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Articles 1 - 9 of 9
Full-Text Articles in Engineering
Development And Characterization Of Forcespinning® Mesquite Gum Nanofibers, Cristobal Rodriguez, Victoria I. Padilla, Karen Lozano, Alexa Villarreal, Luis A. Materon, Robert Gilkerson
Development And Characterization Of Forcespinning® Mesquite Gum Nanofibers, Cristobal Rodriguez, Victoria I. Padilla, Karen Lozano, Alexa Villarreal, Luis A. Materon, Robert Gilkerson
Mechanical Engineering Faculty Publications and Presentations
In this study, nanofibers incorporating Prosopis glandulosa mesquite gum (MG) exudate combined with biodegradable polymers, pullulan (PL) and chitosan (CH), were produced via the Forcespinning® technique. The nonwoven composite membranes were characterized via scanning electron microscopy followed by thermogravimetric and Fourier-transform infrared spectroscopy analysis. MG nanofiber composites comprised long, continuous fibers with an average fiber diameter of 523 ± 180 nm and 760 ± 225 nm for 18.1 and 28 wt% of MG, respectively. These composite membranes were water-stable after crosslinking via heat treatment with a ∼3 % water absorption capacity, and demonstrated a thermal capability with an increasing …
Antimicrobial Mechanisms Of Biomaterials: From Macro To Nano, Shounak Roy, Sanchita Sarkhel, Deepali Bisht, Samerender Nagam Hanumantharao, Smitha Rao, Amit Jaiswal
Antimicrobial Mechanisms Of Biomaterials: From Macro To Nano, Shounak Roy, Sanchita Sarkhel, Deepali Bisht, Samerender Nagam Hanumantharao, Smitha Rao, Amit Jaiswal
Michigan Tech Publications
Overcoming the global concern of antibiotic resistance is one of the biggest challenge faced by scientists today and the key to tackle this issue of emerging infectious diseases is the development of next-generation antimicrobials. The rapid emergence of multi-drug resistant microbes, superbugs and mutated strains of viruses have fueled the search for new and alternate antimicrobial agents with broad-spectrum biocidal activity. Biomaterials, ranging from macroscopic polymers, proteins, and peptides to nanoscale materials such as nanoparticles, nanotubes and nanosheets have emerged as effective antimicrobials. An extensive body of research has established the antibacterial and antiviral efficiencies of different types of biomaterials. …
Fabrication Of Forcespinning® Nanofibers Incorporating Nopal Extract, Cristobal Rodriguez, Victoria Padilla, Karen Lozano, J. Andrew Mcdonald, Luis Materon, Alejandra Chapa, Fariha Ahmad, Carlos Trevino De Leon, Robert Gilkerson
Fabrication Of Forcespinning® Nanofibers Incorporating Nopal Extract, Cristobal Rodriguez, Victoria Padilla, Karen Lozano, J. Andrew Mcdonald, Luis Materon, Alejandra Chapa, Fariha Ahmad, Carlos Trevino De Leon, Robert Gilkerson
Biology Faculty Publications and Presentations
In this study, nanofibers composed of Opuntia cochenillifera nopal mucilage (N) extract combined with chitosan (CH) and pullulan (PL) (N/CH/PL) were produced via Forcespinning®. The developed nonwoven composite membranes are comprised of long, continuous, and homogenous fibers with fiber average diameter varying between 251±77 nm and 406±127 nm depending on the concentration of N. After crosslinking, the developed membranes were highly stable in water. The water absorption capacity of the N/CH/PL composite nanofiber membranes was shown to be 65% higher when compared to the CH/PL nanofiber membranes. Nopal dipcoated membranes show inhibition of gram-negative Escherichia coli, indicating antibacterial properties. These …
Measurement Of Antibacterial Properties Of Foil‑Backed Electrospun Nanofibers, Mary Ann Wagner-Graham, Herbert Barndt, Mark Andrew Sunderland
Measurement Of Antibacterial Properties Of Foil‑Backed Electrospun Nanofibers, Mary Ann Wagner-Graham, Herbert Barndt, Mark Andrew Sunderland
College of Life Sciences Faculty Papers
Current methodologies for evaluation of antibacterial properties of traditional textiles are not applicable to foil‑backed, poorly‑absorbent electrospun nanofiber materials, since existing test methods require absorbent fabrics. Since electrospun nanofibers are adhered to the foil backing only by electrostatic interactions, methods used to evaluate antibacterial properties of surfaces cannot be used because these protocols cause the nanofibers to lift from the foil backing. Therefore, a novel method for measurement of the antibacterial properties of electrospun metallic foil‑backed nanofiber materials was developed. This method indicated that acetate‑based nanofibers manufactured to contain 5 to 30 weight percent of cold‑pressed hemp seed oil or …
Antibacterial Properties Of Mussel-Inspired Polydopamine Coatings Prepared By A Simple Two-Step Shaking-Assisted Method, Pegah Kord Fooroshani, Elizabeth Polega, Kevin Thomson, Mohammad Saleh Akram Bhuiyan, Rattapol Pinnaratip, Mikhail Trought, Chito E. Kendrick, Yuesheng Gao, Kahryn Perrine, Lei Pan, Bruce P. Lee
Antibacterial Properties Of Mussel-Inspired Polydopamine Coatings Prepared By A Simple Two-Step Shaking-Assisted Method, Pegah Kord Fooroshani, Elizabeth Polega, Kevin Thomson, Mohammad Saleh Akram Bhuiyan, Rattapol Pinnaratip, Mikhail Trought, Chito E. Kendrick, Yuesheng Gao, Kahryn Perrine, Lei Pan, Bruce P. Lee
Michigan Tech Publications
A simple two-step, shaking-assisted polydopamine (PDA) coating technique was used to impart polypropylene (PP) mesh with antimicrobial properties. In this modified method, a relatively large concentration of dopamine (20 mg ml−1) was first used to create a stable PDA primer layer, while the second step utilized a significantly lower concentration of dopamine (2 mg ml−1) to promote the formation and deposition of large aggregates of PDA nanoparticles. Gentle shaking (70 rpm) was employed to increase the deposition of PDA nanoparticle aggregates and the formation of a thicker PDA coating with nano-scaled surface roughness (RMS = 110 …
Polyelectrolyte-Functionalized Nanofiber Mats Control The Collection And Inactivation Of Escherichia Coli, Katrina A. Rieger, Michael Porter, Jessica D. Schiffman
Polyelectrolyte-Functionalized Nanofiber Mats Control The Collection And Inactivation Of Escherichia Coli, Katrina A. Rieger, Michael Porter, Jessica D. Schiffman
Chemical Engineering Faculty Publication Series
Quantifying the effect that nanofiber mat chemistry and hydrophilicity have on microorganism collection and inactivation is critical in biomedical applications. In this study, the collection and inactivation of Escherichia coli K12 was examined using cellulose nanofiber mats that were surface-functionalized using three polyelectrolytes: poly (acrylic acid) (PAA), chitosan (CS), and polydiallyldimethylammonium chloride (pDADMAC). The polyelectrolyte functionalized nanofiber mats retained the cylindrical morphology and average fiber diameter (~0.84 µm) of the underlying cellulose nanofibers. X-ray photoelectron spectroscopy (XPS) and contact angle measurements confirmed the presence of polycations or polyanions on the surface of the nanofiber mats. Both the control cellulose and …
Antibacterial Performance Of Bovine Lactoferrin-Fish Gelatine Electrospun Membranes, J Padrão, Raul Machado, Margarida Casal, Senentxu Lanceros-Méndez, L R. Rodrigues, F Dourado, Vitor Sencadas
Antibacterial Performance Of Bovine Lactoferrin-Fish Gelatine Electrospun Membranes, J Padrão, Raul Machado, Margarida Casal, Senentxu Lanceros-Méndez, L R. Rodrigues, F Dourado, Vitor Sencadas
Faculty of Engineering and Information Sciences - Papers: Part A
The increase of antibiotic resistant microorganisms urged the development and synthesis of novel antimicrobial biomaterials to be employed in a broad range of applications, ranging from food packaging to medical devices. This work describes the production and characterization of a protein-based electrospun fibrous membranes bearing antimicrobial properties. Its composition is exclusively comprised of proteins, with fish gelatine as structural matrix and bovine lactoferrin (bLF) as the active antimicrobial agent. The bLF bactericidal effect was determined against clinical isolates of Escherichia coli and Staphylococcus aureus through microdilution assays. Two distinctive methods were used to incorporate bLF into the fish gelatine nanofibres: …
Novel Microwave Assisted Synthesis Of Zns Nanomaterials, Suresh Pillai, Michael Seery, Damian Synnott, John Colreavy, Stephen Hinder
Novel Microwave Assisted Synthesis Of Zns Nanomaterials, Suresh Pillai, Michael Seery, Damian Synnott, John Colreavy, Stephen Hinder
Articles
A novel ambient pressure microwave-assisted technique is developed in which silver and indium modified ZnS is synthesised. The as prepared ZnS is characterised by X-ray diffraction, UV-Vis spectroscopy, X-ray photoelectron spectroscopy and luminescence spectroscopy. This procedure produced crystalline materials with particle sizes below 10 nm. The synthesis technique leads to defects in the crystal which induce mid energy levels in the band gap and lead to indoor light photocatalytic activity. Increasing the amount of silver causes a phase transition from cubic blende to hexagonal phase ZnS. In a comparative study, when the ZnS cubic blende is heated in a conventional …
An Investigation Of The Biochemical Properties Of Tetrazines As Potential Coating Additives, Swarna Jaiswal, Brendan Duffy, Luke O'Neill, Patrick Mchale
An Investigation Of The Biochemical Properties Of Tetrazines As Potential Coating Additives, Swarna Jaiswal, Brendan Duffy, Luke O'Neill, Patrick Mchale
Articles
1,2,4,5-Tetrazine and its 3,6-disubstituted derivatives are currently used for a range of industrial and medical applications as they exhibit particular coordination chemistries, characterized by electron and charge transfer phenomena. The aim of the present work is to describe the synthesis of two tetrazine derivatives, namely 3,6-dihydrazino-1,2,4,5-tetrazine (DHDTZ) and 1,2,4,5-tetrazine dicarboxylic acid (DCTZ), and determine their antibacterial, antioxidant and anticorrosion characteristics as additives in a sol-gel coating on SS316L steel. The structure of the tetrazines was confirmed by NMR and FTIR while the surface morphology of bacterial cells in their presence was observed by AFM. Their ability to inhibit corrosion on …