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Engineering Science and Materials

2016

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Quantifying Amorphous Content Of Commercially Available Silicon Carbide Fibers, Ian Mark Wolford Jan 2016

Quantifying Amorphous Content Of Commercially Available Silicon Carbide Fibers, Ian Mark Wolford

Browse all Theses and Dissertations

SiC/SiC ceramic matrix composites (CMCs) with potential applications at =2700°F (1482°C) are of significant interest to the Air Force. The high temperature performance of SiC fibers used within these composites is greatly affected by the presence of amorphous SiOC and free carbon in the fibers. Therefore quantification of this non SiC material in commercially available SiC fibers is extremely important. In this work Hi Nicalon, Hi-Nicalon Type-S, Tyranno-SA3, Cef-NITE, and Sylramic SiC fibers were studied. Changes in mass, grain size, and amorphous content were measured as a function of processing temperature and time. The amorphous material in each fiber was …