used for medical purposes are often costly, especially without the help of insurance. The new prosthetic was designed to be taken in and out of shoes so that it is fast and easy for the user to move the device from shoe to shoe. The manufacturing method for this project was using a 3D printer to build the initial …

Analysis Of Ni And Fe-Based Alloys For Turbine Seal Ring Applications, Dawei She

USF Tampa Graduate Theses and Dissertations

Metal sealing rings have been used widely in compressors, turbines and hydraulic devices. Such rings can extend out due to elasticity, and keep close contact with the valve wall, resulting in the formation of a functional seal under pressure. In this project, the failure of metal sealing rings is considered. Sealing component failure due to stress relaxation can threaten the safety of the whole steam turbine. The object of this study was to examine the stress relaxation response and corresponding changes in microstructure of metal sealing rings used in nuclear steam turbine under high temperature and applied stress. The two …

Raman Spectroscopy Of The Skeleton Of The Coral Acropora Cervicornis, Zachary C. Shepard

Honors Undergraduate Theses

Coral reefs are an important element of marine ecosystem that are critical to maintain a healthy environment. Unfortunately, in recent years coral reefs are doing poorly and many in parts of the ocean are simply dying. Therefore, study of coral’s structural response to external loads could answer what will happen with their structures, while they exhibit different types of loading. Therefore, the proposition of using in-situ micro-Raman spectroscopy to study skeletons of Acropora cervicornis was used. Coral skeleton samples I subjected to mechanical loading studied their vibrational properties by exciting the material with 532nm visible light. A uniaxial compressive load …

Investigation Of Microstructure Effects On Hardness And Oxidation Resistance Of New Generation Ceramic Coatings, Minghui Zhang

Material Science and Engineering Dissertations

This work was motivated by the demand for a new generation of materials capable for harsh environment applications, and focused on developing a better understanding of the effects of elemental composition and microstructure on the mechanical and thermal properties of coatings. The knowledge gained from this work can be used to design protective coatings with tailored properties for harsh environment applications in the future. High resolution transmission electron microscopy (HRTEM) and electron diffraction have been mainly employed in the microstructure studies of the new generation ceramics, with the assistance of other materials characterization techniques, such as x-ray diffraction (XRD), x-ray …

Failure Analysis Of High Nickel Alloy Steel Seal Ring Used In Turbomachinery, Wenbo Wang

USF Tampa Graduate Theses and Dissertations

The system of upper high nickel alloying steel seal ring and lower high nickel alloying steel seal ring, installed in the grooves of turbine, can extend out and fit with the wall of valve cage, resulting in forming a good seal under the pressure. In the project, the failure steel seal ring is considered. This situation had threatened the safety of the whole steam turbine system. The purpose of this study is to identify the failure cause of the steel seal ring used in nuclear steam turbines. New high nickel steel alloy seal ring was compared with the failed seal …

Effect Of Sintering Temperature On Microstructure, Corrosion Behavior, And Hardness Of Nanocrystalline Al-5at.%Ni And Al-5at.%V Alloys, Matthew G. Wachowiak

Williams Honors College, Honors Research Projects

The purpose of this project was to investigate thermal stability of high energy ball milled Al-5at.%Ni and Al-5at.%V alloys. Characterization was done by analyzing grain size and solid solubility. Samples were created using high energy ball milling, cold compaction to 3 GPa, and sintering from 100 °C to 500 °C at 100 °C increments, as well 450 °C and 614 °C. Microstructure, mechanical properties, and corrosion properties were determined using scanning electron microscopy, energy dispersive x-ray spectroscopy, x-ray diffraction, hardness testing, and cyclic potentiodynamic polarization. Vickers hardness of Al-5at.%Ni decreased with increasing temperature. For Al-at.%V, hardness increased with sintering temperature …

Cryogenic Processing Of Al 7050-T7451 Alloy For Improved Surface Integrity, Bo Huang

Theses and Dissertations--Mechanical Engineering

Al 7050-T7451 alloy with good combinations of strength, stress corrosion cracking resistance and toughness, is used broadly in the aerospace/aviation industry for fatigue-critical airframe structural components. However, it is also considered as a highly anisotropic alloy as the crack growth behavior along the short transverse direction is very different from the one in the long transverse direction, due to the inhomogeneous microstructure with the elongated grains distributed in the work material used in the sheet/plate applications. Further processes on these materials are needed to improve its mechanical and material properties and broaden its applications.

The material with ultra-fine or nano …

An Investigation Of Friction Stir Welding Parameter Effects On Post Weld Mechanical Properties In 7075 Aa, Steven B. Dickson

Theses and Dissertations

The effects of weld temperature, travel speed, and backing plate thermal diffusivity on themechanical properties of a weld have been studied. A face centered cubic experiment of designwas completed in which the response variables were yield strength, minimum hardness in the HAZ, and charpy impact toughness. Three models were created from the data gathered usinga stepwise regression in order to see the effects of each parameter. For the yield strength andminimum hardness it was found that only travel speed and backing plate thermal diffusivities werestatistically significant to the properties. The charpy impact toughness saw that all three parameterswere statistically significant …

Plastic Anisotropy Of Complex Crystals And Hierarchically Structured Alloys Using Micro-Mechanical Computational Analysis, Lin Li

Doctoral Dissertations

The material anisotropy is one of the most important material properties that cannot be disregarded in today’s world of materials designing and manufacturing. As new materials being developed and new material demands are introduced the inevitable focus on anisotropic materials has been brought under the spotlight. In this dissertation, several experimental and simulation project regarding material anisotropic effects on hexagonal close packed crystals such as Silicon Carbide as well and hierarchically structured solid solution ferritic based alloys. The general purpose was to demonstrate the improvement on various intended material properties using finite element method. Since indentation is a widely used …

Gadolinia Doped Hafnia (Gd2o3- Hfo2) Thermal Barrier Coatings For Gas Turbine Applications, Satya Kiran Gullapalli

Open Access Theses & Dissertations

Thermal efficiency of the gas turbines is influenced by the operating temperature of the hot gas path components. The material used for the hot gas path components can only withstand temperature up to a certain limit. Thermal barrier coatings (TBC) provide the additional thermal protection for these components and help the gas turbine achieve higher firing temperatures. Traditionally available yttria stabilized zirconia (YSZ) TBCs have a limitation up to 1200 C due to their phase transformation. The present work focuses on gadolinia based hafnia (GSH) TBCs to study their potential to replace the YSZ coatings. Different compositions of gadolinia doped …

Study On The Fracture Toughness Of Friction Stir Welded Api X80, Allan M. Tribe

Theses and Dissertations

High strength low alloy (HSLA) steels have been developed to simultaneously have high yield strength and high fracture toughness. However, in practical applications steel must be welded. Traditional arc welding has proven detrimental to the fracture toughness of HSLA steels. Friction stir welding has recently shown mixed results in welding HSLA steels. The range of welding parameters used in these recent studies however has been very limited. With only a few welding parameters tested, the effect of spindle speed, travel speed, and heat input on the fracture toughness of friction stir welded HSLA steel remains unknown. To understand how the …

Influences Of Sample Preparation On The Indentation Size Effect And Nanoindentation Pop-In On Nickel, Zhigang Wang

Doctoral Dissertations

Careful experiments were performed with a well characterized indenter to systematically investigate the influences of sample preparation on the indentation size effect (ISE) and nanoindentation pop-in behavior in nickel. The Ni (100) surface was prepared by electropolishing and then damaged in a controlled way by polishing with alumina slurry. The damaged layer was systematically removed in steps by colloidal silica polishing (0.02 µm (micrometer)) with the pop-in behavior statistically characterized and the depth dependence of the hardness measured at each step. AFM observation revealed that the electropolished surface is free from scratches, and has the largest roughness. Numerous scratches were …

Measuring The Nanoindentation Properties Of Alendronate-Time Treated Canine Cortical, Folorunso Ashaolu

Master's Theses

This study examines the nanoindentation (energy inclusive) properties of 0.2 mg/kg alendronate treated ribs at one and three years against a vehicle treated control in a fresh-frozen, non-cold-mounted, condition. This was to verify if the tissue-level properties for 0.2 ALN treated beagles would increase because of an increased level of mineralization despite a microdamage increase.

A total of twelve (12) skeletally mature (1–2 years old) female beagle dogs were treated daily for three years and one year with oral doses of vehicle (VEH, 1 mL/kg saline) or alendronate (ALN, 0.2 Merck, Rahway, NJ). The 0.2 mg dose corresponds, on a …

Nanoindentation Of Annealed And As-Sputtered Thin Films Of Nickel Titanium Shape Memory Alloys, Matthew Tyson Lewis

Master's Theses

The bottom-up processing techniques used for making Microelectromechanical systems (MEMS) devices can produce material properties different from bulk processing. The material properties must be evaluated with the process parameters used and for changes in the process parameters. The mechanical properties are needed to design MEMS devices. A material of interest for MEMS devices is nickel titanium (NiTi) shape memory alloy (SMA) because of the high work output (~107 J/m3). This thesis will focus on the fabrication of thin film NiTi by DC magnetron sputtering deposition and testing mechanical properties of the fabricated films by nanoindentation. Thin film NiTi SMA was …

Methods For Characterizing Mechanical Properties Of Wood Cell Walls Via Nanoindentation, Yujie Meng

Masters Theses

Nanoindentation is a method of contacting a material whose mechanical properties are unknown with another material whose properties are known. Nanoindentation has the advantage of being able to probe a material’s microstructure while being sensitive enough to detect variations in mechanical properties. However, nanoindentation has some limitations as a testing technique due to the specific formation and structure of some biomaterials. The main objective of this research is to identify any factors that influence the nanoindentation measurement of wood cell walls (a typical biomaterial).

The function of the embedding media in describing the properties of wood cells is poorly understood. …

Tribological Comparison Of Traditional And Advanced Firearm Coatings, Greg Boban

Master's Theses

The objective of this project is to find which type of coating has the best performance characteristics for finishing firearms. This is accomplished by measuring and comparing several performance characteristics, such as: adhesion, hardness, wear resistance, friction control, and corrosion resistance. Appearance is not a factor since any exterior coating that is flashy can be subdued or camouflaged with special purpose paints, which have proven durable enough for such purposes. Cost will not be a limiting factor for this experiment, but will be discussed in the conclusion as a secondary concern. This data will be used to identify the best …

Nanomechanics Of Muscovite Subjected To Nanoindentation And The Pertinent Indentation Size Effect, Hang Yin

LSU Master's Theses

Two groups of nanoindentation experiments, including repeated loading tests and monotonic loading tests, were performed on muscovite with a sharp indenter tip and loading direction normal to the basal plane. By varying the maximum load in the first group of repeated experiments, influences of the load level can be examined on the modes of nanoscale deformation and the resulting estimation of hardness and elastic modulus. The incipient kink band concept was employed to interpret the observed dispersed loading-unloading hysteresis loops by considering formation and annihilation of IKBs. Furthermore, the material’s contact stiffness behavior was characterized by comparing the normalized unloading …

Mechanical And Chemical Characterization Of Biological Composite Structures, Bonnie Zimmerman

All Theses

A better understanding of the bioresponse of naturally occurring systems will help
to optimize the engineering of synthetic biomaterials. The aim of this thesis was to
characterize the mechanical and chemical behavior of two distinct biological composite
systems, human teeth and wool fibers. These mechanical and chemical properties were
also studied as a function of natural structure and environmental conditions.
Human teeth are composite systems consisting primarily of hydroxylapatite and
protein. This project investigated how the use of clinical dental treatments and
procedures, such as whitening and etching, affects mechanical properties. Analysis of
nanoindentation with the Oliver-Pharr model provided elastic …

Friction Stir Welding Of High-Strength Automotive Steel, Eric Michael Olsen

Theses and Dissertations

The following thesis is a study on the ability to create acceptable welds in thin-plate, ultra-high-strength steels (UHSS) by way of friction stir welding (FSW). Steels are welded together to create tailor-welded blanks (TWB) for use in the automotive industry. Dual Phase (DP) 590, 780, and 980 steel as well as Transformation-Induced Plasticity (TRIP) 590 steel with thicknesses ranging from 1.2 mm to 1.8 mm were welded using friction stir welding under a variety of processing conditions, including experiments with dissimilar thicknesses. Samples were tested under tensile loads for initial determination if an acceptable weld had been created. Acceptable welds …

Processing, Microstructure And Mechanical Behavior Of Nanocomposite Multilayers, Zuqiang Qi

LSU Doctoral Dissertations

Nanoscale multilayer coatings have high potential for numerous engineering applications because they can exhibit enhanced properties due to nanoscale effects and combine different properties from individual components. At present, scale effects on the mechanical behavior of multilayers are not well understood. Three multilayer nanocomposite systems, namely Al/Al2O3, Ti/TiN, and Cr/a-C, have been synthesized by using a dual-gun e-beam physical vapor deposition, to investigate the effect of layer thickness, the nature of components and their microstructures on the mechanical behavior. The deposited Al and Ti nanolayers were found to have polycrystalline fcc and hcp structure, respectively, the Cr and TiN layers …

The Heat Treatment Of An Eight Percent Manganese-Titanium Alloy, Robert Alden Loucks

Bachelors Theses and Reports, 1928 - 1970

The subject of this particular investigation, manganese titanium alloy, has a sufficient amount of manganese present to retain beta upon quenching from the alpha plus beta or beta ranges. Thus, improvement of properties of this alloy is possible by selective heat treatments.