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Chemical Engineering

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Full-Text Articles in Engineering

Single-And Multi-Hole Baffles-A Heat Transfer And Fluid Flow Control For Hydrothermal Growth, Edward Evans, Hongmin Li, Guo-Xiang Wang Apr 2015

Single-And Multi-Hole Baffles-A Heat Transfer And Fluid Flow Control For Hydrothermal Growth, Edward Evans, Hongmin Li, Guo-Xiang Wang

Dr. Guo-Xiang Wang

Hydrothermal solution growth is an important technique to grow high-quality single crystals. An autoclave, a closed cylindrical low-carbon steel vessel, is used to grow the large size crystals. A baffle located at the median height divides an autoclave into two chambers. Previous numerical studies indicate that the buoyancy-driven flow within an autoclave is very sensitive to the temperatures on the wall established by the heating. Baffles are required to establish the conditions for growth of high quality single crystals. This paper presents a numerical study of the effects of various baffles on the fluid flow and temperature fields in an …


Natural Convection Flow Structures And Heat Transfer In A Model Hydrothermal Growth Reactor, Hongmin Li, Minel Braun, Edward Evans, Guo-Xiang Wang, Govind Paudel, Jason Miller Apr 2015

Natural Convection Flow Structures And Heat Transfer In A Model Hydrothermal Growth Reactor, Hongmin Li, Minel Braun, Edward Evans, Guo-Xiang Wang, Govind Paudel, Jason Miller

Dr. Guo-Xiang Wang

Due to the experimental difficulties brought about by high pressure and temperature growth conditions, flow and heat transfer in industrial hydrothermal autoclaves for the growth of single quartz crystals have been studied mostly numerically. To date, most of the numerical models and associated results are not experimentally validated; only qualitative validation data from experiments done during actual crystal growth production is partly available. In this study, the authors used a model simulated reactor represented by an enclosure with two lower half sidewalls uniformly heated while the upper half sidewalls are uniformly cooled. Flow structures in the reactor are qualitatively visualized …


A Three-Dimensional Conjugate Model With Realistic Boundary Conditions For Flow And Heat Transfer In An Industry Scale Hydrothermal Autoclave, Hongmin Li, Edward Evans, Guo-Xiang Wang Apr 2015

A Three-Dimensional Conjugate Model With Realistic Boundary Conditions For Flow And Heat Transfer In An Industry Scale Hydrothermal Autoclave, Hongmin Li, Edward Evans, Guo-Xiang Wang

Dr. Guo-Xiang Wang

This paper presents a conjugate heat transfer model for industry size hydrothermal autoclaves. The electric heating on the wall outside surfaces is represented by constant heat fluxes. The circumferential heat flux deviation is introduced for the asymmetric factors from the surroundings. The results indicate that the temperature at the solution/wall interface is far from uniform. Circumferential temperature deviation is large enough to establish an asymmetric flow. To accurately simulate flows in industry autoclaves, one needs to use the conjugate model. The growth environment in current industry autoclaves, however, can be improved by establishing a uniform temperature on the wall/solution interface.


Three-Dimensional Flow Of Solution In An Industry-Size Hydrothermal Autoclave Subjected To Non-Uniform Heating Effects Of A Baffle On Flow And Temperature Separation, Hongmin Li, Guo-Xiang Wang, Edward Evans Apr 2015

Three-Dimensional Flow Of Solution In An Industry-Size Hydrothermal Autoclave Subjected To Non-Uniform Heating Effects Of A Baffle On Flow And Temperature Separation, Hongmin Li, Guo-Xiang Wang, Edward Evans

Dr. Guo-Xiang Wang

Hydrothermal growth takes place in a closed cylindrical container called an autoclave. Natural convection flow of an aqueous solution at a high temperature and a high pressure carries the nutrient. The high temperature growth condition and the natural convection flow are maintained by two independently controlled electrical heaters on the outside of the autoclave. In practice, the heating is circumferentially non-uniform. Many theoretical and numerical studies, however, assume axially symmetric heating conditions. This paper presents a numerical analysis of the three-dimensional heat transfer and fluid flow with a non-uniform heating condition. The analysis is based on an industry-size autoclave with …