Engineering Commons^™

Development Of A Potassium Permanganate Catalyst-Infused Fuel Grain For Hydrogen Peroxide Hybrid Thruster Ignition Enhancement, Ryan J. Thibaudeau

All Graduate Theses and Dissertations, Fall 2023 to Present

This thesis describes and addresses the need for reliable ignition in small satellite hybrid propulsion systems using hydrogen peroxide. It describes process of creating custom 3D printed ABS plastic fuel grains with small amounts of catalysts. These catalysts lead to a more reliable and energy-efficient ignition of a hybrid rocked propulsion system using catalyst-infused ABS and high-test hydrogen peroxide (HTP). Hydrogen peroxide is a high-density oxidizer and therefore more volumetrically efficient for a small satellite using hybrid rocket technology when compared to gaseous oxygen (GOX). The traditional ignition methods of hybrid rocket propulsion systems using HTP are compared to and …

Fusion Bonding Behavior Of 3d Printed Pa6/Cf Composites Via Post Fabrication Compaction, Gonzalo Fernandez Mediavilla

Mechanical & Aerospace Engineering Theses & Dissertations

Additive manufacturing (AM) is becoming a robust production technology for aerospace, healthcare, and construction industries among others. Fused Deposition Modelling (FDM) is one of the methods most used to 3D print products. FDM has limitation due to interlayer adhesion and restriction imposed by the printing direction. Specially with AM composites, as reinforced nylon PA6 with short fibers, parts show more strength along the direction of the filament due to the alignment of the carbon fibers, but weaker in other directions. The proposed method to solve this issue is to print parts separately and join them together by fusion bonding. PA6/CF …

Development Of A Regeneratively Cooled Liquid Rocket Engine, Dillon Petty, Nicole Zimmerli

Williams Honors College, Honors Research Projects

An additively manufactured (AM) liquid rocket engine, consisting of an injector, combustion chamber, and nozzle, was designed and printed using state-of-the-art methods and materials. The parts were manufactured using laser powder bed fusion. Additive manufacturing allowed for complex geometries and features, such as printing manifolds onto the components with a reduced number of parts. Additive, regenerative cooling channels were designed into the chamber and nozzle to allow for long-duration steady-state operation.

The feed system for the engine was designed and built to allow for pressure-regulated and steady-state testing. Tanks for the fuel and oxidizer were designed and built for a …

Mechanical Properties And Tension-Tension Fatigue Behavior Of A Novel Additively Manufactured Polymer Matrix Composite At Room And Elevated Temperature, Grayson M. Harber

Theses and Dissertations

The tension-tension fatigue behavior of a novel additively manufactured AM carbon fiber reinforced polymer matrix composite was studied. This novel material system consists of T1100 carbon fibers, and a UV photocured resin developed by Continuous Composites and Sartomer. Tensile properties and tension-tension fatigue were investigated for the 090 fiber orientation as well as for the ±45 fiber orientation. Specimens with 0/90 fiber orientation were tested at ambient laboratory temperature 23 °C and at elevated temperature 150 °C, while the specimens with the ±45 fiber orientation were tested only at ambient laboratory temperature. Tension-tension fatigue testing was carried out with a …

Finite Fatigue Life Prediction Of Additively Manufactured Aircraft Engine Turbine Blade With Respect To Internal Defect Size And Location, Daniel G. Miller

Theses and Dissertations

Current fatigue life modeling techniques with respect to defects emphasize the dependence on the defect size with respect to fatigue life, but does not account for the effects of where a defect might be located. This research outlines a process to include defect location into the model analysis for a more precise prediction of the number of cycles to failure and where the finial failure could occur within a component. The focus is on a turbine blade structure using IN718 subjected to a pure vibratory load. The basic model predicts component life using a stress map from the frequency analysis …

Additive Manufacturing Of Molybdenum For High Temperature Structural Applications, Megan L. Bustin

Theses and Dissertations

This research considered additive manufactured (AM) molybdenum (Mo) and the effect of three variables on microstructure, mechanical properties, and the relationship between the two. Test temperature, laser speed, and shield gas or build atmosphere were varied, and samples tested and analyzed using a three-point bending test, chemical composition, and optical and scanning electron microscopy. The relationship among variables and results using a Design of Experiments was limited compared to the inclusion of every tested sample. Most effects were expected: samples tested at room temperature were brittle without statistical significance; increasing laser speed resulted in decreased ductility and strain, smaller grain …

Characterization Of 3d Printed Parts Containing Integrated Functionality Via Ultrasonically Embedded Wires, David Abraham Sepulveda

Open Access Theses & Dissertations

Material extrusion additive manufacturing has been widely adopted because it offers freedom of design, which allows complex geometry fabrication, and rapid prototyping. Interest in producing components with integrated functionality allowed forms of hybrid manufacturing to be developed such as the Multi3D system. This system produces parts with embedded components by combining additive, subtractive, soldering, dispensing, and embedding techniques. However, this involves pausing the printing process (which takes place in a controlled environment) and exposing it to ambient temperature where embedding takes places. In this research, the effect of embedding parts with 24 AWG copper for improved functionality was quantified mechanically. …

Fabrication And Testing Of Catalyst-Infused Filament For 3d Printing Of Ignition-Augmented Hybrid Rocket Fuels, Kurt C. Olsen

All Graduate Theses and Dissertations, Spring 1920 to Summer 2023

This thesis describes and addresses the need for reliable ignition in small satellite hybrid propulsion systems using higher density oxidizers. It describes methods of creating custom 3D printing ABS plastic based filaments that contain small amounts of catalysts. These catalysts lead to a more reliable and energy-efficient ignition of a hybrid rocked propulsion system using catalyst-infused ABS and nitrous oxide and oxygen blend called Nytrox, commonly known as ”laughing gas.” The ”laughing gas” has a higher density and can therefore provide more ”miles per gallon” in a hybrid propulsion system on a small satellite when compared to gaseous oxygen (GOX). …

Experimental Characterization Of Additively Manufactured Multi-Feather Wingtip Devices, Patricio Garzon

Doctoral Dissertations and Master's Theses

Soaring birds have evolved to fly for long periods of time without flapping their wings. Inspired by the flight of these birds, the proposed thesis presents an experimental investigation focused on wingtip devices designed based on biomimicry. The overarching engineering objective was to reduce the induced drag as a means to improve the fuel efficiency via these experimental wingtips. An associated secondary objective was to establish a method for manufacturing complex structures suitable for wing tunnel testing. A manufacturing technique that involved using composite weaves to reinforce additively manufactured structures was developed. This technique has the potential to reduce manufacturing …

Performance Study Of Post-Processed Additively Manufactured Low Thrust Nozzles, Tyler W. Gerhold

Theses and Dissertations

This research explores metal post-processing techniques to effectively reduce the large anomalous protrusions found in small additively manufactured low thrust rocket nozzles. Research has found that nozzles of this kind can experience losses in thrust of over 40%. Analytic theory of adiabatic nozzle flow with viscous losses for additively manufactured nozzles does not align with what has been found when tested experimentally. Compressible flow losses, such as shock wave formation inside the nozzle diverging cone, are likely the leading causes of such loss. Reduction in nozzle irregularities can likely yield results seen in analytic theory with similar performance to traditional …

Investigation Of Additively Manufactured Molybdenum-Tungsten-Rhenium Alloys, Randolph T. Abaya

Theses and Dissertations

The process of creating metal components through additive manufacturing is changing the way different industries can avoid the shortcomings of traditional metal production. Metals such as tungsten, molybdenum, and rhenium have many advantages for different applications, especially when alloyed together. In this study, an additively manufactured alloy containing 70% molybdenum, 25% tungsten, and 5% rhenium (70Mo-25W-5Re) is tested for its strength, ductility, hardness, and porosity. The 70Mo-25W-5Re alloy is printed through Laser Powder Bed Fusion (LPBF) under different conditions such as printing speed and printing atmosphere. Additionally, the effects of post printing heat treatment are conducted to understand the advantages …

Design And Testing Of A Composite Compressor Rotor, Mauro Noel V. De Leon

Theses and Dissertations

Additive manufacturing (AM) and molding are manufacturing methods known for building representations or replicas of conceptualized engine components, but was considered impractical for manufacturing operating engine components. More recent technology has rendered composite materials (combining high-temperature polymers and fiber reinforcement) capable of withstanding the temperature and structural requirements to compete with conventional turbomachinery metals. This study explores the application of several high-temperature polymers (ULTEM 9085, Onyx-Carbon fiber, and Epoxy-Carbon fiber) and their survivability in the operating conditions of a P400 Engine compressor. The tests conducted for this study determined their viability as compressor materials. This study required conducting tensile specimen …

Effects Of A Nitrogen And Hydrogen Build Atmosphere On The Properties Of Additively Manufactured Tungsten, Dana C. Madsen

Theses and Dissertations

Additively manufactured tungsten was printed in pure nitrogen, nitrogen-2.5% hydrogen, and nitrogen-5% hydrogen atmospheres as part of a 2^3 full factorial designed experiment and subjected to room temperature and high-temperature three-point-bend testing, chemical analysis, hardness testing, and microstructural imaging techniques. The pure nitrogen specimens exhibited the highest strength and ductility at both high temperature and room temperature. Chemical analysis showed a 2-8x reduction in compositional oxygen relative to unprocessed powder. Hardness values for all samples was between 306.8 and 361.5 HV1. It is proposed that adding hydrogen into the build atmosphere reduced the available energy density for tungsten melting by …

Post-Processing And Characterization Of Additive Manufactured Carbon Fiber Reinforced Semi-Crystalline Polymers, Patricia Revolinsky

Mechanical & Aerospace Engineering Theses & Dissertations

The aim of this work is to study the effect of post-processing on additive manufactured (AM) continuous carbon fiber reinforced plastics (CFRPs) performance. As-printed AM CFRPs do not perform as well as conventionally manufactured CFRPs with the same composition. Possible improvements to AM CFRP performance include annealing and applying uniaxial pressure with elevated temperature. Samples were subjected to pressure and temperature treatments and annealing at a constant temperature. Treated materials were subjected to three-point bending tests, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM) to characterize and assess sample performance. Results were assessed for flexural strength, …

Evaluation Of Additively Manufactured Lattices Under High Strain Rate Impact, Derek G. Spear

Theses and Dissertations

Several additively manufactured lattice designs and configurations were evaluated under compression loads under various strain rates from quasi-static to highly dynamic. These experiments examined how the mechanical behavior of the lattice changed based on the lattice design properties and the applied strain rates. The modulus of elasticity, yield strength, plateau stress, and toughness were observed to decrease with an increase in strain rate, revealing that the lattice designs exhibit a negative strain rate sensitivity. A new lattice flow stress model was developed to account for the mechanical response of the lattice and was incorporated into a computational model for simulation. …

A Reduced Order Model Of The Celestial Icosahedron As The Substructure For A Lighter Than Air Vehicle, Torin C. Quick

Theses and Dissertations

A finite element approach was used to investigate a novel reduced order model to determine the minimum structure dimensionality to support vacuum for a VLTAV. This modeling technique represented the individual segments of the substructure as curved beams with clamped radially-resisted boundary conditions. The full structure was then modeled as a bare structure and structure with skin to validate the results of the reduced order model. The beam geometry for the material Ultem 9085 was determined through this process leading to the 3-D printing of the structure. It was then experimentally tested under uniaxial compression complimented with a FEA model.

Improving Manufacturability And Reducing Cracking In Additively Manufactured Tungsten Alloys, Christopher P. Fassio

Theses and Dissertations

Additively Manufactured tungsten suffers from low () densities due to high concentrations of microcracks as the printed layers cool past tungsten's high ductile to brittle transition temperature. In this study, tungsten-rhenium and tungsten rhenium hafnium carbide compositions were evaluated on density and tensile strength. In addition to varying the compositions of each alloy, printing parameters and post-processing methods were also compared. Print parameters varied for all compositions on an MLab 200R C using included the laser scan strategy, hatch spacing, scan speed, laser power, and print bed material. Post processing techniques of the WRe compositions included hot isostatic pressing and …

The Effect Of Compaction Temperature And Pressure On Mechanical Properties Of 3d Printed Short Glass Fiber Composites, Pushpashree Jain Ajith Kumar Jain

Mechanical & Aerospace Engineering Theses & Dissertations

Among many thermoplastics that are used in engineering, polyamide 6 (nylon 6) is an extremely versatile engineering thermoplastic. Nylon filled with glass fibers has higher mechanical strength and high wear resistance than general purpose nylon. 3D printed composites, based on fused filament modeling, typically suffer from poor bead-to-bead bonding and relatively high void content, limiting their mechanical properties

This thesis explores the effect of compaction pressure and temperature on improving the mechanical properties of 3D printed composites. Engineering moduli in the printing and transverse to printing direction, as well as ultimate strength were measured using the tensile testing with Digital …

Analysis For Hybrid Rocket Fuel Regression Using Stereolithographic Geometry, Michael P. King

Theses and Dissertations

Hybrid Rocket Engines (HRE) have characteristically low fuel regression that limits their performance. Additive manufacturing and rapid prototyping can possibly solve some of the problems with Hybrid propulsion regression by creating geometry not possible with conventional manufacturing. This work is attempting to make geometric regression simulation of HRE easier by using STereoLithography (STL files) as the geometry. This analysis sets flow conditions, boundary conditions, propellant selection, and allows for fuel geometry to be altered to simulate geometry’s effects on regression rate and propellant performance. This model can be used for more advanced geometric analysis to improve and predict performance.

Investigation Of Ultem 9085 For Use In Printed Orbital Structures, William R. Gallagher

Theses and Dissertations

Additive manufacturing is revolutionizing industries ranging from medicine to space. However, the structural characteristics of plastic parts created by these methods are not as well understood as their more established counterparts. This research explored two relevant areas: how the structural characteristics of ULTEM 9085 plastic behaved after exposure to orbital conditions and the design of the cross-sectional area of a beam to be 3-D printed in microgravity based on the expected loads from the printer. To study orbital effects, ULTEM 9085 was printed into 1/4th scale ASTM D638- 14 dogbones using a Stratasys 450mc printer. These dogbones were placed in …

Structural Dynamic And Inherent Damping Characterization Of Additively Manufactured Airfoil Components, Andrew W. Goldin

Theses and Dissertations

The push for low cost and higher performance/efficient turbine engines have introduced a new demand for novel technologies to improve robustness to vibrations resulting in High Cycle Fatigue (HCF). There have been many proposed solutions to this, some passive and some active. With the advent of Additive Manufacturing (AM), new damping techniques can now be incorporated directly into the design and manufacture process to suppress the vibrations that create HCF. In this study, this novel unfused pocket damping technology is applied to a blade structure and the resulting damping effectiveness is quantified. The application of this technology to complex geometries …

Solution Anneal Heat Treatments To Enhance Mechanical Performance Of Additively Manufactured Inconel 718, David J. Newell

Theses and Dissertations

The nickel-based superalloy Inconel 718 (IN718) is an excellent candidate among aerospace alloys for laser powder-bed fusion (LPBF) manufacturing. As-built LPBF IN718 has a vertically aligned columnar (001) microstructure which translates into orthotropic mechanical behavior. The post-process heat treatments for IN718 were developed 60 years ago for wrought and cast processes and do not mitigate the columnar microstructure of the LPBF process. Recrystallization is required to remove the columnar microstructure, which would allow for parts to be fabricated on different machines or in different orientations but still achieve the same properties. This research investigated the microstructure of LPBF IN718 as …

Analysis Of Additively Manufactured Rings Under Compression Loading For Use In A Vacuum Lighter Than Air Vehicle Structure, Kevin D. Greenoe

Theses and Dissertations

A Vacuum Lighter Than Air Vehicle (VLTAV) utilizes a lightweight structure paired with an internal vacuum to achieve buoyancy; this allows it to float through-out a given atmosphere. The pressure differential between the internal vacuum andexternal atmosphere places the vehicle under intense loading. A specific structure under investigation is the celestial icosahedron, which features nine intersecting rings that have an outer diameter of 0.2032m and circular cross-sectionalthickness of 5.08mm.The celestials rings are positioned in three different orientations and are analyzed both experimentally and analytically.

Design, Development, And Testing Of A Low Cost, Additively-Manufactured, Centrifugal Compressor, Aaron P. Bauer

Theses and Dissertations

The three objectives of this research were to: 1.) design, build, and test AM compressors to substitute into COTS micro-gas turbine engines, 2.) provide initial correlations between FEA and compressor failure speed, and 3.) characterize the effects of AM on compressor performance. These goals improved the design cycle cost and the design-validation time cycle. ULTEM 9085, 300-AMB, and Onyx-Kevlar temperature-dependent tensile properties were measured. FEA-predicted failure speeds of stock compressor designs led design improvements, potentially fulfilling the original compressor requirements. Physical testing of the stock and ULTEM 9085 compressors occurred. Comparing these compressors' performances demonstrated that low cost, AM materials …

Fabrication And Characterization Of Multifunctional Composites, Aditya R. Thakur

Doctoral Dissertations

“This study details the research to facilitate fabrication and characterization of novel structural composites reinforced with carbon fibers. Across industries, materials with high performance-to-weight ratio are sought after. Using carbon fibers as secondary phases in these proposed composites, specific characteristics can be tailored in these materials to manufacture strong, lightweight, high performance structures. The first part of the research focused on the improvement in the mechanical properties of the composites using carbon fiber reinforcement. As a part of this study, toughened ceramic composites with predictable failure patterns were produced using carbon fiber inclusions. A closed-form analytical model was developed to …

Application Of Metamaterials For Multifunctional Satellite Bus Enabled Via Additive Manufacturing, Michael A. Macchia

Theses and Dissertations

Space systems require materials with superior stiffness to weight ratios to provide structural integrity while minimizing mass. Additive manufacturing processes enable the design of metamaterials that exceed the performance of naturally occurring materials in addition to allowing the integration of non-structural functions. This research explored the use of a high stiffness, high density, small melt pool track width AM material, Inconel 718, to enable the production of metamaterials with finer features possible than can possibly be created using a lower density aluminum alloy material. Various metamaterials were designed utilizing thin wall triply periodic minimal surface infilled sandwich structures. The performance …

Thermal Management Of Satellite Electronics Via Gallium Phase Change Heat Sink Devices, Brian O. Palmer

Theses and Dissertations

The purpose of this research was to determine the effectiveness and feasibility of additively manufactured heat sinks using gallium as a phase change material in the thermal management of satellite electronics. A design was created based on the footprint of an Astronautical Development, LLC Lithium 1 UHF radio and six heat sinks were additively manufactured; two each of stainless steel 316, Inconel 718, and ULTEM 9085. Each heat sink was filled with gallium for testing purposes. Models were created to simulate the behavior of the heat transfer and phase change processes occurring within the heat sink. Additionally, laboratory data was …

Additively-Manufactured Hybrid Rocket Consumable Structure For Cubesat Propulsion, Britany L. Chamberlain

All Graduate Theses and Dissertations, Spring 1920 to Summer 2023

Three-dimensional, additive printing has emerged as an exciting new technology for the design and manufacture of small spacecraft systems. Using 3-D printed thermoplastic materials, hybrid rocket fuel grains can be printed with nearly any cross-sectional shape, and embedded cavities are easily achieved. Applying this technology to print fuel materials directly into a CubeSat frame results in an efficient, cost-effective alternative to existing CubeSat propulsion systems. Different 3-D printed materials and geometries were evaluated for their performance as propellants and as structural elements. Prototype "thrust columns" with embedded fuel ports were printed from a combination of acrylonitrile utadiene styrene (ABS) and …

Ultrasonic Nondestructive Evaluation Of Metal Additive Manufacturing., Venkata Karthik Nadimpalli

Electronic Theses and Dissertations

Metal Additive Manufacturing (AM) is increasingly being used to make functional components. One of the barriers for AM components to become mainstream is the difficulty to certify them. AM components can have widely different properties based on process parameters. Improving an AM processes requires an understanding of process-structure-property correlations, which can be gathered in-situ and post-process through nondestructive and destructive methods. In this study, two metal AM processes were studied, the first is Ultrasonic Additive Manufacturing (UAM) and the second is Laser Powder Bed Fusion (L-PBF). The typical problems with UAM components are inter-layer and inter-track defects. To improve the …

Effects Of Manufacturing Process Variables On Ultrasonic Testing In Electron Beam Melted Ti-6al-4v, Andrew D. Durkee

Theses and Dissertations

Further research on validating additive manufacturing production quality is required before the realization of direct print-to-fly application of critical components. This research examines the response of ultrasonic testing as a function of various manufacturing variables in electron beam melted samples of Ti-6Al-4V. Four dimensionally identical blocks with 6 spherical voids at varying depths were manufactured using different combinations of stock powder, edge treatments, and void melting. Scans were completed on two sides of each specimen with the transducer focused on the mid-plane. Additionally, one specimen was scanned 6 times, with the focal plane adjusted for each scan to match the …