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Full-Text Articles in Engineering
In Situ Sem Solidification Study Of Ga And Egain: A Characterization Technique For Monitoring The Microstructural Evolution Of Liquid Metals, Jeremy Geovann Del Aguila
In Situ Sem Solidification Study Of Ga And Egain: A Characterization Technique For Monitoring The Microstructural Evolution Of Liquid Metals, Jeremy Geovann Del Aguila
Materials Engineering
Scanning electron microscopy (SEM) video recording is used to characterize the solidification of small volumes of 99.999% pure gallium (Ga) and eutectic gallium-indium (eGaIn) under a high vacuum environment. Specimen are superheated to 55℃ using a hot plate, cast into spherical droplets, and cooled in situ by means of a Peltier cooling stage. Special attention is given to the preparation of the specimen prior to viewing because of gallium and its alloys’ nature to form an oxide layer when melted and air cooled. The oxide acts as a skin that inhibits the observation of microstructural features during solidification. Heated samples …
The Effects Of Carboxylic Acids In Aluminum Anodizing, Abby E. Koczera
The Effects Of Carboxylic Acids In Aluminum Anodizing, Abby E. Koczera
Honors Theses and Capstones
Hard-anodized alumina coatings were formed in sulfuric acid at low temperature and high current density in the presence of carboxylic acid additives. Citric acid, trimesic acid, mellitic acid and ethylenediaminetetraacetic acid (EDTA) were utilized in varying concentrations. The additives were chosen for their capacity to form complexes with tri-valent aluminum and hence impart chemical stability to the coatings. The coatings were sealed in boiling water, and corrosion resistance was observed in a high pH solution of potassium hydroxide. The coatings were examined using scanning electron microscopy (SEM) to assess coating thickness and pore dimensions. Thicker coatings were produced when the …
Minimizing Sheet Resistance Of Organic Photovoltaic Cell Top Contact Electrode Layer: Silver Nanowire Concentration Vs. Conductive Polymer Doping Concentration, Caitlyn Cook
Materials Engineering
The top contact electrode layers of nine organic photovoltaic cells were prepared with two varying factors: three Silver nanowire (AgNW) densities deposited on a conductive polymer doped with three concentrations. Silver’s low sheet resistance of 20-Ω/sq is hypothesized to lower the sheet resistance of the anode layer and thus enhance the overall efficiency of the cell. Four-point probe measurements indicated that increasing AgNW density in the top contact electrode layer of an organic photovoltaic cell significantly reduces sheet resistance from 52.2k-Ω/sq to 18.0 Ω/sq. Although an increase in doping concentration of the conductive polymer reduced sheet resistance in low AgNW …