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Composite materials

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In Situ High Temperature Fiber-Optic Raman Sensor For Industrial Applications, Bohong Zhang Jan 2024

In Situ High Temperature Fiber-Optic Raman Sensor For Industrial Applications, Bohong Zhang

Doctoral Dissertations

"Continuous casting in steel production uses specially developed oxyfluoride glasses (mold fluxes) to lubricate a mold and control the solidification of the steel in the mold. The composition of the flux impacts properties, including basicity, viscosity, and crystallization rate, all of which affect the stability of the casting process and the quality of the solidified steel. However, mold fluxes interact with steel during the casting process, resulting in flux chemistry changes that must be considered in the flux design. Currently, the chemical composition of mold flux must be determined by extracting flux samples from the mold during casting and then …


Nonlinear Finite Element Model For Functionally Graded Porous Circular/Annular Micro-Plates Under Thermal And Mechanical Load, Enrique Nava Munoz Dec 2023

Nonlinear Finite Element Model For Functionally Graded Porous Circular/Annular Micro-Plates Under Thermal And Mechanical Load, Enrique Nava Munoz

Masters Theses

A nonlinear finite element model for micro circular/annular plates under thermal and mechanical loading is developed using a third order shear deformation theory. In the kinematic assumptions, the change of plate thickness is allowed and no transverse shear strains are considered on the top and bottom surfaces. A power-law distribution is utilized to account for variations of two constituents through the thickness of the plate. Three different types of porosity distributions are considered. The strain gradient effect in micro scale structures is considered using the modified couple stress theory. The dynamic version of the principle of virtual displacements is used …


Biomass Characterization And Insulation Optimization Studies, Hussein Awad Kurdi Saad Nov 2022

Biomass Characterization And Insulation Optimization Studies, Hussein Awad Kurdi Saad

Doctoral Dissertations and Master's Theses

This study indicates how biomass materials can be effectively used as naturally sustainable alternatives to insulation materials. Barley grains and oak leaves, straw, and jute are collected, and crushed into powders/ chopped pieces. The physical characteristics are measured to characterize each powder. The biomass powder reinforced composites are manufactured in varying weight ratios. The density and thermal conductivity of composite materials are measured. The properties of composites compared to those of commercial insulation materials are found to be close to them. Furthermore, genetic algorithms (GA) can be used to achieve multi-objective optimization entailing maximizing insulation (minimizing heat transfer) and simultaneously …


Analysis Guidelines And Functionalities Of The Catia Native Fea Solver For Composite Materials, Mohamed Edrisy Feb 2022

Analysis Guidelines And Functionalities Of The Catia Native Fea Solver For Composite Materials, Mohamed Edrisy

Electronic Theses and Dissertations

The emergence of commercial FEA solvers was a significant breakthrough that boosted the accuracy and complexity of engineering design. While composite materials are special materials, their mechanical properties can be custom made by considering the needs and requirements of the design problem. Given the rapidly expanding global consumption of composite materials, access to FEA solvers capable of assigning these materials is an absolute requirement.The CATIA software is a platform for designing, analyzing, and manufacturing of parts. However, there is no meaningful documentation in the public domain exploring the finite element functionalities of CATIA software for composite materials. Isotropic materials are …


Microscale Transverse Compression Modeling: A Comparative Study Of The Analytical Mac/Gmc Methods To Experimental Results, Emily Zeitunian Jan 2022

Microscale Transverse Compression Modeling: A Comparative Study Of The Analytical Mac/Gmc Methods To Experimental Results, Emily Zeitunian

Dissertations, Master's Theses and Master's Reports

Composite materials require a multi-scale approach to fully understand its behavior. At the micro level, material behavior analysis is conducted most often using numerical or analytical approaches. These models, however, require validation from experimental data to ensure material predictions are accurate. This study compares a semi-analytical micromechanical analysis tool, MAC/GMC, to experimental results of in-situ microscale transverse compression testing conducted at AFRL facilities. Effective properties, stress-strain curves, stress and strain fields, and damage predictions are compared with experimental outputs. Both generalized method of cells (GMC) and high-fidelity generalized method of cells (HFGMC) theories implemented within MAC/GMC show results that agree …


Data-Driven Damage Initiation Criteria For Carbon Fiber Reinforced Polymer Composites, Alexander Richard Post Nov 2021

Data-Driven Damage Initiation Criteria For Carbon Fiber Reinforced Polymer Composites, Alexander Richard Post

College of Computing and Digital Media Dissertations

Computational progressive failure analysis (PFA) is vital for the design, verification, and validation of carbon fiber reinforced polymer (CFRP) composites. However, the computational cost of PFA is usually high due to the complexity of the model. The damage initiation criterion is one of the essential components of a PFA code to determine the transition of a material’s state from pristine or microscopically damaged to macroscopically damaged. In this thesis, data-driven models are developed to determine the matrix damage initiation based on the Mohr-Coulomb model and Hashin model. For 2D plane stress states, the computational cost for determining damage initiation can …


Solvent Analysis Of Phenolic Resin Glass Fiber Reinforced Prepreg During Out-Time, Sixin Zhai, Crystal Ipong Jun 2021

Solvent Analysis Of Phenolic Resin Glass Fiber Reinforced Prepreg During Out-Time, Sixin Zhai, Crystal Ipong

Materials Engineering

Phenolic resin glass fiber reinforced prepregs are highly suitable for airplane interior components due to their high fire resistance, high temperature performance, and low-density characteristics. Safran Cabin seeks to improve their storage of the phenolic resin prepreg during their manufacturing process. The issues the company faces are the occasional delamination of prepreg laminas or the loss of tackiness rendering the lamina unfit for use. The area of investigation was determining the weight loss of volatiles during out-time. The term “out-time” consists of the time the prepreg experiences in transit, on the shop floor, and in short-term temperature-controlled storage. Simulated storage …


Experimental And Computational Analysis Of Progressive Failure In Bolted Hybrid Composite Joints, John S. Brewer Dec 2020

Experimental And Computational Analysis Of Progressive Failure In Bolted Hybrid Composite Joints, John S. Brewer

Theses and Dissertations

Composite materials are strong, lightweight, and stiff making them desirable in aerospace applications. However, a practical issue arises with composites in that they behave unpredictably in bolted joints, where damage and cracks are often initiated. This research investigated a solution to correcting the problem with composite bolted joints. A novel hybrid composite material was developed, where thin stainless steel foils were placed between and in place of preimpregnated composite plies during the cure cycle to reinforce stress concentrations in bolted joints. This novel composite was compared to control samples experimentally in quasi-static monotonic loading in double shear configuration in 9-ply …


Modeling Hybrid Composites Using Tsai-Wu And Hashin Failure Criterion, Candice R. Roberts Mar 2020

Modeling Hybrid Composites Using Tsai-Wu And Hashin Failure Criterion, Candice R. Roberts

Theses and Dissertations

Hybrid composites require further study and testing for future use in various fields. This study focuses on simulating a Hybrid Composite using IM7-977-3 laminae with steel foils in Abaqus under bolt loading by using Hashin and Tsai-Wu failure criterion. Initial simulations contain only the IM7-977-3 composite with cohesive layers. Foil samples were then tested for accurate material properties from which the simulations were then updated to include steel foils. The two models show that Tsai-Wu failure criterion, while great for anisotropic material in tension, does not prove accuracy around the hole of the composite material which is in compression. Hashin …


Low Weight Design Of A Pressure-Fed System For A Small Payload Launch Vehicle, Lucero Buendia Jan 2020

Low Weight Design Of A Pressure-Fed System For A Small Payload Launch Vehicle, Lucero Buendia

Open Access Theses & Dissertations

Carbon fiber reinforced polymer (CFRP) composites have become of great interests to aerospace industries because of their low-cost, lightweight and their tailorable mechanical properties. In aerospace structures, for example, heavy metals have been used in cryogenic fuel and oxidizer tanks for over 50 years. However, weight savings can be substantial if materials such as composites are used instead. From Delta IV heavy-lift launch vehicle it is known that cryogenic composite tanks can save approximately up to 30% of weight in fuel and oxidizer tanks. Although there is a wealth of studies in the mechanical behavior of composites at room temperature, …


Seismic Behavior Of Composite Bridge Columns, Mohanad M. Abdulazeez Jan 2020

Seismic Behavior Of Composite Bridge Columns, Mohanad M. Abdulazeez

Doctoral Dissertations

“This study investigates experimentally and numerically the seismic behavior of large-scale hollow-core fiber-reinforced polymer-concrete-steel (HC-FCS) innovative bridge columns as a sustainable approach to endure and rapidly recover from natural disasters such as earthquakes. The HC-FCS column consisted of a concrete shell sandwiched between an outer fiber-reinforced polymer (GFRP) tube and an inner steel tube to provided continuous confinement for the concrete shell along with the height of the column. The columns have a slender inner steel tube with diameter-to-thickness (Ds/ts) ratios ranged between 85 to 254. Each steel tube was embedded into the footing, while the …


Predicting The Mechanical Properties Of Nanocomposites Reinforced With 1-D, 2-D And 3-D Nanomaterials, Scott Edward Muller May 2019

Predicting The Mechanical Properties Of Nanocomposites Reinforced With 1-D, 2-D And 3-D Nanomaterials, Scott Edward Muller

Graduate Theses and Dissertations

Materials with features at the nanoscale can provide unique mechanical properties and increased functionality when included as part of a nanocomposite. This dissertation utilizes computational methods at multiple scales, including molecular dynamics (MD) and density functional theory (DFT), and the coupled atomistic and discrete dislocation multiscale method (CADD), to predict the mechanical properties of nanocomposites possessing nanomaterials that are either 1-D (carbyne chains), 2-D (graphene sheets), or 3-D (Al/amorphous-Si core-shell nanorod).

The MD method is used to model Ni-graphene nanocomposites. The strength of a Ni-graphene nanocomposite is found to improve by increasing the gap between the graphene sheet and a …


Interlaminar Damage Detection In Composite Materials, Hariharan Rangarajan Jan 2019

Interlaminar Damage Detection In Composite Materials, Hariharan Rangarajan

Williams Honors College, Honors Research Projects

Using ceramic matrix composites (CMCs) for high-temperature applications in jet engines increases durability and reduces weight and cooling requirements resulting in improved efficiency and fuel savings. Understanding, detecting, and monitoring different types of damage is essential to achieve optimal performance of CMC components. The Direct Current Potential Drop (DCPD) method is a non-destructive technique of estimating damage in composite materials.

DCPD technique works by measuring nodal potential differences when current is flown through the material. Direct current spreading in different woven and laminate composites is modeled to follow a ladder resistor network in which the nodal voltages decrease exponentially as …


Form Stable Phase-Change Materials, Russell Dent, Marjan Kashfipour, Nitin Mehra, Jiahua Zhu Jan 2019

Form Stable Phase-Change Materials, Russell Dent, Marjan Kashfipour, Nitin Mehra, Jiahua Zhu

Williams Honors College, Honors Research Projects

This work investigates the use of two different polyols, xylitol (Xyl) and erythritol (Ery), in conjunction with boron nitride (BN) aerogels, for the purpose of creating thermally conductive composites. While the BN filler in Xyl composites achieved a high anisotropic thermal conductivity of up to 4.53 W/m-K at 18.2 weight percent filler loading, they do not exhibit good phase-change material qualities due to a low solidification enthalpy even at low cooling rates. Alternatively, the BN-Ery composites have shown promising results with a solidification enthalpy of 225.14 J/g and a melting enthalpy of 385.84 J/g at a heat rate of 5 …


Effective Magnetic And Electric Response Of Composite Materials, Mona Hassan Alsaleh Nov 2018

Effective Magnetic And Electric Response Of Composite Materials, Mona Hassan Alsaleh

Doctoral Dissertations

Metamaterials (MMs) are nanocomposite materials consisting of metal-dielectric resonators much smaller in size than the wavelength of the incident light. Common examples of metamaterials are based on split ring resonators (SRRs), parallel wires or strips and fishnet structures. These types of materials are designed and fabricated in order to provide unique optical responses to the incident electromagnetic radiation that are not available in naturally existing materials. The MMs can exhibit unusual properties such as strong magnetism at terahertz (THz) and optical frequencies. Additionally, negative index materials (NIMs) can provide negative index of refraction which can be used in many applications …


Direct Sheet Molding Compound Process (D-Smc), Atieh Motaghi Feb 2018

Direct Sheet Molding Compound Process (D-Smc), Atieh Motaghi

Electronic Thesis and Dissertation Repository

The combination of highly crosslinked resin and long glass fiber reinforcement in direct sheet molding compound (D-SMC) provides the parts with high physical properties and low density suitable for large interior and exterior automotive applications. Different stages of D-SMC process including maturation zone and compression molding are studied using mathematical analysis, numerical simulation and experimental investigations.

An analytical analysis is used to calculate the pressure and velocity in the first section of maturation zone and then the permeability of fiber bundle is calculated by simulation and the agreement between the available empirical equation and simulation was obtained. The flow is …


Synthesis And Behavior Characterization Of Multi-Scale Hierarchical Structured Composites, Jacob M. Mayfield Jan 2018

Synthesis And Behavior Characterization Of Multi-Scale Hierarchical Structured Composites, Jacob M. Mayfield

Electronic Theses and Dissertations

The purpose of the synthesis of a multi-scale hierarchical composite material was to create a material with a high specific strength, a low mass, and high strength material. To achieve this the material categorization of the Formlabs Tough V2 resin was conducted. The resin was used in the construction of a bio-mimicry diamond lattice structure. The structure was subjected to compression testing to characterize the material properties. The Tough V2 resin structure combined with cellulose created a multi-scaled material on Macro and Micro levels to show the bio-inspired design to increase the material properties in a favorable manor. The Tough …


In Mold Flow Of Long Fibers In Compression Molding Process, Gleb Meirson Dec 2016

In Mold Flow Of Long Fibers In Compression Molding Process, Gleb Meirson

Electronic Thesis and Dissertation Repository

Long Fiber Thermoplastics (LFT) are promising new materials with high physical properties and low density. These high properties are obtained by embedding very long fibers (~100 mm) into a thermoplastic matrix. Such a high fiber length dictates the use of a compression molding process for manufacturing as the length of discontinuous fibers in injection molding is limited by pellet length.

LFT composites are of great interest for the automotive industry. These materials are already used in some interior and exterior car parts such as bumpers, seat structures, door module etc. This research is inspired by the desire to manufacture load …


Mechanical Properties And Fatigue Behavior Of Unitized Composite Airframe Structures At Elevated Temperature, Mohamed Noomen Sep 2016

Mechanical Properties And Fatigue Behavior Of Unitized Composite Airframe Structures At Elevated Temperature, Mohamed Noomen

Theses and Dissertations

The tension-tension fatigue behavior of a newly developed unitized composite material system was investigated. The unitized composite consisted of a polymer matrix composite (PMC) co-cured with a ceramic matrix composite (CMC). The PMC portion consisted of an NRPE high-temperature polyimide matrix reinforced with carbon fibers woven in an eight harness satin weave (8HSW). The CMC layer is a single-ply non-crimp 3D orthogonal weave composite consisting of ceramic matrix reinforced with glass fibers. In order to assess the performance and suitability of this composite for use in aerospace components designed to contain high-temperature environments, mechanical tests were performed under temperature conditions …


Swelling-Etching Characterization Of Copper (I) Oxide - Pdms For The Development Of Micro/Nano - Particles Composite Mems Corrosion Sensor, Abdoul Kader Maiga Jul 2015

Swelling-Etching Characterization Of Copper (I) Oxide - Pdms For The Development Of Micro/Nano - Particles Composite Mems Corrosion Sensor, Abdoul Kader Maiga

Graduate Theses and Dissertations

The primary objective for this thesis is to contribute to the understanding of the oxide removal process for a corrosion sensing device. The goal for designing such a device is for monitoring corrosion on metallic structures. The sensing material (6.35mm x 1mm discs) of the device is composed of copper (I) oxide particles mixed in some polydimethylsiloxane (PDMS). The PDMS, “housing,” is meant for controlling the oxidation rate through the sensing material. A solvent was used to facilitate the etchant diffusion through the PDMS matrix. Toluene and acetic acid were the ideal solvent and etchant, respectively, for carrying out the …


Creep Of Sylramic-Ibn Fiber Tows At Elevated Temperature In Air And In Silicic Acid-Saturated Steam, Kevin B. Sprinkle Jun 2015

Creep Of Sylramic-Ibn Fiber Tows At Elevated Temperature In Air And In Silicic Acid-Saturated Steam, Kevin B. Sprinkle

Theses and Dissertations

Stressed oxidation experiments on Sylramic-iBN fiber tows were performed to evaluate the novel fiber's mechanical performance, creep behavior, and creep mechanisms. This research effort investigated creep response of Sylramic-iBN fiber tows at elevated temperatures in both air and in silicic acid-saturated steam environments. Creep experiments were conducted at creep stresses ranging from 127 to 762 MPa at 400°C and 500°C in order to examine the mechanical behavior of the Sylramic-iBN fiber tows at temperatures below and above the melting point of boria (450°C). Sylramic-iBN fibers are known to have excellent creep resistance, better than most other non-oxide fibers and significantly …


Effect Of Prior Exposure At Elevated Temperatures On Tensile Properties And Stress-Strain Behavior Of Three Oxide/Oxide Ceramic Matrix Composites, Christopher J. Hull Mar 2015

Effect Of Prior Exposure At Elevated Temperatures On Tensile Properties And Stress-Strain Behavior Of Three Oxide/Oxide Ceramic Matrix Composites, Christopher J. Hull

Theses and Dissertations

Thermal stability of three oxide-oxide ceramic matrix composites was studied. The materials studied were NextelTM610/aluminosilicate (N610/AS), NextelTM720/aluminosilicate (N720/AS), and NextelTM720/Alumina (N720/A), commercially available oxide-oxide ceramic composites (COI Ceramics, San Diego, CA). The N610/AS composite consists of a porous aluminosilicate matrix reinforced with laminated woven alumina N610 fibers. The N720/AS and N720/A composites consist of a porous oxide matrix reinforced with laminated, woven mullite/alumina (NextelTM720) fibers. The matrix materials are aluminosilicate in N720/AS and alumina in N720/A. All three composites have no interface between the fibers and matrix, and rely on the porous …


Tension-Compression Fatigue Of An Oxide/Oxide Ceramic Matrix Composite At Elevated Temperature In Air And Steam Environments, Richard L. Lanser Mar 2015

Tension-Compression Fatigue Of An Oxide/Oxide Ceramic Matrix Composite At Elevated Temperature In Air And Steam Environments, Richard L. Lanser

Theses and Dissertations

Tension-compression fatigue behavior of an oxide-oxide ceramic matrix composite was investigated at 1200°C in air and steam. The composite is comprised of an alumina matrix reinforced with Nextel 720 fibers woven in an eight harness satin weave. The composite relies on a porous matrix for damage tolerance. Compression and tension tests to failure were conducted to characterize basic mechanical properties. Tension-compression fatigue tests were performed at 1 Hz frequency with a ratio of minimum to maximum stress of -1. Maximum stresses ranged from 60-120 MPa. Fatigue run-out (defined as 105 cycles) was achieved in air at 80 MPa and in …


Fatigue Behavior Of Im7/Bmi 5250-4 Composite At Room And Elevated Temperatures, James T. Tipton Mar 2015

Fatigue Behavior Of Im7/Bmi 5250-4 Composite At Room And Elevated Temperatures, James T. Tipton

Theses and Dissertations

The tension-tension fatigue and tension-compression fatigue behaviors of the IM7/BMI 5250-4 composite were investigated. The tension-tension fatigue of the composite with 0/90 and ±45 fiber orientations was studied at 23, 170, and 190°C. The tension-compression fatigue of the composite with 0/90 fiber orientation was examined at 23°C. The tensile and compressive properties of the composite were also evaluated at room and elevated temperatures for both 0/90 and ±45 fiber orientations. Elevated temperature had little effect on the tensile properties of the 0/90 fiber orientation, but strongly influenced the ±45 tensile properties as well as the compressive properties of both fiber …


Ultrasonics Transduction In Metallic And Composite Structures For Structural Health Monitoring Using Extensional And Shear Horizontal Piezoelectric Wafer Active Sensors, Ayman Kamal Abdelrahman Aug 2014

Ultrasonics Transduction In Metallic And Composite Structures For Structural Health Monitoring Using Extensional And Shear Horizontal Piezoelectric Wafer Active Sensors, Ayman Kamal Abdelrahman

Theses and Dissertations

Structural health monitoring (SHM) is crucial for monitoring structures performance, detecting the initiation of flaws and damages, and predicting structural life span. The dissertation emphasizes on developing analytical and numerical models for ultrasonics transduction between piezoelectric wafer active sensors (PWAS), and metallic and composite structures.

The first objective of this research is studying the power and energy transduction between PWAS and structure for the aim of optimizing guided waves mode tuning and PWAS electromechanical (E/M) impedance for power-efficient SHM systems. Analytical models for power and energy were developed based on exact Lamb wave solution with application on multimodal Lamb wave …


Experimental And Finite Element Studies Of Shock Transmission, Eldon Jerry Goddard Dec 2013

Experimental And Finite Element Studies Of Shock Transmission, Eldon Jerry Goddard

UNLV Theses, Dissertations, Professional Papers, and Capstones

Composite materials are more widely used today in engineering products than ever before. Shock transmission in jointed composite sections needs to be investigated to understand the affect of composite materials on the dynamic response of the system. There exists limited published work on transient shock propagation through composite sections. The aim of this study is to analyze the transient behavior of joints in composite materials subjected to low impact loads and to develop a computational model that provides an improved physics based shock model. The jointed connection will be investigated experimentally and using Finite Element Analysis (FEA). The bolted joint …


Solution To Certain Problems In The Failure Of Composite Structures, Jonathan Goodsell Oct 2013

Solution To Certain Problems In The Failure Of Composite Structures, Jonathan Goodsell

Open Access Dissertations

The present work contains the solution of two problems in composite structures. In the first, an approximate elasticity solution for prediction of the displacement, stress and strain fields within the m-layer, symmetric and balanced angle-ply composite laminate of finite-width subjected anticlastic bending deformation is developed. The solution is shown to recover classical laminated plate theory predictions at interior regions of the laminate and thereby illustrates the boundary layer character of this interlaminar phenomenon. The results exhibit the anticipated response in congruence with the solutions for uniform axial extension and uniform temperature change, where divergence of the interlaminar shearing stress is …


Mechanical And Electro-Chemical Investigation Of Carbon Farbric/Epoxy And Aluminum Foam Sandwich Composite Beams, Narin Sara Fatima Jan 2013

Mechanical And Electro-Chemical Investigation Of Carbon Farbric/Epoxy And Aluminum Foam Sandwich Composite Beams, Narin Sara Fatima

Wayne State University Theses

In this study the mechanical and electrochemical response of a sandwich composite comprising of carbon fiber fabric skin and aluminum foam core was evaluated. The three point flexural test was chosen to investigate the mechanical behavior in terms of finding the deformation and failure behavior. The flexural test exhibited an excellent bond between the skin and the core. The specimens mainly failed in three different modes - indentation, core shear and face yielding and showed three distinct regions: a linear rise in load with displacement region, a rapid load drop region and a plateau region followed by a densification region. …


Effect Of Thermal Annealing And Carbon Implantation On The Functional Properties Of Nanocomposite Tisin Coatings On Steel, Mohammad Shoeb Ahmed Jan 2013

Effect Of Thermal Annealing And Carbon Implantation On The Functional Properties Of Nanocomposite Tisin Coatings On Steel, Mohammad Shoeb Ahmed

Theses: Doctorates and Masters

This PhD research contributes to the part of advanced materials technology. The machining industry currently faces tremendous pressures with the need for durable cutting tools suitable for eco-friendly high speed machining operations becoming acute. In this thesis innovative design and synthesis strategies are explored to tailor the properties of nanocomposite coatings. Advanced characterisation techniques are applied to identify the mechanisms that control the mechanical, tribological, and corrosion behaviours of these coatings. Cutting tools protected by these coatings are anticipated to exhibit a unique combination of superior toughness and greater resistance to wear and corrosion, providing significant economic and environmental benefits. …


Creep Behavior In Interlaminar Shear Of A Cvi Sic/Sic Composite At Elevated Temperatures In Air And Steam, Matthew T. Pope Mar 2012

Creep Behavior In Interlaminar Shear Of A Cvi Sic/Sic Composite At Elevated Temperatures In Air And Steam, Matthew T. Pope

Theses and Dissertations

This research investigated the interlaminar shear performance of a SiC/SiC ceramic matrix composite. The interlaminar shear performance was observed in compression of double notched specimens (DNS) at 1200°C in both laboratory air and in steam. Compression to failure tests determined the as-processed interlaminar shear strength and interlaminar shear creep tests were conducted with stresses ranging from -22 MPa to -16 MPa. Primary and secondary creep regimes were observed in all creep tests. The specimens tested in creep at -16 MPa in air achieved run-out, defined as 100 hours at creep stress. The residual strength decreased slightly after 100 h of …