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Full-Text Articles in Engineering

Graphene-Fibers Hybrid Structures As Adsorbents For Heavy Metal Ions In Aqueous Solutions, Dulce C. Capitanachi Dec 2019

Graphene-Fibers Hybrid Structures As Adsorbents For Heavy Metal Ions In Aqueous Solutions, Dulce C. Capitanachi

Theses and Dissertations

The project focuses on the study of graphene-fiber hybrid structures for adsorption of heavy metal ions in aqueous solutions. Polyvinyl alcohol-based graphene–fiber structures were created using centrifugal spinning and a carbonization process.

Characterization methods of the graphene–fiber hybrid structures (GFHS) include SEM, FTIR, TGA, and EDX. Single-step batch-type adsorption studies were performed to analyze the interaction of Cu (II) and Pb (II) ions onto GFHS surface. Different heavy metal ion concentrations were used, as well as a variation of pH values. Elemental analysis of the adsorbent’s surface after filtration experiments was studied by EDX and spectroscopy to verify the presence …


In Situ Chemical Probing Of Vacancy Defects In Graphene And Boron Nitride At Room Temperature, Ali Ihsan Altan May 2019

In Situ Chemical Probing Of Vacancy Defects In Graphene And Boron Nitride At Room Temperature, Ali Ihsan Altan

Theses and Dissertations

IN SITU CHEMICAL PROBING OF VACANCY DEFECTS IN GRAPHENE AND BORON NITRIDE AT ROOM TEMPERATURE

by

Ali Ihsan Altan

The University of Wisconsin-Milwaukee, 2019

Under the Supervision of Professor Jian Chen

Chemical vapor deposition (CVD) has emerged as the most promising technique towards manufacturing of large area, high quality graphene. Characterization, understanding, and controlling of various structural defects in CVD-grown graphene are essential to realize its true potential for real-world applications. We report a new method for in situ chemical probing of vacancy defects in CVD-grown graphene at room temperature. Our approach is based on a solid–gas phase reaction that …


In Situ Chemical Probing Of Vacancy Defects In Graphene And Boron Nitride At Room Temperature, Ali Ihsan Altan May 2019

In Situ Chemical Probing Of Vacancy Defects In Graphene And Boron Nitride At Room Temperature, Ali Ihsan Altan

Theses and Dissertations

IN SITU CHEMICAL PROBING OF VACANCY DEFECTS IN GRAPHENE AND BORON NITRIDE AT ROOM TEMPERATURE

by

Ali Ihsan Altan

The University of Wisconsin-Milwaukee, 2019

Under the Supervision of Professor Jian Chen

Chemical vapor deposition (CVD) has emerged as the most promising technique towards manufacturing of large area, high quality graphene. Characterization, understanding, and controlling of various structural defects in CVD-grown graphene are essential to realize its true potential for real-world applications. We report a new method for in situ chemical probing of vacancy defects in CVD-grown graphene at room temperature. Our approach is based on a solid–gas phase reaction that …