Engineering Commons^™

Design Methodology For Input Shapers Using Genetic Algorithms In Flexible Nonlinear Systems, Mohab Adel Hakim Meshreki

Archived Theses and Dissertations

No abstract provided.

Smooth Muscle Cells Affect Differential Nanoparticle Accumulation In Disturbed Blood Flow-Induced Murine Atherosclerosis, Hunter Miller, Morgan A. Schake, Badrul Alam Bony, Evan T. Curtis, Conner C. Gee, Ian Mccue, Thomas J. Ripperda Jr., Yiannis S. Chatzizisis, Forrest Kievit, Ryan M. Pedrigi

Department of Mechanical and Materials Engineering: Faculty Publications

Atherosclerosis is a lipid-driven chronic inflammatory disease that leads to the formation of plaques in the inner lining of arteries. Plaques form over a range of phenotypes, the most severe of which is vulnerable to rupture and causes most of the clinically significant events. In this study, we evaluated the efficacy of nanoparticles (NPs) to differentiate between two plaque phenotypes based on accumulation kinetics in a mouse model of atherosclerosis. This model uses a perivascular cuff to induce two regions of disturbed wall shear stress (WSS) on the inner lining of the instrumented artery, low (upstream) and multidirectional (downstream), which, …

Microfabricated Platforms To Investigate Cell Mechanical Properties, Amir M. Esfahani, Grayson Minnick, Jordan Rosenbohm, Haiwei Zhai, Xiaowei Jin, Bahareh Tajvidi Safa, Justin Brooks, Ruiguo Yang

Department of Mechanical and Materials Engineering: Faculty Publications

Mechanical stimulation has been imposed on living cells using several approaches. Most early investigations were conducted on groups of cells, utilizing techniques such as substrate deformation and flow-induced shear. To investigate the properties of cells individually, many conventional techniques were utilized, such as AFM, optical traps/optical tweezers, magnetic beads, and micropipette aspiration. In specific mechanical interrogations, microelectro- mechanical systems (MEMS) have been designed to probe single cells in different interrogation modes. To exert loads on the cells, these devices often comprise piezo-electric driven actuators that attach directly to the cell or move a structure on which cells are attached. Uniaxial …

Interfacial Bonding Between Thermoset And Thermoplastic Polyurethane Reinforced Textile Grade Carbon Fiber: Structure Property Relationships, Surbhi Subhash Kore

Doctoral Dissertations

The research work focused on examining the interfacial adhesion of unsized, epoxy, and urethane-sized textile grade carbon fiber (TCF) reinforced in different classes of polyurethane (PU) thermoplastic (TPU) and thermoset (TSU) polyurethane (PU) through the structure-property relationship. The Carbon Fiber Technology Facility (CFTF) at Oak Ridge National Laboratory (ORNL) has produced TCF to reduce the cost of commercial-grade carbon fiber. The first part of the research examined the fundamental relationships between (a) soft segment thermoplastic polyurethane (S-TPU), (b) hard segment thermoplastic polyurethane (H-TPU), (c) thermoset polyurethane (TSU) and TCF reinforcement’s molecular behavior at the interface using the surface and thermal …

Structural Stability Of Thermosets During Material Extrusion Additive Manufacturing, Stian K. Romberg

Doctoral Dissertations

Over the past decade, the scale of polymer additive manufacturing has been revolutionized with machines that print massive thermoplastic parts with greater geometric complexity than can be achieved by traditional manufacturing methods. However, the heat required to print thermoplastics consumes energy and induces thermal gradients that can reduce manufacturing flexibility and final mechanical properties. With the ability to be extruded at room temperature and excellent compatibility with fibers and fillers, thermoset resins show promise to decrease the energy consumption, expand the manufacturing flexibility, and broaden the material palette offered by large-scale polymer additive manufacturing. However, structural instability in the uncured …

Rational Design Of Multifunctional Nanocatalysts For Environmental Remediation And Energy Conversion Technologies, Md Ariful Ahsan

Open Access Theses & Dissertations

The discovery of efficient and sustainable carbon-based nanotechnologies to solve both the scarcity of drinking water and global energy crisis has become a paramount task in the last decades. Owed to the fast population growth and industrialization of the modern society, access to potable water and clean energy technologies is becoming very hard around the globe. Water pollutants have become a serious threat to the environment and ecology because of their toxic nature. Parallelly, the current hydrocarbon-based fuel industries are generating high levels of contamination across the planet, making imperative the development of cleaner energy technologies. In this regard, the …

Thermodynamic Modeling Of Aqueous Fe-Cu-As-Sb-Bi-H2so4 Solutions And Its Application For Redox Potential Determination In Copper Electrorefining From 25°C To 70°C, Yongteng Dong

Open Access Theses & Dissertations

Impurity elements in copper electrorefining (ER) electrolyte have been becoming a crucial issue on purity of copper cathode. The objective of this doctoral research is to develop a speciation model to understand impurity behavior in aqueous ER solutions.

A thermodynamic model of Fe(II)-Fe(III)-Cu(II)-H2SO4-H2O system is developed and shown to reliably simulate the species distribution in industrial copper electrorefining electrolyte from 25°C to 70°C. The previously developed model of Fe(II)-Fe(III)-H2SO4-H2O system under leaching conditions was first evaluated. It has proved that its applicability can be extended to much higher acid concentration (185 g/L) and high amount of copper (40-50 g/L). Cu(II) …

Synthesis And Characterization Of Tin (Sn) Incorporated Ga2o3, Guillermo Nicolas Gutierrez

Open Access Theses & Dissertations

In this work, we report on the synthesis, characterization of tin (Sn) incorporated gallium oxide Ga2O3 compounds, also included in this work is the effect of tin concentration related to the optical and electrochemical properties. The Sn incorporation into Ga2O3 creates a significant reduction in the bandgap and causes a nonlinear optical activity as the concentration varies. Substantial investigation performed to the structure, phase, and morphology of the mixed compounds governed by the stoichiometry equation Ga2−2xSnxO3-ɗ indicates that the Sn incorporation from 0.00 ≤ x ≤ 0.30 has a significant effect on these properties. To synthesize the Ga-Sn-O compounds a …

Synthesis, Characterization, And Direct-Ink-Writing Of Syntactic Foams, Andrea Irigoyen

Open Access Theses & Dissertations

This project encompasses three different methods to fabricate syntactic foams using a PDMS matrix i.e., hollow spheres inclusion, pore generator leaching by solvent, and emulsion. The foam formation by using polysiloxane hollow spheres is done in a 3-step process. The first step is to create a core of polystyrene following a dispersion polymerization process. The goal for the size of the pore is to monodisperse and have an average diameter of 5-10 μm, so the polystyrene core must be as well within that range. After that, the cores are coated with a polysiloxane shell by following a polymerization by condensation …

Phase Transformation And Strain Hardening Mechanisms In Advanced Engineering Steels, Hangyu Dong

Open Access Theses & Dissertations

Strain hardening and associated deformation mechanisms play a determining role in the performance of metallic materials. The objective of the doctoral research was to explore and fundamentally understand the strain hardening mechanisms in the next generation of advanced engineering steels. Two main work hardening mechanisms, notably, twinning-induced plasticity (TWIP) and transformation-induced plasticity (TRIP)) were identified that governed strength and ductility. In the nanograined austenitic steel with high strength-high ductility combination, processed by the novel phase reversion concept, twinning-induced plasticity (TWIP) was the governing deformation mechanism and contributed to good ductility. In striking contrast, transformation-induced plasticity (TRIP) was the deformation mechanism …

Microstructure And Hardness Comparison Of Inconel 625 Alloy Of Various Additive Manufacturing Processes Following Heat Treatments, Ariel Gamon

Open Access Theses & Dissertations

This research study presents experimental examples of as-built microstructures and associated microindentation hardnesses (HV) for a variety of metal additive manufacturing (AM) methods for Inconel 625 alloy. Cold spray (CS), laser powder bed fusion (L-PBF), wire arc additive manufacturing (WAAM), electron beam directed energy deposition (EB-DED), laser hot wire (LHW), binder jetting (BJT), and laser power directed energy deposition (LP-DED), laser wire directed energy deposition (LW-DED) and electron beam melting (EBM) were among the techniques employed. Microstructures varied from impact-bonded, flattened grains containing microdendrites and dislocations with a microindentation hardness of HV 590 for cold spray to large, equiaxed grains …

Innovations In Aligned And Overmolded Long Fiber Thermoplastic Composites, Shailesh P. Alwekar

Doctoral Dissertations

Long fiber thermoplastic (LFT) composite materials are increasingly used in high performance lightweight automotive, sporting, and industrial applications. LFT composites are processed with extrusion-compression molding (ECM) and/or injection molding (IM). Melt extrusion offers unique opportunities to align long fibers in a thermoplastic polymer melt. The properties of LFT materials are highly influenced by processing techniques which leads to different porosity content, fiber length distribution, and fiber orientation distribution. Hence, it is important to understand the various LFT processing techniques and their effect on mechanical, thermal, and microscopic properties.

The fundamental process-property relationships in LFT composites are investigated in this dissertation. …

Understanding The Chemical Structures Of Polydopamine, Deborah Takyibea Okyere

Graduate Theses and Dissertations

Polydopamine (PDA) is described as a bioinspired polymer produced by a method involving the chemical oxidation of dopamine in a pH-dependent medium. It has been used for the functionalization of nanomaterials in diverse applications including drug delivery and biosensing because of its strong adhesiveness, functionality is easily modified, and biocompatibility with mammalian cells and tissues. The polymerization process is believed to be initiated by the autoxidation of dopamine to dopaminequinone. However, the repeating units, as well as the final structure of PDA, are not well understood. Hence, this work focuses on the characterizations of the PDA structures during formation and …

Assessing Mechanical Performance Of Dissimilar Steel Systems Made Via Wire-Arc Additive Manufacturing, Obed Daniel Acevedo

Masters Theses

Hot stamping is part of a specific type of metalworking procedure widely used in the automotive industry. This research seeks to help make hot stamp tooling component production more cost-effective by using large-scale additive manufacturing. Additive manufacturing can produce dissimilar steel components that can be more cost-effective and time-efficient and allow for complex geometries to be made. A dissimilar steel system consisting of 410 martensitic stainless steel and AWS ER70S-6 mild steel is proposed to make hot stamps, making them more cost-efficient. However, the material interface's mechanical behavior in 410SS-mild steel additively manufactured material systems is not well understood. This …

Mechanical Properties And Microstructure Evolution Of Thermally Treated Laser Powder Bed Fusion Alsi10mg, Jorge Merino-Gomez

Open Access Theses & Dissertations

The optimization of mechanical properties with thermal postprocessing treatments was investigated in this study across a wide variety of variants. The relationship between heat treatments and the impacts on the mechanical properties and microstructure of printed materials is a crucial part of additive manufacturing. As a result, the current paper provides a comprehensive overview of postprocess heat treatments for Laser Powder Bed Fusion fabricated AlSi10Mg alloy, including stress relief anneals at 190 and 285 degrees Celsius for 2 hours, hot isostatic pressing at 515 degrees Celsius for 3 hours, hot isostatic pressing + T6 treatment for 6 hours, and final …

Autonomous Control And Signal Acquisition System, Rion Krampe

Scholars Week

Dr. Bunget has an autonomous control and signal acquisition system that he wants to be repaired and improved upon. This requires that we identify the current issues with the system and repair them as well as make innovations to the system to meet customer needs. The position control needs to be autonomous, and the acquisition of the oscilloscope signal and the transducer position needs to be synchronous. The user should be able to control the position, speed, and how often the signals are captured. The waveform of the scan should be appended into a spreadsheet. The system code also needs …

Quick - Release End Effector Tool Interface, Shane Farritor, Thomas Frederick

Department of Mechanical and Materials Engineering: Faculty Publications

The various embodiments herein relate to a coupling apparatus for a medical device having a coupler body, a cavity defined in the coupler body, a rotatable drive component disposed within the cavity and having at least two pin receiving openings, and an actuable locking ring disposed around the cavity.

In Situ Characterization Of Tensile Behavior Of Laser Rapid Solidified Al–Si Heterogeneous Microstructures, Bingqiang Wei, Wenqian Wu, Dongyue Xie, Huai-Hsun Lien, Metin Kayitmazbatir, Amit Misra, Jian Wang

Department of Mechanical and Materials Engineering: Faculty Publications

Heterogeneous Al–Si microstructure comprising of sub-micron-scale Al dendrites and nanoscale Al–Si fibrous eutectic was fabricated by processing as-cast Al-20wt.%Si alloy using laser rapid solidification. In situ tension tests explored high tensile strength ( ∼ 600 MPa) and ductility ( ∼ 10%) and high strain hardening rate ( ∼ 7 GPa). Microstructural characterization revealed the plastic co[1]deformation mechanisms between soft Al dendrites and hard nanoscale Al–Si eutectic. The progression of plasticity in nanoscale Al–Si eutectic with increasing applied strain is accommodated by dislocation plasticity in the nano-Al channels and cracking Si nanofibers. The propagation of nano-cracks is suppressed by surrounding Al, …

Digitally Twinned Additive Manufacturing: Detecting Flaws In Laser Powder Bed Fusion By Combining Thermal Simulations With In-Situmeltpool Sensor Data, R Yavari, A Riensche, E Tekerek, L Jacquemetton, H Halliday, M Vandever, A Tenequer, V Perumal, A Kontsos, Z Smoqi, K Cole, P Rao

Department of Mechanical and Materials Engineering: Faculty Publications

The goal of this research is the in-situ detection of flaw formation in metal parts made using the laser powder bed fusion (LPBF) additive manufacturing process. This is an important area of research, because, despite the considerable cost and time savings achieved, precision-driven industries, such as aerospace and biomedical, are reticent in using LPBF to make safety–critical parts due to tendency of the process to create flaws. Another emerging concern in LPBF, and additive manufacturing in general, is related to cyber security – malicious actors may tamper with the process or plant flaws inside a part to compromise its performance. …

Evaluation Of Additively Manufactured Lattices Under High Strain Rate Impact, Derek G. Spear

Theses and Dissertations

Several additively manufactured lattice designs and configurations were evaluated under compression loads under various strain rates from quasi-static to highly dynamic. These experiments examined how the mechanical behavior of the lattice changed based on the lattice design properties and the applied strain rates. The modulus of elasticity, yield strength, plateau stress, and toughness were observed to decrease with an increase in strain rate, revealing that the lattice designs exhibit a negative strain rate sensitivity. A new lattice flow stress model was developed to account for the mechanical response of the lattice and was incorporated into a computational model for simulation. …

Molecular Dynamics Simulations Of Self-Assemblies In Nature And Nanotechnology, Phu Khanh Tang

Dissertations, Theses, and Capstone Projects

Nature usually divides complex systems into smaller building blocks specializing in a few tasks since one entity cannot achieve everything. Therefore, self-assembly is a robust tool exploited by Nature to build hierarchical systems that accomplish unique functions. The cell membrane distinguishes itself as an example of Nature’s self-assembly, defining and protecting the cell. By mimicking Nature’s designs using synthetically designed self-assemblies, researchers with advanced nanotechnological comprehension can manipulate these synthetic self-assemblies to improve many aspects of modern medicine and materials science. Understanding the competing underlying molecular interactions in self-assembly is always of interest to the academic scientific community and industry. …

Contact Angle Measurement Using A Hele-Shaw Cell: A Proof-Of-Concept Study, Haipeng Zhang, Jacob Gottberg, Sangjin Ryu

Department of Mechanical and Materials Engineering: Faculty Publications

Contact angle is an important property to quantify the wettability of a solid surface with a liquid, which characterizes interactions of the solid-liquid pair. Generally, to measure contact angle, special instruments such as a goniometer are necessary, but they are not readily available in certain research settings. In this study, an alternative method to measure contact angle based on a Hele-Shaw cell, microscopy imaging, and image processing is suggested. In this method, a liquid drop is injected into a transparent Hele-Shaw cell, the meniscus of the drop is captured in the top or bottom view using a brightfield microscope, and …

Contact Angle Measurement Using A Hele-Shaw Cell: A Proof-Of-Concept Study, Haipeng Zhang, Jacob Gottberg, Sangjin Ryu

Department of Mechanical and Materials Engineering: Faculty Publications

Contact angle is an important property to quantify the wettability of a solid surface with a liquid, which characterizes interactions of the solid-liquid pair. Generally, to measure contact angle, special instruments such as a goniometer are necessary, but they are not readily available in certain research settings. In this study, an alternative method to measure contact angle based on a Hele-Shaw cell, microscopy imaging, and image processing is suggested. In this method, a liquid drop is injected into a transparent Hele-Shaw cell, the meniscus of the drop is captured in the top or bottom view using a brightfield microscope, and …

Nucleation Studies In Barium Silicate Glasses And Soda-Lime Silicate Glass, Xinsheng Xia

McKelvey School of Engineering Theses & Dissertations

Controlling nucleation is key for the manufacture of glasses and glass-ceramics. It has been observed by different researchers in many silicate glasses that at low temperatures the critical work of cluster formation (i.e. the nucleation barrier) slowly rises rather than decreasing with decreasing temperature. However, this experimental observation is in contradiction with nucleation theories. In this dissertation, crystal nucleation was studied in BaO·2SiO2, 5BaO·8SiO2, and Na2O·2CaO·3SiO2 glasses. The main research topics include measurements of the nucleation rate, the structural evolution of the glass, and the low-temperature nucleation behavior. A special focus is given to the low-temperature nucleation anomaly. In total, …

Flexible Electronics For Neurological Electronic Skin With Multiple Sensing Modalities, Haochuan Wan

McKelvey School of Engineering Theses & Dissertations

The evolution of electronic skin (E-skin) technology in the past decade has resulted in a great variety of flexible electronic devices that mimic the physical and chemical sensing properties of skin for applications in advanced robotics, prosthetics, and health monitoring technologies. The further advancement of E-skin technology demands closer imitation of skin receptors' transduction mechanisms, simultaneous detection of multiple information from different sources, and the study of transmission, processing and memory of the signals among the neurons. Motivated by such demands, this thesis focuses on design, fabrication, characterization of novel flexible electronic devices and integration of individual devices to realize …

Novel Photothermal Materials And Thermally Engineered Membranes For Solar Desalination, Sisi Cao

McKelvey School of Engineering Theses & Dissertations

Although 71% of earth surface is covered with water, more than 97% of it is saltwater, and freshwater is limited to only about 2.5%. The freshwater shortage has been exacerbated due to the environmental pollution, increased agriculture needs, socio-economic development, and population growth. Among various desalination technologies, membrane distillation has gained wide attention due to its ability to treat highly saline water utilizing waste heat from industrial processes. However, the implementation of conventional membrane distillation is hindered in the remote regions and disaster-struck communities where the low-grade thermal energy from industrial plants and electricity are not readily available. To address …

Metal Oxide Nanoparticles Synthesized By Nonthermal Plasma For Electrochemical Applications, Qinyi Chen

McKelvey School of Engineering Theses & Dissertations

Metal oxide nanocrystals can be synthesized by colloidal processing and gas-phase processing routes. High-quality nanocrystals produced by colloidal routes typically have surface ligands. Transport of electrons and ions among nanocrystals is hindered by surface ligand, and degrades related electrical performance. Gas-phase processing, for example combustion and thermal plasma, can make free-standing nanocrystals. However, nanocrystals produced by combustion method are heavily agglomerated, which further limits the usage of nanoparticles in electrochemical applications. Nonthermal plasma, as an emerging attractive route, has been initially focused on the synthesis of elemental group IV materials, and extended to include the synthesis of multicomponent materials, such …

Magnesiothermic Combustion Synthesis Of Nanocrystalline Silicon And Oxidation Kinetics Of Magnesium Particles, Sergio Cordova

Open Access Theses & Dissertations

Magnesium (Mg) is a well-known reduction agent in metallurgy (more specifically, in metallothermy). Recently, magnesiothermic reduction of oxides has been used in self-propagating high-temperature synThesis (SHS) of advanced materials such as ultrahigh-temperature ceramics (UHTC). The magnesiothermic SHS has also been used for the conversion of silica (SiO2) to silicon-based materials for thermoelectric applications. However, since oxidation of Mg releases a lot of heat, the direct use of it as the reduction agent leads to excessively high temperatures and undesirable sintering of the products. We have proposed to use magnesium silicide (Mg2Si) instead of Mg in the SHS of nanostructured silicon. …

Structure-Property Relationship In High Strength- High Ductility Combination Austenitic Stainless Steels, Chengyang Hu

Open Access Theses & Dissertations

Austenitic stainless steels are widely used in our daily life, but their mechanical strength is low. In order to improve their yield strength via grain refinement, an investigation was carried out involving phase reversion annealing concept comprising of severe cold roll reduction followed by annealing at different temperatures for short durations. During annealing reversion of deformation-induced martensite to austenite occurred by shear mechanism, leading to fine-grained structure and high strength-high ductility combination.Nanoscale deformation studies suggested that the deformation mechanism of nanograined structure was different from the coarse-grained counterpart. Post-mortem electron microscopy of plastic zone surrounding the indent indicated that the …

Methods , Systems , And Devices Relating To Surgical End Effectors, Shane M. Farritor, Thomas Frederick, Joe Bartels

Department of Mechanical and Materials Engineering: Faculty Publications

The embodiments disclosed herein relate to various medical device components , including components that can be incorporated into robotic and / or in vivo medical devices, and more specifically including end effectors that can be incorporated into such devices. Certain end effector embodiments include various vessel cautery devices that have rotational movement as well as cautery and cutting functions while maintaining a relatively compact structure. Other end effector embodiments include various end effector devices that have more than one end effector.