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Articles 1 - 12 of 12
Full-Text Articles in Engineering
Effect Of Arc Plasma Sintering On The Structural And Microstructural Properties Of Fe-Cr-Ni Austenitic Stainless Steels, Parikin Parikin, M. Dani, A. Dimyati, N. D. Purnamasari, B. Sugeng, M. Panitra, A. Insani, T. H. Priyanto, S. Mustofa, Syahbuddin Syahbuddin, A. Huang
Effect Of Arc Plasma Sintering On The Structural And Microstructural Properties Of Fe-Cr-Ni Austenitic Stainless Steels, Parikin Parikin, M. Dani, A. Dimyati, N. D. Purnamasari, B. Sugeng, M. Panitra, A. Insani, T. H. Priyanto, S. Mustofa, Syahbuddin Syahbuddin, A. Huang
Makara Journal of Technology
X-ray diffraction techniques were performed to determine the actual crystal structure of A2 austenitic stainless steel (ASS) as-cast and A2 ASS after arc plasma sintering (APS) for 2 s. Computations were conducted on the basis of the Bragg arithmetic formula by comparing the S2 arithmetic with the interplanar spacing. The Bragg arithmetic formula is a simple series for the determination of the crystalline phase of materials based on the Miller indices of cubic shapes or other shapes. A2 ASS as-cast was identified to have a crystal structure of face-centered cubic with lattice parameter a = 3.58 Å. A similar crystal …
Raman Spectrum Characteristic And Structural Evolution Of High Rank Coalscryptocrystalline Graphite, Li Huantong, Wang Nan, Zhu Zhirong, Fan Jingjing, Zhang Weiguo
Raman Spectrum Characteristic And Structural Evolution Of High Rank Coalscryptocrystalline Graphite, Li Huantong, Wang Nan, Zhu Zhirong, Fan Jingjing, Zhang Weiguo
Coal Geology & Exploration
Raman spectroscopy can reflect the order degree and structural defects of carbon materials, and can be used to characterize the structural changes during the evolution of high rank coal-cryptocrystalline graphite, and analyze the relationship between Raman parameters of coal with different deformation and metamorphic degrees and the spacing of surface network(d002). The results showed that: (1) there was stepped variation between the G peak position and d002, but the graphite and high rank coal could be distinguished well. The S2 peak, the full width at half maximum of D1 and G had a good linear relationship with d002; (2) the …
Investigation On Structural Evolution And Thermal Reaction Of Coal-Based Graphite From Xinhua County, Hunan Province, Li Kuo, Liu Qinfu, Song Botao, Zhang Shuai, Wu Yingke
Investigation On Structural Evolution And Thermal Reaction Of Coal-Based Graphite From Xinhua County, Hunan Province, Li Kuo, Liu Qinfu, Song Botao, Zhang Shuai, Wu Yingke
Coal Geology & Exploration
To investigate the structural evolution and thermal reaction of coal-based graphite with different graphitization,the anthracite and coal-based graphite from Xinhua County, Hunan were analyzed by X-ray diffraction (XRD), high resolution transformation electron microscope(HRTEM), and temperature programmed oxidation (TPO). The results show that carbon structure transformed from the amorphous anthracite to three dimensionally ordered graphite as graphitization degree increases. The coal-based graphite samples with different graphitization degree are composed of multi carbon phases, suggesting a heterogeneous nature of coal-based graphite, and ordered carbon phases were common in higher rank samples, however, defects can still be detected in most metamorphosed coal-based graphite. …
Structural And Photoluminescence Properties Of Zno Thin Films Deposited By Ultrasonic Spray Pyrolysis, Iwan Sugihartono, Erfan Handoko, Vivi Fauzia, Artoto Arkundato, Lara Permata Sari
Structural And Photoluminescence Properties Of Zno Thin Films Deposited By Ultrasonic Spray Pyrolysis, Iwan Sugihartono, Erfan Handoko, Vivi Fauzia, Artoto Arkundato, Lara Permata Sari
Makara Journal of Technology
Zinc oxide (ZnO) thin films on a silicon (Si) (111) substrate were grown herein using ultrasonic spray pyrolysis at 450 °C with different Zn concentrations. The ZnO thin films had X-ray diffraction patterns of a polycrystalline hexagonal wurtzite structure. The (002) and (101) peak intensities changed under different Zn concentrations. Furthermore, according to Scherer's and Stokes–Wilson equations, the crystallite size and the internal strain of the ZnO thin films in the (002) and (101) peaks changed with the Zn concentration. Optically, the photoluminescence spectra indicated that the ratio of the UV/GB emission of the ZnO thin films was the highest …
Characterization Of Surface Active Shell Charcoal Nyamplung Seeds (Calophyllum Inophyllum Linn), Santiyo Wibowo, Wasrin Syafi, Gustan Pari
Characterization Of Surface Active Shell Charcoal Nyamplung Seeds (Calophyllum Inophyllum Linn), Santiyo Wibowo, Wasrin Syafi, Gustan Pari
Makara Journal of Technology
Characterization of Surface Active Shell Charcoal Nyamplung Seeds (Calophyllum inophyllum Linn). Chemical and physical activation of nyamplung shell with 0%, 5%, and 10% H3PO4 for 60 and 120 minutes has been carried out to prepare activated charcoal. The purpose of this experiment was to look into the characteristic of nyamplung shell activated charcoal surface. Nyamplung shell was carbonized into charcoal, then activated by immersion in H3PO4 solution using 0%, 5% and 10%, for 24 hours, and heated in retort at two temperatures (700 and 800 oC) and two duration (60 and 120 minutes). The material were characterized by fourier transform …
Development Of Layered Zn-Fe Coatings For Better Corrosion Protection, R S. Bhat, R Udupak, A C. Hegde
Development Of Layered Zn-Fe Coatings For Better Corrosion Protection, R S. Bhat, R Udupak, A C. Hegde
Journal of Metals, Materials and Minerals
In this research, the Zn-Fe coating having successive layers of alloys of two different compositions were developed alternatively on mild steel for better corrosion protection. The multilayer coatings, or alternatively, composition modulated alloy (CMA) coatings of different configurations have been developed, and their corrosion behaviors were evaluated by electrochemical DC and AC methods. The cyclic cathode current densities and numbers of layers have been optimised for peak corrosion stability of the coatings. Under optimal condition, the CMA coating having 300 layers, having about 67 nm average thickness was found to be approximately six times higher corrosion resistant than monolayer coating …
Separation Study Of Titanomagnetite Fe3-Xtixo4 From Natural Sand At Indramayu, West Java, Sunaryo Sunaryo, Iwan Sugihartono
Separation Study Of Titanomagnetite Fe3-Xtixo4 From Natural Sand At Indramayu, West Java, Sunaryo Sunaryo, Iwan Sugihartono
Makara Journal of Technology
Separation Study of Titanomagnetite Fe3-xTixO4 from Natural Sand at Indramayu, West Java. Titanomagnetite FeTiO4 has been obtained from metal sand which is separated from natural sand at Indramayu using magnetic separator with the magnetic field 0,3 Tesla. This method can improve titanomagnetite content from 32% to 63,6%. According to X-ray diffractometer (XRD) and data processing by general structure analyses system (GSAS) with χ2= 1,454 and Wrp = 0,1142 as correction factor of the peak to peak intensities, we conclude that χ2 about 0 and Wrp aproximately 10%. It indicates the datas with the error merely 0,1 can be accepted. Furthermore, …
An Investigation Of Microstructural Change Of Low Alloy Steel Aisi 4150 By Seebeck Coefficient, T Samran, P Termsuksawad
An Investigation Of Microstructural Change Of Low Alloy Steel Aisi 4150 By Seebeck Coefficient, T Samran, P Termsuksawad
Journal of Metals, Materials and Minerals
Low alloyed steels, whose hardness can be modified by heat treatment, have been widely used in various applications. After heat treatment, they are normally destructively characterized and tested by many approaches via optical microscope and hardness testing. It is useful to develop a non-destructive method relating to its properties and microstructures. The proposed non-destructive approach in this study is the Seebeck coefficient measurement. The materials in this study were carbon steels AISI 4150 rod with a diameter of 1.3 cm and length of 3 cm. The specimens were heat-treated at 900ºC for 1 hour and were then cooled to room …
Composite Electroplating And Characterizations Of Sn-Sba15 Anode For Lithium-Ion Batteries, Xiao-Yong Fan, Jin-Mei Xu, Quan-Chao Zhuang, Hong-Hong Jiang, Ling Huang, Yan-Xia Jiang, Quan-Feng Dong, Shi-Gang Sun
Composite Electroplating And Characterizations Of Sn-Sba15 Anode For Lithium-Ion Batteries, Xiao-Yong Fan, Jin-Mei Xu, Quan-Chao Zhuang, Hong-Hong Jiang, Ling Huang, Yan-Xia Jiang, Quan-Feng Dong, Shi-Gang Sun
Journal of Electrochemistry
Sn-SBA15 anode was prepared by composite electroplating.The first discharge and charge capacity was 1075mAh/g and 630mAh/g respectively.After fifty charge/discharge cycles,the charge and discharge capacity of Sn-SBA15 were retained above 400mAh/g.XRD patterns indicated that the Sn-SBA15 has tetragonal crystal type.SEM images showed that the Sn-SBA15 had a honeycombed surface.EIS results indicated that there was SEI film formed on the surface of Sn-SBA15 electrode.
Integration Of Nickel Monosilicide (Nisi) Into An Rit Smfl Nmos Device, Phu Do
Integration Of Nickel Monosilicide (Nisi) Into An Rit Smfl Nmos Device, Phu Do
Journal of the Microelectronic Engineering Conference
A nickel silicidation process has been developed for the Semiconductor & Microsystems Fabrication Laboratory (SM FL) at Rochester Institute of Technology (RIT). NISI and Ni2Si were obtained in doped source/drain and polysilicon gate regions respectively at rapid thermal annealing (RTA) condition of 500°C for 60 seconds. The sheet resistance of nickel silicide in both regions was measured to be 0.45Ω/o — 0.5Ω/o. Nickel silicide was also integrated into an RIT NMOSFET process where silicide was formed over the S/D and polysilicon gate regions. Rutherford Backscatter and x-ray diffraction data showed the formation of NiSi phase in the S/D …
Characterization And Electrochemical Investigation Of Boron-Doped Mesocarbon Microbeads Anode Materials For Lithium-Ion Battery, Mao-Hui Chen, Guo-Tao Wu, Guang-Ming Zhu, Jin-Kua You, Zu-Geng Lin
Characterization And Electrochemical Investigation Of Boron-Doped Mesocarbon Microbeads Anode Materials For Lithium-Ion Battery, Mao-Hui Chen, Guo-Tao Wu, Guang-Ming Zhu, Jin-Kua You, Zu-Geng Lin
Journal of Electrochemistry
The anodic performances of boron doped and undoped mesocarbon microbeads(MCMBs) were comparatively studied and the structures were characterized by XPS,SEM,XRD and electrochemical measurements. It was found that boron doping samples greatly increased the degree of graphitization and the crystallite size,leading to quite different morphology. Electrochemical discharge/charge cycle tests indicate that lithium intercalation occurred at a little higher potential for the boron doped MCMBs, being attended by greater irreversible capacity loss.
Microstructure And Electrochemical Properties Of The Melt_Spinning Zr_(0.9)Ti_(0.1) (Ni,Co,Mn,V)_(2.1) Alloy, Ming-Fen Wen, Yu-Chun Zhai, Lian Chen, Min Tong, Hua Zhen, Rong-Jun Ma
Microstructure And Electrochemical Properties Of The Melt_Spinning Zr_(0.9)Ti_(0.1) (Ni,Co,Mn,V)_(2.1) Alloy, Ming-Fen Wen, Yu-Chun Zhai, Lian Chen, Min Tong, Hua Zhen, Rong-Jun Ma
Journal of Electrochemistry
The microstructure and electrochemical properties of Zr 0.9 Ti 0.1 (Ni,Co,Mn,V) 2.1 alloys prepared by both the melt_spinning method and the conventional induction melting were investigated. XRD studies show that Zr 0.9 Ti 0.1 (Ni,Co,Mn,V) 2.1 alloys at as_cast,melt_spinning and annealing are all face center cubic structure with C15 laves phase,the higher the melt_spinning rate,the more the amorphous content.The electrochemical measurements show that melt_spinning alloys have better active behavior,low discharge capacity(<280 mAh/g); but after annealed,the alloys are activated completely with 30 cycles, the capacities about 340 mAh/g are higher than those of as_cast and melt_spinning alloys;the annealec alloys have a better cycle stability than that of as_cast alloy, and the higher the melt_spinning rate is, the more stable the alloy becomes; at 300 mAh/g current density,the capacity of annealed 40 m/s alloy is up to 85% of the maximum capacity after 800 cycles, the capacity decay rate is about 6.9%.