Engineering Commons^™

Surface Treatment Of Fly Ash For Improving The Tensile Strength Of Fly Ash/Unsaturated Polyester Composites, Sugiman Sugiman, Paryanto Dwi Setyawan

Makara Journal of Technology

The paper presents the surface treatment of fly ashes using acid and alkali solution on the tensile strength of the fly ash/unsaturated polyester (UP) composites. Sulfuric acid (H2SO4), hydrofluoric acid (HF) and sodium hydroxide (NaOH) solution with concentration of 0%, 5%, 10%, 15%, and 20% (by weight) were used for surface treatment of fly ashes. Generally, the tensile strength of the treated fly-ash/UP composites shows a significant increase compared to the untreated fly ash. Of all surface treatments studied, the optimum tensile strength was obtained at a concentration of 10%. At this concentration, at a fly ash content of 30% …

Radiation Characteristics Of A Planar Strip Dipole Antenna And A Slot Dipole Antenna For Thz Applications, Catur Apriono, Eko Tjipto Rahardjo

Makara Journal of Technology

The development of a THz system often requires a device that is used to radiate or detect THz waves. One way to fulfill this requirement is to use an antenna. Therefore, we need to consider the radiation characteristics of an antenna working in the THz region. In this paper, we present simulation study of two dipole antennas, i.e. a planar strip dipole antenna and a slot dipole antenna. The simulation results show that a planar strip dipole antenna has a better radiation efficiency (more than 95%) compared to the slot dipole. It also shows that an efficiency of more than …

Recycling Roof Tile Waste Material For Wall Cover Tiles, Ambar Mulyono, Silfia Mona Aryani, Joko Lulut

Makara Journal of Technology

Prior research on roof tile waste treatment has attempted to find the appropriate technology to reuse old roof tile waste by create wall cladding materials from it. Through exploration and experimentation, a treatment method has been discovered to transform the tile fragments into artificial stone that resembles the shape of coral. This baked clay artificial stone material is then processed as a decorative element for vertical surfaces that are not load-bearing, such as on the interior and exterior walls of a building. Before applying the fragments as wall tiles, several steps must be taken: 1) Blunting, which changes the look …

The Effect Of Pressing Temperature And Time On The Quality Of Particle Board Made From Jatropha Fruit Hulls Treated In Acidic Condition, Apri Heri Iswanto, Fauzi Febrianto, Yusuf Sudo Hadi, Surdiding Ruhendi, Dede Hermawan

Makara Journal of Technology

The high of pH of jatropha fruit hulls causes the negative properties of particleboard made from this material. Adjusting the particle acidity and pressing conditions (temperature and time) is among the technical modifications available to improve this particleboard’s properties. Particle acidity has been adjusted in a previous research project, and immersing the particles in acetic acid was found to be the best treatment in this preliminary research. In order to improve the particleboard’s properties, an experiment was conducted to determine the best pressing temperature and time. The objective of the research was to evaluate the influence of pressing temperature and …

Synthesis Of Tungsten Oxide Nanowires Onto Ito Glass Using T-Cvd, Tomy Abuzairi, Bohr-Ran Huang, Tzu-Ching Lin

Makara Journal of Technology

Tungsten oxide is an n-type semiconductor with interesting physical and chemical properties that make it suitable for various technological applications. Tungsten oxide nanowires were synthesized not only at low temperature but also without the use of any catalysts. The tungsten oxide nanowires were synthesized at 550 °C with tungsten layers onto the ITO glass using thermal chemical vapor deposition (T-CVD). The SEM image shows that the tungsten oxide nanowires are effectively grown with the 200 nm tungsten film. The Raman spectra shoulder at ~690 cm-1 proves the synthesized of tungsten oxide nanowires.

Microgrid Development Using A Grid Tie Inverter, Hartono Budi Santoso, Budiyanto Budiyanto

Makara Journal of Technology

The use of renewable energy sources (RES), especially photovoltaic (PV), to meet the demand of electrical energy has been getting a great deal of attention as an alternative solution to electrical energy deficit problems. RES are being applied in power systems in a variety of configurations including microgrid systems. One of the characteristics of a microgrid is capability to supplying power to grid when there is an excess power to supply local load. This research examines the chances of saving power consumption from grid using power converters grid tie inverter (GTI) in a microgrid configuration. The test is done by …

Semiconductor Thermal Neutron Detector, Toru Aoki, Aki Miyake, Takayuki Nakano, Akifumi Koike, Hisashi Morii, Hidenori Mimura

Makara Journal of Technology

The CdTe and GaN detector with a Gd converter have been developed and investigated as a neutron detector for neutron imaging. The fabricated Gd/CdTe detector with the 25 mm thick Gd was designed on the basis of simulation results of thermal neutron detection efficiency and spatial resolution. The Gd/CdTe detector shows the detection of neutron capture gamma ray emission in the 155Gd(n, g)156Gd, 157Gd(n, g)158Gd and 113Cd(n, g)114Cd reactions and characteristic X-ray emissions due to conversion-electrons generated inside the Gd film. The observed efficient thermal neutron detection with the Gd/CdTe detector shows its promise in neutron radiography application. Moreover, a …

High Energy Synchrotron X-Ray Study Of Fatigue Damage In Amorphous And Polycrystalline Engineering Alloys, Chih-Pin Chuang

Doctoral Dissertations

The dissertation summarizes a series of studies on the fatigue damage of both amorphous and crystalline engineering alloys. The attention focuses on the utilization of synchrotron x-ray scattering related techniques for advanced material characterizations. In the first part of the research, critical issues regarding the mechanical response and structural evolution of Bulk-Metallic Glasses (BMGs) in the elastic region are addressed. The effects of cyclic-loading on the microstructures of an amorphous alloy are investigated, aiming to provide better mechanistic understandings of fatigue damage in BMGs. The second part of the research focuses on the characterization method based on two-dimensional X-ray diffraction …

Understanding Mechanical And Fatigue Behavior Of A Wrought Magnesium Alloy Using In-Situ Neutron And Synchrotron X-Ray Diffraction, Wei Wu

Doctoral Dissertations

Magnesium (Mg) alloys have received great attentions in the past several decades, due to their unique properties of low density, high strength-to-weight ratio, and high specific stiffness. Previous work on fatigue behavior of Mg alloys typically relies on ex situ microstructural characterization and crack-growth monitoring with replica techniques. The primary challenge is thus the lack of an in situ, non-destructive measurement on microstructural length scales, which prevents us from linking the stress analyses (top-down point of view) to the failure mechanisms on inter- and intra-granular scales (bottom-up point of view). A unique opportunity that resolves many of these difficulties …

Evaluation Of Alternate Mouthpiece Material Types To Minimize Vibrations And Heat Loss - The Research And Execution Of Prototypes, Kristen Bobuk

Theses, Dissertations and Capstones

This paper is based on the idea of current horn mouthpieces being made solely out of brass with a limited market of stainless steel and titanium with plating being silver or gold. This is an opportunity to explore alternate materials; specifically steel, cast iron and aluminum for the base material and chrome, copper and nickel for plating materials. Readers will learn about metal properties such as hardness, thermal conductivity and specific heat and learn why certain materials are more beneficial than others.

Ultrasonic Propagation And Scattering In Pearlitic Steel, Hualong Du

Department of Engineering Mechanics: Dissertations, Theses, and Student Research

Diffuse ultrasonic backscatter measurements have been especially useful for extracting microstructural information and for improving flaw detection in materials. In this dissertation, this approach is applied to inspection of railroad wheels. To improve the wear resistance, the tread surfaces of railroad wheels are usually quenched with water to increase the hardness. The pearlite phase of iron, characterized by alternating ferrite and cementite phases, is created by the quenching and the lamellar spacing within grains increases progressively from the quenched tread surface to deeper locations due to the non-uniform cooling rate. The quench depth is an important parameter governing the wheel …

Reflectance Anisotropy Of Gd5si2ge2 And Tb5si2.2ge1.8, S. J. Lee, Joong Mok Park, J. E. Snyder, David C. Jiles, Deborah L. Schlagel, Thomas A. Lograsso, A. O. Pecharsky, David W. Lynch

Professor David Lynch

Reflectance difference (RD) spectra for the a–b plane of the single crystals of Gd5Si2Ge2and b–c planes of Gd5Si2Ge2 and Tb5Si2.2Ge1.8 were obtained in the photon energy range of 1.5–5.5 eV. Several peaks were observed for these crystals in the measured spectrum range. Similar features were observed in the RD spectra for the b–c planes ofGd5Si2Ge2 and Tb5Si2.2Ge1.8, while different features were observed for the a–b plane and b–c plane of Gd5Si2Ge2. The RD spectra for the crystals arise not only from the surface anisotropy but also from the bulk anisotropy due to the monoclinic structure of the bulk crystal.

Intermetalic Growth Rate In Transient Liquid Phase Sintering Of Pb-Free Solder Interconnects, Shuqing Zhang, John Blendell

The Summer Undergraduate Research Fellowship (SURF) Symposium

Following the electron devices are widely used in daily life, Pb-free solder alloy, as the replacement of Pb solder joint material, needs extensive researches to observe the properties for using and simulation purpose. Solder are used as the joint to connect two work pieces in printed wiring board of electronics. Most lead-free solders comprise tin (Sn) as the majority component, and nominally pure b-Sn is the majority phase in the microstructure of these solders. The most important thing for solder joint that researchers care about is its life cycle. Due to the incomplete of the mechanical profile of Pb-free solder …

Numerical Modeling Of Solidification Process And Prediction Of Mechanical Properties In Magnesium Alloys, Mehdi Farrokhnejad

Electronic Thesis and Dissertation Repository

A formulation used to simulate the solidification process of magnesium alloys is developed based upon the volume averaged finite volume method on unstructured collocated grids. To derive equations, a non-zero volume fraction gradient has been considered and resulting additional terms are well reasoned. For discretization the most modern approximations for gradient and hessians are used and novelties outlined. Structure-properties correlations are incorporated into the in-house code and the proposed formulation is tested for a wedge-shaped magnesium alloy casting. While the results of this study show a good agreement with the experimental data, it was concluded that a better understanding of …

Probabilistic Simulation Of Solidification Microstructure Evolution During Laser-Based Metal Deposition, Jingwei Zhang, Frank W. Liou, William Seufzer, Joseph William Newkirk, Zhiqiang Fan, Heng Liu, Todd E. Sparks

Mechanical and Aerospace Engineering Faculty Research & Creative Works

A predictive model, based on a Cellular Automaton (CA) - Finite Element (FE) method, has been developed to simulate microstructure evolution during metal solidification for a laser based additive manufacturing process. The macroscopic FE calculation was designed to update the temperature field and simulate a high cooling rate. In the microscopic CA model, heterogeneous nucleation sites, preferential growth orientation and dendritic grain growth kinetics were simulated. The CA model was able to show the entrapment of neighboring cells and the relationship between undercooling and the grain growth rate. The model predicted the dendritic grain size, structure, and morphological evolution during …

The Effect Zeolite Addition In Natural Rubber Polypropylene Composite On Mechanical, Structure, And Thermal Characteristics, Nurdin Bukit, Erna Frida

Makara Journal of Technology

This study was conducted to determine the effect of zeolite as filler on mechanical properties, and thermal structure blends of natural rubber and polypropylene (NR/PP). In this study, NR/PP/PP-g-MA blends was filled uncalcined zeolite and calcined zeolite at different weight percent of the 2, 4, and 6%. Samples were characterized to determine the tensile strength, fracture elongation and Young's modulus. Structure of the samples was investigated using XRD method and thermal characteristics were analyzed using DTA/TGA technique. The results obtained for tensile strength showed a significant influence with the addition zeolite of the NR/PP blends at 2% by weight of …

Improvement In Performance Of Zno Based Dsc Prepared By Spraying Method, Rangga Winantyo, Devinda Liyanage, Kenji Murakami

Makara Journal of Technology

This paper reports the effect of TiCl4 on the performance of ZnO based DSC. ZnO was used due to its stability against photo-corrosion and photochemical properties similar to TiO2. Thin films of nanocrystalline ZnO were deposited on transparent conducting oxide glass using spray method. The ZnO films were treated using TiCl4. The cell’s efficiency was found to be 2.5% with TiCl4 post-treatment and 1.9% without TiCl4 post-treatment.

Characteristics Of Vacuum Freeze Drying With Utilization Of Internal Cooling And Condenser Waste Heat For Sublimation, Muhammad Idrus Alhamid, Nasruddin Yusuf, Indra Teuku Meurah Mahlia, Engkos Ahmad Kosasih, Muhamad Yulianto, Rio Ricardi

Makara Journal of Technology

Vacuum freeze drying is an excellent drying method, but it is very energy-intensive because a relatively long drying time is required. This research investigates the utilization of condenser waste heat for sublimation as a way of accelerating the drying rate. In addition, it also investigates the effect of internal cooling combined with vacuum cooling in the pressure reduction process. Jelly fish tentacles were used as the specimen, with different configurations for condenser heat waste and internal cooling valve opening. The results show that heating with condenser heat waste can accelerate the drying rate up to 0.0035 kg/m2.s. In addition, pre-freezing …

The Plasma Electrolysis Phenomenon In A Two-Compartment Reactor For Chlor-Alkali Production, Nelson Saksono, Fakhrian Abqari, Setijo Bismo

Makara Journal of Technology

Chlor-alkali is one of the most important processes in the chemical industry. It produces chlorine and caustic soda, which become the main feedstock of daily products. The aim of this study is to report the phenomenon of plasma electrolysis and how it can be used in chlor-alkali production for more efficient energy consumption. When the plasma is formed, the current fluctuates and gradually declines. Plasma electrolysis begins with the process of electrolysis itself. Due to Joule heating, gas bubbles are formed and a sheath is made on both electrodes, resulting in the plasma field. Plasma electrolysis can be identified by …

Observation Of Photovoltaic Effect And Single-Photon Detection In Nanowire Silicon Pn-Junction, Arief Udhiarto, Sri Purwiyanti, Daniel Moraru, Takeshi Mizuno, Michiharu Tabe

Makara Journal of Technology

We study nanowire silicon pin and pn-junctions at room and low temperature. Photovoltaic effects are observed for both devices at room temperature. At low temperature, nanowire pn-junction devices show their ability to detect single photon. This ability was not been observed for pin devices. Phosphorus-boron dopant cluster in the depletion region is considered to have the main role for single-photon detection capability. Fundamental mechanism of dopant-based single-photon detection in nanowire pn-junction is described in details.

Influences Of Surface Morphology Of Nanostructured Rutile Tio2 Nanorods/Nanoflowers As Photoelectrode On The Performance Of Dye-Sensitized Solar Cell, Mohd Khairul Bin Ahmad, Kenji Murakami

Makara Journal of Technology

Aligned Rutile TiO2 nanorods (r-TNRs) and TiO2 nanoflowers (r-TNFs) were successfully prepared by hydrothermal method. Using hydrochloric acid (HCl) as chelating agent and titanium butoxide (TBOT) as precursor, aligned r-TNRs with r-TNFs were successfully growth onto fluorine-doped tin oxide (FTO) with different morphologies. The influences of surface morphologies to the rutile based Dye-sensitized solar cell (DSC) efficiency are discussed. The highest lightto- electric energy conversion efficiency, 1.80% is achieved using different concentration under simulated solar light illumination of 100 mWcm-2 (1.5 AM).

Fatigue Life Prediction Of The Keel Structure Of A Tsunami Buoy Using Spectral Fatigue Analysis Method, Angga Yustiawan, Ketut Suastika, Wibowo Harso Nugroho

Makara Journal of Technology

One of the components of the Indonesia Tsunami Early Warning System (InaTEWS) is a surface buoy. The surface buoy is exposed to dynamic and random loadings while operating at sea, particularly due to waves. Because of the cyclic nature of the wave load, this may result in a fatigue damage of the keel structure, which connects the mooring line with the buoy hull. The operating location of the buoy is off the Java South Coast at the coordinate (10.3998 S, 108.3417 E). To determine the stress transfer function, model tests were performed, measuring the buoy motions and the stress at …

Determining The Air Gap Length Of An Axial Flux Wound Rotor Synchronous Generator, Abdul Multi, Iwa Garniwa, Uno Bintang Sudibyo

Makara Journal of Technology

The air gap length of the designed axial flux wound rotor (AFWR) synchronous generator is determined properly according to the design parameters. One of the distinct advantages of an axial flux (AF) machine is its adjustable air gap. An AF generator’s performance might be controlled by adjusting its air gap. The designed generator has a smallscale capacity that has 1 kW, 380 V, and 50 Hz. The windings are laid into slots made from laminated core. The slots are carved in the face of the stator and rotors. The generator has a single-double-sided slotted wound stator sandwiched between twin rotors. …

Production Optimization For Plan Of Gas Field Development Using Marginal Cost Analysis, Suprapto Soemardan, Widodo Wahyu Purwanto, Arsegianto Arsegianto

Makara Journal of Technology

Gas production rate is one of the most important variables affecting the feasibility plan of gas field development. It take into account reservoir characteristics, gas reserves, number of wells, production facilities, government take and market conditions. In this research, a mathematical model of gas production optimization has been developed using marginal cost analysis in determining the optimum gas production rate for economic profit, by employing the case study of Matindok Field. The results show that the optimum gas production rate is mainly affected by gas price duration and time of gas delivery. When the price of gas increases, the optimum …

A New Experimental Approach To Evaluate Plasma-Induced Damage In Microcantilever, Yuki Nishimori, Shinji Ueki, Masakazu Sugiyama, Seiji Samukawa, Gen Hashiguchi

Makara Journal of Technology

Plasma etching, during micro-fabrication processing is indispensable for fabricating MEMS structures. During the plasma processes, two major matters, charged ions and vacuum–ultraviolet (VUV) irradiation damage, take charge of reliability degradation. The charged ions induce unwanted sidewall etching, generally called as “notching”, which causes degradation in brittle strength. Furthermore, the VUV irradiation gives rise to crystal defects on the etching surface. To overcome the problem, neutral beam etching (NBE), which use neutral particles without the VUV irradiation, has been developed. In order to evaluate the effect of the NBE quantitatively, we measured the resonance property of a micro-cantilever before and after …

Strain-Driven Transition From E-Type To A-Type Magnetic Order In Ymno₃ Epitaxial Films, F. Jiménez-Villacorta, J. A. Gallastegui, I. Fina, X. Marti, J. Fontcuberta

Felix Jiménez-Villacorta

Single-crystal (100)-oriented YMnO3 thin films grown on (110)-oriented SrTiO3 substrates have been studied by polarized extended x-ray absorption fine structure to determine the Mn-O bond lengths. Using a simple geometrical model and previously reported x-ray diffraction data on the same samples, the Mn-O-Mn bonding angles are calculated. We show that the epitaxy-induced in-plane anisotropic strain has a dramatic impact on the bonding angles, allowing the rationalization of the reported existence of cycloidal magnetic order and concomitant ferroelectricity in moderately strained films and the gradual suppression by larger strains. We shall argue that epitaxial strain allows shifting YMnO3 from an E-type …

Deformation Behavior Of Bulk Metallic Glasses And High Entropy Alloys By Nanoindentation, Yuting Li

Masters Theses

Nanoindentation has become a powerful tool in the measurement of the mechanical properties of diverse materials, such as metallic materials, polymer materials, and even biomaterials.

In this thesis, three types of Zr-based bulk metallic glasses (BMGs) were investigated by nanoindentation. Our work focuses on the characterization of the hardness, the reduced modulus, and the deformation behavior under different indentation conditions. The study of the hardness and the reduced modulus is to access the effect of the indentation load on deformation behavior and to determine the inhomogeneous deformation. The morphological profiles of the residual indentation on the surface of the specimen …

Effect Of Zinc Galvanization On The Microstructure And Fracture Behavior Of Low And Medium Carbon Structural Steels, Ignatius C. Okafor, Ronald J. O'Malley, Kaushal R. Prayakarao, Heshmat A. Aglan

Materials Science and Engineering Faculty Research & Creative Works

Microstructure and fracture behavior of ASTM 572 Grade 65 steels used for wind tower applications have been studied. Steels of two carbon level chemistries designed for this grade were used in the study. Fracture toughness of the steels was studied using 3-point bend test on samples coated with zinc and not coated with zinc. Lower carbon steel showed higher resistance to fracture than medium carbon steel after zinc galvanization. SEM study suggests that zinc and zinc bath additives that migrated to crack tips are responsible for the loss in ductility. The phenomenon of Liquid Metal Embrittlement (LME) is suggested to …

Site Specifc Growth Of Metal Catalyzed Silica Nanowires For Biological And Chemical Sensing, Eric G. Huey

FIU Electronic Theses and Dissertations

In this research the integration of nanostructures and micro-scale devices was investigated using silica nanowires to develop a simple yet robust nanomanufacturing technique for improving the detection parameters of chemical and biological sensors. This has been achieved with the use of a dielectric barrier layer, to restrict nanowire growth to site-specific locations which has removed the need for post growth processing, by making it possible to place nanostructures on pre-pattern substrates. Nanowires were synthesized using the Vapor-Liquid-Solid growth method. Process parameters (temperature and time) and manufacturing aspects (structural integrity and biocompatibility) were investigated.

Silica nanowires were observed experimentally to determine …

Influence Of Microstructure On The Propagation Of Fatigue Cracks In Inconel 617, Benjiman Michael Albiston

Boise State University Theses and Dissertations

Inconel 617 is a candidate material for use in the intermediate heat exchanger of the Next Generation Nuclear Plant. Because of the high temperatures and the fluctuations in stress and temperature, the fatigue behavior of the material is important to understand. The goal of this study was to determine the influences of the microstructure during fatigue crack propagation. For this investigation, Inconel 617 compact tension samples, fatigue tested by Julian Benz at the Idaho National Laboratory, were obtained. The testing conditions included two environments at 650 °C (lab air and impure-He) and varied testing parameters including: loading waveform (triangular, trapezoidal), …