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2024

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Full-Text Articles in Engineering

Enhancing Electrical Network Vulnerability Assessment With Machine Learning And Deep Learning Techniques, M Mishkatur Rahman, Ayman Akash, Harun Pirim, Chau Le, Trung Le, Om Prakash Yadav May 2024

Enhancing Electrical Network Vulnerability Assessment With Machine Learning And Deep Learning Techniques, M Mishkatur Rahman, Ayman Akash, Harun Pirim, Chau Le, Trung Le, Om Prakash Yadav

Northeast Journal of Complex Systems (NEJCS)

This research utilizes advanced machine learning techniques to evaluate node vul-
nerability in power grid networks. Utilizing the SciGRID and GridKit datasets, con-
sisting of 479, 16,167 nodes and 765, 20,539 edges respectively, the study employs
K-nearest neighbor and median imputation methods to address missing data. Cen-
trality metrics are integrated into a single comprehensive score for assessing node
criticality, categorizing nodes into four centrality levels informative of vulnerability.
This categorization informs the use of traditional machine learning (including XG-
Boost, SVM, Multilayer Perceptron) and Graph Neural Networks in the analysis.
The study not only benchmarks the capabilities of these …

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Fitness For Service (Ffs) And Fatigue Assessment For Shell Distorted Steel Storage Tank Based On Api 579-1/Asme Ffs-1, Wira Herucakra Sr. Structure Engineer, Luh Putri Adyani, Ic Farid Hadi Prasetyo, Alviani Rahma Rizkhita May 2024

Fitness For Service (Ffs) And Fatigue Assessment For Shell Distorted Steel Storage Tank Based On Api 579-1/Asme Ffs-1, Wira Herucakra Sr. Structure Engineer, Luh Putri Adyani, Ic Farid Hadi Prasetyo, Alviani Rahma Rizkhita

Journal of Materials Exploration and Findings

A shell distortion was occurred due to incorrect in the welding procedure during construction of a new built above ground steel storage tank. The assessment level 1 then performed referred to original construction code of API Standard 650 was performed, the roundness data of tank plate was obtained through to laser scanning survey, and the result on assessment level 1 known that the minimum radius of measured point is exceeding the radius tolerance. This unacceptable condition of assessment level 1 requires to be performed the higher level of assessment. A fitness for service assessment level 3 for tank 1000 KL …

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Development Of 485 Mpa Class High Strength Low Alloy Steel For Power Plant Infrastructures, Agung Baskoro, Rini Riastuti May 2024

Development Of 485 Mpa Class High Strength Low Alloy Steel For Power Plant Infrastructures, Agung Baskoro, Rini Riastuti

Journal of Materials Exploration and Findings

Currently, Indonesia is progressing to build 35,000 MW of power plants, which will increase the demand for materials, especially steel. One of these power plants is fossil fuel-based, which generates not only electricity but also flue gas containing sulfur that may cause corrosion to power plant infrastructure such as chimney or boiler areas. In addition, apart from being resistant to corrosion in sulfuric and hydrochloric acid conditions, the steel used in power plant infrastructure must also have good strength, toughness, and weldability. Therefore, the present paper describes about steel development for power plant applications that has not only corrosion resistance …

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Effects Of Ti Addition On The Characteristics Of Al-10zn-6mg-2si/Zro2 Composites Produced By Squeeze Casting, Qesha Diva Prameshvara, Pipin Indah Lestari, Bondan Tiara Sofyan May 2024

Effects Of Ti Addition On The Characteristics Of Al-10zn-6mg-2si/Zro2 Composites Produced By Squeeze Casting, Qesha Diva Prameshvara, Pipin Indah Lestari, Bondan Tiara Sofyan

Journal of Materials Exploration and Findings

Metal matrix composite (MMC) with 7xxx aluminum matrix is potential for ballistic applications due to the combination of strength, toughness, and light weight. Previous study successfully produced aluminum-based composites with SiC particles which were able to stop type III bullet, however cracks remained on back of the plate. Therefore, in this research, SiC was replaced by zirconia (ZrO2) due to its high fracture toughness. Ti-B grain refiner was added to further improve toughness through grain boundary strengthening mechanism. This research developed 5 vol.% ZrO2 strengthened Al-10Zn-6Mg-2Si composite with addition of Al-5Ti-1B grain refiner produced through squeeze casting …

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Integration Of The Ashby Technique And Pahl-Beitz Quantitative Ranking For Railway Axle Material Selection, Helya Chafshoh Nafisah, Jaka Fajar Fatriansyah, Siti Norasmah Surip May 2024

Integration Of The Ashby Technique And Pahl-Beitz Quantitative Ranking For Railway Axle Material Selection, Helya Chafshoh Nafisah, Jaka Fajar Fatriansyah, Siti Norasmah Surip

Journal of Materials Exploration and Findings

Railway axle serves as a vital connection between the train's wheels and its body. However, cyclic loading and high speed can induce fatigue in railway axle, which potentially leads to damage human safety. Therefore, it is important to find materials that have good mechanical properties with the lowest weight and cost. In this paper, a comprehensive method using Ashby chart has been performed to select candidate materials of railway axle. The methods begin with analyzing function by determining the problem, objective function, and constraints. After that, the results obtained are ranked using Pahl and Beitz quantitative weighting method. The results …

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Study On Human Integrity Management System Maturity Level For Supporting Asset Integrity And Process Safety Implementation, Anggiat M. Sihotang, Dedi Priadi, Datu Rizal Asral May 2024

Study On Human Integrity Management System Maturity Level For Supporting Asset Integrity And Process Safety Implementation, Anggiat M. Sihotang, Dedi Priadi, Datu Rizal Asral

Journal of Materials Exploration and Findings

The human factors (HF) are recognized as one of critical process safety barriers involved in normal and abnormal conditions in the oil and gas industry. In order to strengthen the HF roles as barriers we need to ensure that the actions generated are based on a valid risk assessment of the operation to be addressed by a relevant human factor analysis. Organizations within the oil and gas process have made much progress in understanding and implementing HF improvement programs. However, organizations are not always clear about what are their current situations in managing HF, their priorities for HF to be …

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Analysis Of The Effect Of Different Surface Preparation Methods On Corrosion Resistance And Adhesion Strength Of Astm A36 Steel Substrate With Surface Tolerant Epoxy Paint As Coating Material, Irwan Wijaya Santoso, Daffa Aqila, Rini Riastuti, Rizal Tresna Ramadhani May 2024

Analysis Of The Effect Of Different Surface Preparation Methods On Corrosion Resistance And Adhesion Strength Of Astm A36 Steel Substrate With Surface Tolerant Epoxy Paint As Coating Material, Irwan Wijaya Santoso, Daffa Aqila, Rini Riastuti, Rizal Tresna Ramadhani

Journal of Materials Exploration and Findings

In the industrial world, to extend the service life of materials, protection methods are carried out to slow down the material's corrosion rate. The protection method that is often used is the coating method. The coating method is a protection method by coating the substrate material using a coating material to prevent contact between the substrate material and the environment. In this research, the substrate material used is ASTM A36 steel and the coating material used is Surface Tolerant Epoxy paint. The independent variable used in this study lies in the surface preparation method which consists of: solvent cleaning, hand …

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Effect Of Recommending Users And Opinions On The Network Connectivity And Idea Generation Process, Sriniwas Pandey, Hiroki Sayama May 2024

Effect Of Recommending Users And Opinions On The Network Connectivity And Idea Generation Process, Sriniwas Pandey, Hiroki Sayama

Northeast Journal of Complex Systems (NEJCS)

The growing reliance on online services underscores the crucial role of recommendation systems, especially on social media platforms seeking increased user engagement. This study investigates how recommendation systems influence the impact of personal behavioral traits on social network dynamics. It explores the interplay between homophily, users’ openness to novel ideas, and recommendation-driven exposure to new opinions. Additionally, the research examines the impact of recommendation systems on the diversity of newly generated ideas, shedding light on the challenges and opportunities in designing effective systems that balance the exploration of new ideas with the risk of reinforcing biases or filtering valuable, unconventional …

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Bibliometric Review Of The Landscape And Thematic Structure Of Research On Sustainable Mining In Asean, 1942–2022, Nathatai Janjirawatna, Sirisuhk Rakthin, Philip Hallinger May 2024

Bibliometric Review Of The Landscape And Thematic Structure Of Research On Sustainable Mining In Asean, 1942–2022, Nathatai Janjirawatna, Sirisuhk Rakthin, Philip Hallinger

Journal of Sustainable Mining

This bibliometric review addressed the lack of consolidated information on the current state of sustainable mining in the ASEAN region. The review analyzed bibliographic data associated with 539 Scopus-indexed documents on sustainable mining in ASEAN nations published through the end of 2022. Descriptive statistics identified a great disparity in the scope of research on sustainable mining practices across the ASEAN countries. Surprisingly, a significant portion of the extant research on sustainable mining in the region has been authored by scholars from outside of ASEAN. Keyword analyses highlighted several emerging research topics including life cycle assessment, conservation of natural resources, climate …

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An Overview Of How To Measure The Kinetic Properties Of An Anode Material For The Chlorine Evolution Reaction, Cameron Vann May 2024

An Overview Of How To Measure The Kinetic Properties Of An Anode Material For The Chlorine Evolution Reaction, Cameron Vann

Reviews, Analyses, and Instructional Studies in Electrochemistry (RAISE)

The process of generating chlorine gas using electrolysis in aqueous systems is well established. However, a new process requires chlorine to be generated at high temperatures using molten salt. This harsh environment requires a new study of anode materials for the chlorine evolution reaction. Anode materials can be compared by their kinetic parameters, the transfer coefficient α and the exchange current i0. The basic theory of these properties as they relate to the chlorine evolution reaction has been detailed and an analysis method for finding these effective parameters has been shown and demonstrated.

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Model Of The Effect Of Voltage On Contact Angle In An Electrolytic Cell Reaction, Aaron Essilfie May 2024

Model Of The Effect Of Voltage On Contact Angle In An Electrolytic Cell Reaction, Aaron Essilfie

Reviews, Analyses, and Instructional Studies in Electrochemistry (RAISE)

This paper investigates the hypothesis that the contact angle at the meniscus of an electrode-electrolyte can be altered during a redox reaction through the coupled understanding of electrowetting and capillarity rise. Recent studies in electrowetting have focused on dielectric surfaces but research on contact angle at the electrode-electrolyte surface is lacking. The study employs a basic electrolytic cell. By applying principles of electrowetting and capillary rise the research aims to understand the relationship between applied voltage and contact angle, to advancements in electrochemistry and microfluidics.

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Review Of Cyclic Voltammetry Measurements For Uranium In Flinak Molten Salt, Jackson Ivory May 2024

Review Of Cyclic Voltammetry Measurements For Uranium In Flinak Molten Salt, Jackson Ivory

Reviews, Analyses, and Instructional Studies in Electrochemistry (RAISE)

The electrochemical behavior of uranium FLiNaK molten salts is explored, focusing on cyclic voltammetry (CV) as a powerful tool for redox characterization and diffusion studies. Through a comprehensive review of recent research, the study highlights the significance of CV in understanding electrode kinetics, material compatibility, and process optimization in molten salt environments. The findings underscore the potential of FLiNaK molten salt reactors in advancing nuclear energy technologies, fuel processing, and waste management strategies. Collaborative interdisciplinary efforts are emphasized to address challenges and accelerate innovation in electrochemical methods for nuclear applications.

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Model To Demonstrate Effects Of Mass Transfer And Applied Current In An Electrolytic Cell, George Ankrah May 2024

Model To Demonstrate Effects Of Mass Transfer And Applied Current In An Electrolytic Cell, George Ankrah

Reviews, Analyses, and Instructional Studies in Electrochemistry (RAISE)

This study investigates the relationship between applied current and resulting cell potential in an electrolytic system, considering the transport of electroactive species. By applying Michael Faraday's laws of electrolysis and the Nernst-Planck equation, the behavior of electroactive species in diffusion-controlled systems with and without stirring is modeled. The plots demonstrate how stirring enhances ion transport and establishes a stable Nernst diffusion layer, affecting the kinetics of electrochemical reactions. Understanding these dynamics is crucial for optimizing electrolysis processes.

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Ionic Conductivity, Li+ Transference Number, And Diffusion Coefficient Of A Solid-State Electrolyte Composite, Lizbeth Zurita May 2024

Ionic Conductivity, Li+ Transference Number, And Diffusion Coefficient Of A Solid-State Electrolyte Composite, Lizbeth Zurita

Reviews, Analyses, and Instructional Studies in Electrochemistry (RAISE)

The design of solid-state electrolyte (SSE) composites involves the fundamental study of transport properties, such as ionic conductivity. This transport property is influenced by the transport mechanisms of the charge species inside the composite, such as diffusion and migration. In this work, we perform the measurement of these three parameters through defined techniques. The resulting parameters were: ionic conductivity, the diffusion coefficient, and the Li+ transference number.

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Improving Ethics Surrounding Collegiate-Level Hacking Education: Recommended Implementation Plan & Affiliation With Peer-Led Initiatives, Shannon Morgan, Dr. Sanjay Goel May 2024

Improving Ethics Surrounding Collegiate-Level Hacking Education: Recommended Implementation Plan & Affiliation With Peer-Led Initiatives, Shannon Morgan, Dr. Sanjay Goel

Military Cyber Affairs

Cybersecurity has become a pertinent concern, as novel technological innovations create opportunities for threat actors to exfiltrate sensitive data. To meet the demand for professionals in the workforce, universities have ramped up their academic offerings to provide a broad range of cyber-related programs (e.g., cybersecurity, informatics, information technology, digital forensics, computer science, & engineering). As the tactics, techniques, and procedures (TTPs) of hackers evolve, the knowledge and skillset required to be an effective cybersecurity professional have escalated accordingly. Therefore, it is critical to train cyber students both technically and theoretically to actively combat cyber criminals and protect the confidentiality, integrity, …

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Using Digital Twins To Protect Biomanufacturing From Cyberattacks, Brenden Fraser-Hevlin, Alec W. Schuler, B. Arda Gozen, Bernard J. Van Wie May 2024

Using Digital Twins To Protect Biomanufacturing From Cyberattacks, Brenden Fraser-Hevlin, Alec W. Schuler, B. Arda Gozen, Bernard J. Van Wie

Military Cyber Affairs

Understanding of the intersection of cyber vulnerabilities and bioprocess regulation is critical with the rise of artificial intelligence and machine learning in manufacturing. We detail a case study in which we model cyberattacks on network-mediated signals from a novel bioreactor, where it is important to control medium feed rates to maintain cell proliferation. We use a digital twin counterpart reactor to compare glucose and oxygen sensor signals from the bioreactor to predictions from a kinetic growth model, allowing discernment of faulty sensors from hacked signals. Our results demonstrate a successful biomanufacturing cyberattack detection system based on fundamental process control principles.

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Characterizing Advanced Persistent Threats Through The Lens Of Cyber Attack Flows, Logan Zeien, Caleb Chang, Ltc Ekzhin Ear, Dr. Shouhuai Xu May 2024

Characterizing Advanced Persistent Threats Through The Lens Of Cyber Attack Flows, Logan Zeien, Caleb Chang, Ltc Ekzhin Ear, Dr. Shouhuai Xu

Military Cyber Affairs

Effective cyber defense must build upon a deep understanding of real-world cyberattacks to guide the design and deployment of appropriate defensive measures against current and future attacks. In this abridged paper (of which the full paper is available online), we present important concepts for understanding Advanced Persistent Threats (APTs), our methodology to characterize APTs through the lens of attack flows, and a detailed case study of APT28 that demonstrates our method’s viability to draw useful insights. This paper makes three technical contributions. First, we propose a novel method of constructing attack flows to describe APTs. This abstraction allows technical audiences, …

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Generative Machine Learning For Cyber Security, James Halvorsen, Dr. Assefaw Gebremedhin May 2024

Generative Machine Learning For Cyber Security, James Halvorsen, Dr. Assefaw Gebremedhin

Military Cyber Affairs

Automated approaches to cyber security based on machine learning will be necessary to combat the next generation of cyber-attacks. Current machine learning tools, however, are difficult to develop and deploy due to issues such as data availability and high false positive rates. Generative models can help solve data-related issues by creating high quality synthetic data for training and testing. Furthermore, some generative architectures are multipurpose, and when used for tasks such as intrusion detection, can outperform existing classifier models. This paper demonstrates how the future of cyber security stands to benefit from continued research on generative models.

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Machine Learning Security For Tactical Operations, Dr. Denaria Fields, Shakiya A. Friend, Andrew Hermansen, Dr. Tugba Erpek, Dr. Yalin E. Sagduyu May 2024

Machine Learning Security For Tactical Operations, Dr. Denaria Fields, Shakiya A. Friend, Andrew Hermansen, Dr. Tugba Erpek, Dr. Yalin E. Sagduyu

Military Cyber Affairs

Deep learning finds rich applications in the tactical domain by learning from diverse data sources and performing difficult tasks to support mission-critical applications. However, deep learning models are susceptible to various attacks and exploits. In this paper, we first discuss application areas of deep learning in the tactical domain. Next, we present adversarial machine learning as an emerging attack vector and discuss the impact of adversarial attacks on the deep learning performance. Finally, we discuss potential defense methods that can be applied against these attacks.

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Securing The Void: Assessing The Dynamic Threat Landscape Of Space, Brianna Bace, Dr. Unal Tatar May 2024

Securing The Void: Assessing The Dynamic Threat Landscape Of Space, Brianna Bace, Dr. Unal Tatar

Military Cyber Affairs

Outer space is a strategic and multifaceted domain that is a crossroads for political, military, and economic interests. From a defense perspective, the U.S. military and intelligence community rely heavily on satellite networks to meet national security objectives and execute military operations and intelligence gathering. This paper examines the evolving threat landscape of the space sector, encompassing natural and man-made perils, emphasizing the rise of cyber threats and the complexity introduced by dual-use technology and commercialization. It also explores the implications for security and resilience, advocating for collaborative efforts among international organizations, governments, and industry to safeguard the space sector.

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Commercial Enablers Of China’S Cyber-Intelligence And Information Operations, Ethan Mansour, Victor Mukora May 2024

Commercial Enablers Of China’S Cyber-Intelligence And Information Operations, Ethan Mansour, Victor Mukora

Military Cyber Affairs

In a globally commercialized information environment, China uses evolving commercial enabler networks to position and project its goals. They do this through cyber, intelligence, and information operations. This paper breaks down the types of commercial enablers and how they are used operationally. It will also address the CCP's strategy to gather and influence foreign and domestic populations throughout cyberspace. Finally, we conclude with recommendations for mitigating the influence of PRC commercial enablers.

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Using Chatgpt With Novice Arduino Programmers: Effects On Performance, Interest, Self-Efficacy, And Programming Ability, Donald M. Johnson, Will Doss, Christopher M. Estepp May 2024

Using Chatgpt With Novice Arduino Programmers: Effects On Performance, Interest, Self-Efficacy, And Programming Ability, Donald M. Johnson, Will Doss, Christopher M. Estepp

Journal of Research in Technical Careers

A posttest-only control group experimental design compared novice Arduino programmers who developed their own programs (self-programming group, n =17) with novice Arduino programmers who used ChatGPT 3.5 to write their programs (ChatGPT-programming group, n = 16) on the dependent variables of programming scores, interest in Arduino programming, Arduino programming self-efficacy, Arduino programming posttest scores, and types of programming errors. Students were undergraduates in an introductory agricultural systems technology course in Fall 2023. The results indicated no significant (p < .10) differences between groups for programming rubric scores (p = .50) or interest in Arduino programming (p = .50). There were significant differences for Arduino programming self-efficacy, (p = .03, Cohen’s d = 0.75) and Arduino posttest scores, (p = .03, Cohen’s d = 0.76); students in the self-programming group scored significantly higher on both measures. Analysis of students’ errors indicated the ChatGPT group made significantly (p < .01) more program punctuation errors. These results indicated novice students writing their own programs developed greater Arduino programming self-efficacy and programming ability than novice students using ChatGPT. Nevertheless, ChatGPT may still play an important role in assisting novices to write microcontroller programs.

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Synthesis Of Acetylene Diols With The Participation Of The Bu4noh/Dmso/H2o Catalytic Systems, Muyassar K. Salieva, Odiljon E. Ziyadullayev, Guzal K. Otamukhamedova, Rifkat F. Talipov, Lochin K. Ablakulov May 2024

Synthesis Of Acetylene Diols With The Participation Of The Bu4noh/Dmso/H2o Catalytic Systems, Muyassar K. Salieva, Odiljon E. Ziyadullayev, Guzal K. Otamukhamedova, Rifkat F. Talipov, Lochin K. Ablakulov

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this work in this study, acetylene alcohols containing heteroatomic substituents in their molecular composition- 2-(-thiophen-2-yl)but-3-yn-2-ol, 2-(3-methylthiophen-2-yl)but-3-yn-2-ol, 2-(furan-2-yl)but-3yn-2-ol, 2-(pyridin-4-yl)but-3-yn-2-ol, 2-(5-chlorothiophen-2-yl)but-3-yn-2-ol, 2-(5-bromothiophen-2yl)but-3-yn-2-ol acetylene diols were synthesized based on the reaction with acetone in a dimethyl sulfoxide solvent in the presence of the Bu4NOH/DMSO/H2O catalytic system. The influence of the molar ratio of starting materials, reaction duration, temperature, nature of the catalyst and solvents on the product yield was systematically studied. The composition, purity and structure of the new generation of synthesized acetylenediols have been confirmed by modern physicochemical methods. The mechanism of the reaction process …

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Synthesis Of High Molecular Mass Resins Based On Furfuryl Alcohol, Boysayid U. Sayidov, Latif E. Jumanov, Muzaffar G. Alimukhamedov, Sherali A. Umarov, Farhod A. Magrupov May 2024

Synthesis Of High Molecular Mass Resins Based On Furfuryl Alcohol, Boysayid U. Sayidov, Latif E. Jumanov, Muzaffar G. Alimukhamedov, Sherali A. Umarov, Farhod A. Magrupov

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of the work is to study the process of synthesis of furfuryl oligomers with high molecular weight at various ratios of furfuryl alcohol and hydroxyl-containing polyether polyol. The influence of the process method on the yield of high-molecular furfuryl oligomer is shown - with a one-step synthesis method with an increase in the amount of furfuryl alcohol from 20 to 50 moles per 1 mole of polyether polyol, the yield of the final product decreases from 75% to 56%, apparently due to high exothermic effects, causing gelation systems. In contrast to the one-time introduction of the catalyst, its …

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Synthesis And Technology Of Vinyl Esters Of Aromatic Carboxylic Acids Based On Vinyl Acetate, Askar B. Parmanov, Suvonkul E. Nurmanov, Saida S. Abdurakhmanova, Sarvinoz I. Tirkasheva, Begzod F. Adashev May 2024

Synthesis And Technology Of Vinyl Esters Of Aromatic Carboxylic Acids Based On Vinyl Acetate, Askar B. Parmanov, Suvonkul E. Nurmanov, Saida S. Abdurakhmanova, Sarvinoz I. Tirkasheva, Begzod F. Adashev

CHEMISTRY AND CHEMICAL ENGINEERING

In this work the vinylation reactions of aromatic carboxylic acids with vinyl acetate, which contain various substituents, in the presence of 2-chloro-4,6-dimethoxy-1,3,5-triazine were studied for the first time. The influence of the nature of the starting materials, temperature, reaction duration, solvent and reagents - zinc triflate (Zn(OTf)2, 3,3-diphenylbinaphthol (3,3'-Ph2BINOL-2Li), tertiary potassium butylate (KOtrBu), butyllithium (BuLi) for the synthesis of vinyl esters. The synthesis of vinyl esters of aromatic carboxylic acids was carried out: benzoiс, 2-phenylacetic, 4-methylbenzoic, 4-methoxybenzoic, 3,4-dimethoxybenzoic, 2-brombenzoic, 4-brombenzoic, 4-fluorobenzoic, 3-nitrobenzoic, 4-nitrobenzoic, 4-tertiary butylbenzoic, 2-chlorobenzoic, 4-chlorobenzoic, 3-hydroxybenzoic and 4-hydroxybenzoic acids has been studied. …

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Synthesis Of Internal Acetylene Alcohols Based On The Sonogashira Reaction Of Terminal Acetylene Alcohols And Benzolchloride, Guzal K. Otamukhamedova, Odiljon E. Ziyadullayev, Abduvahob Ikramov, Sarvinoz I. Tirkasheva May 2024

Synthesis Of Internal Acetylene Alcohols Based On The Sonogashira Reaction Of Terminal Acetylene Alcohols And Benzolchloride, Guzal K. Otamukhamedova, Odiljon E. Ziyadullayev, Abduvahob Ikramov, Sarvinoz I. Tirkasheva

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of the study is to develop a new catalytic system for the synthesis of internal acetylene alcohols from the Sonogastric coupling reaction of terminal acetylene alcohols and benzolchloride. For the first time in this work, internal acetylene alcohols have been synthesized based on reactions of some terminal acetylene alcohols – 3,4-dimethylpentin-1-ol-3, 3,4,4-trimethylpentin-1-ol-3, 1-ethynylcyclohexanol-1, 2-ethynyladamantanol-2, 2-phenylbutin-3-ol-2, 2-(naphthyl-2)butyn-3-ol-2, 2-(furanyl-2)butyn-3-ol-2 and 2-(pyridinyl-4)butyn-3-ol-2 with chloridebenzene. In order to achieve high product productivity in the Sonogashira reaction, alternative conditions have been identified by studying the molar ratios, spatial structure, induction effects of substituents, solvent and catalyst nature, as well as temperature, reaction duration …

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Study Of The Influence Of B2o3 Oxide On The Physical And Technical Properties Of Ground Enamel Obtained Based On Local Raw Material Components, Shoxrux B. Naimov, Mastura Kh. Aripova May 2024

Study Of The Influence Of B2o3 Oxide On The Physical And Technical Properties Of Ground Enamel Obtained Based On Local Raw Material Components, Shoxrux B. Naimov, Mastura Kh. Aripova

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of the study was to obtain ground enamel based on local raw materials and to study the effect of boron oxide. The selection of local raw materials for producing ground enamel showed that the resulting glass compositions are in the SiO2–Al2O3–Na2O–K2O–CaO–B2O3 system. To adjust the properties, additives of nickel oxide and cobalt oxide were used. The properties of the developed compositions of primer enamels meet the requirements of GOST 24405-80. It has been determined that the addition of boron and an increase in its amount …

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Formation Of Luminescent Coatings With The Use Of Low Melting Glass, Eygeniy N. Poddenezhny, Ekaterina E. Trusova, Andrei A. Boiko, Ekaterina R. Kravcova, Olga V. Davydova May 2024

Formation Of Luminescent Coatings With The Use Of Low Melting Glass, Eygeniy N. Poddenezhny, Ekaterina E. Trusova, Andrei A. Boiko, Ekaterina R. Kravcova, Olga V. Davydova

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the present research is to develop compounds and technologies for applying the luminous vitrocrystalline compounds to smooth and ribbed glass substrates in LED lamp structure with a remote photoconverter that contains oxide low melting glass as the base and nanostructured cerium–doped yttrium–aluminum garnet powder as the luminophore. The luminescent coatings based on nanostructured cerium doped yttrium-aluminum garnet powder and low melting glass of composition BaO-Bi2O3-B2O3-K2O-SiO2 where prepared. YAG:Ce3+ powder was synthesized by the method of thermochemical reaction. Silica glass powder was introduced into the composition …

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Anomalous Of Resistance And Magnetic Susceptibility At 280-310 K And Ambient Pressure In Bismuth Cuprates Synthesized By Solar Energy, Dilbara Dj. Gulamova, Elyor B. Eshonkulov, Valeriya R. Li, Grigor I. Mamniashvili, Timur I. Gulamov May 2024

Anomalous Of Resistance And Magnetic Susceptibility At 280-310 K And Ambient Pressure In Bismuth Cuprates Synthesized By Solar Energy, Dilbara Dj. Gulamova, Elyor B. Eshonkulov, Valeriya R. Li, Grigor I. Mamniashvili, Timur I. Gulamov

CHEMISTRY AND CHEMICAL ENGINEERING

In order to obtain the full content of high-temperature superconducting phases using the “Super Fast Alloys Quenching” technology in the Large Solar Furnace (Parkent), precursors of bismuth cuprates of the series Bi1,7Pb0,3Sr2Ca(n-1)CunOy, n=3-30 were synthesized. Methods for study the properties of precursors are presented. The oriented nano-sized microstructure and layered structure of nanocrystalline nuclei are shown. The phase composition of the precursors at the beginning of the series (n=3-5) is represented by X-ray amorphous and crystalline phases. An increase in the content of CaO and CuO destabilizes the …

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Waste Utilization In Korean Cement Plants, Geun-Seong Lee, Zebo Abdullaevna Babakhanova, Mastura Khikmatovna Aripova May 2024

Waste Utilization In Korean Cement Plants, Geun-Seong Lee, Zebo Abdullaevna Babakhanova, Mastura Khikmatovna Aripova

CHEMISTRY AND CHEMICAL ENGINEERING

The kiln process in cement plant has the advantage of completely and effectively destroying and burning all organic substances due to high temperature and long residence time, oxygen atmosphere and excellent mixing effect, alkaline conditions of raw materials, and incorporation of trace metals into clinker, and plays a role as a pollutant emission barrier during waste utilization. Waste utilization technology is now proven and successful in cement plants. The waste utilization in Korean cement plants are greatly expanding in the view of energy and material recoveries, and economics as well as environmental preservation. Research on waste utilization in the Korean …

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