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In Situ Sem Solidification Study Of Ga And Egain: A Characterization Technique For Monitoring The Microstructural Evolution Of Liquid Metals, Jeremy Geovann Del Aguila
In Situ Sem Solidification Study Of Ga And Egain: A Characterization Technique For Monitoring The Microstructural Evolution Of Liquid Metals, Jeremy Geovann Del Aguila
Materials Engineering
Scanning electron microscopy (SEM) video recording is used to characterize the solidification of small volumes of 99.999% pure gallium (Ga) and eutectic gallium-indium (eGaIn) under a high vacuum environment. Specimen are superheated to 55℃ using a hot plate, cast into spherical droplets, and cooled in situ by means of a Peltier cooling stage. Special attention is given to the preparation of the specimen prior to viewing because of gallium and its alloys’ nature to form an oxide layer when melted and air cooled. The oxide acts as a skin that inhibits the observation of microstructural features during solidification. Heated samples …