Engineering Commons^™

Effect Of Ultrasonic Treatment On The Microstructure And Mechanical Properties Of Al6061 And Composite, Ana S. Exime

FIU Electronic Theses and Dissertations

In this study, the effect of ultrasonic treatment (UST) parameters such as amplitude, sonication time, and melt temperature on microstructure and microhardness of Al 6061 alloy is evaluated. The effect of UST on the dispersion of tungsten disulfide (WS₂) and carbon nanotubes (CNT) as reinforcement particles in Al 6061 during casting is also studied. The cast Al 6061 with UST demonstrated 32% grain size reduction and 8% increase in the microhardness for optimum processing conditions. The cavitation process induced by UST is responsible for the refinement in microstructure and increase of hardness by enhancing the degassing and nucleation …

Microstructure And Mechanical Properties Of Nanofiller Reinforced Tantalum-Niobium Carbide Formed By Spark Plasma Sintering, Christopher Charles Rudolf

FIU Electronic Theses and Dissertations

Ultra high temperature ceramics (UHTC) are candidate materials for high temperature applications such as leading edges for hypersonic flight vehicles, thermal protection systems for spacecraft, and rocket nozzle throat inserts due to their extremely high melting points. Tantalum and Niobium Carbide (TaC and NbC), with melting points of 3950°C and 3600°C, respectively, have high resistivity to chemical attack, making them ideal candidates for the harsh environments UHTCs are to be used in. The major setbacks to the implementation of UHTC materials for these applications are the difficulty in consolidating to full density as well as their low fracture toughness. In …

Synthesis Of Carbon Nanotubes Using High Voltage And High Frequency Induction Field, Kalty Vazquez

FIU Electronic Theses and Dissertations

The fields of nanomaterial and nanostructures are some of the fastest growing fields in material science today. Carbon nanotubes are at the forefront of these fields and their unique mechanical and electrical properties are of great interest to those working in multiple engineering fields.

The overall objective of this study was to design and develop a new process and the equipment necessary, to synthesize carbon nanotubes using high voltage and a high-frequency induction field. This was the first time that a high voltage and an induction field have been used simultaneously in high yield production of carbon nanotubes.

The source …