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Full-Text Articles in Engineering

Aerosol-Assisted Synthesis Of Monodisperse Single-Crystalline Α-Cristobalite Nanospheres, Xingmao Jiang, Lihong Bao, Yung-Sung Cheng, Darren R. Dunphy, Xiaodong Li, C. Jeffrey Brinker Dec 2011

Aerosol-Assisted Synthesis Of Monodisperse Single-Crystalline Α-Cristobalite Nanospheres, Xingmao Jiang, Lihong Bao, Yung-Sung Cheng, Darren R. Dunphy, Xiaodong Li, C. Jeffrey Brinker

Faculty Publications

Monodisperse single-crystalline α-cristobalite nanospheres have been synthesized by hydrocarbon-pyrolysis-induced carbon deposition on amorphous silica aerosol nanoparticles, devitrification of the coated silica at high temperature, and subsequent carbon removal by oxidation. The nanosphere size can be well controlled by tuning the size of the colloidal silica precursor. Uniform, high-purity nanocrystalline α-cristobalite is important for catalysis, nanocomposites, advanced polishing, and understanding silica nanotoxicology.


Synthesis, Structural, Optical And Mechanical Characterization Of Srb2O4 Nanorods, Rui Li, Lihong Bao, Xiaodong Li Oct 2011

Synthesis, Structural, Optical And Mechanical Characterization Of Srb2O4 Nanorods, Rui Li, Lihong Bao, Xiaodong Li

Faculty Publications

Single crystalline strontium borate (SrB2O4) nanorods were synthesized for the first time via a facile sol–gel route at low temperature. The SrB2O4 nanorods have a good crystalline nature with the growth direction along the [511] orientation and they are transparent from the ultraviolet to the visible regimes. Nanoscale three-point bending tests were performed directly on individual nanorods to probe their mechanical properties using an atomic force microscope. The elastic modulus of SrB2O4 nanorods was measured to be 158.2 ± 2.8 GPa, exhibiting a significant increase compared with other borate nanostructures …