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Thermal Characterization Of Natural And Synthetic Spider Silks By Both The 3Ω And Transient Electrothermal Methods, Troy Munro, Changhu Xing, Heng Ban, Cameron G. Copeland, Randolph V. Lewis, Colby Jensen
Thermal Characterization Of Natural And Synthetic Spider Silks By Both The 3Ω And Transient Electrothermal Methods, Troy Munro, Changhu Xing, Heng Ban, Cameron G. Copeland, Randolph V. Lewis, Colby Jensen
Faculty Publications
Thermal conductivity, thermal diffusivity and volumetric heat capacity of three spider silks are measured in this paper as a benchmark for further studies. These silks include the major and minor ampullate silks of the Nephila clavipes spider, and a synthetic spider silk fiber made from recombinant dragline silk proteins purified from transgenic goats’ milk. Two complementary measurement techniques are employed in the thermal characterization of these microscale single fibers for self-verification. One is the transient electrothermal technique (TET) and the other is the 3ω method. Experimental measurements indicate that thermal properties of the dragline silk are very close to those …
Investigation Of Synthetic Spider Silk Crystallinity And Alignment Via Electrothermal, Pyroelectric, Literature Xrd, And Tensile Techniques, Troy Munro, Tristan Putzeys, Michael Wubbenhorst, Christ Glorieux, Cameron G. Copeland, Randolph V. Lewis, Changhu Xing, Heng Ban
Investigation Of Synthetic Spider Silk Crystallinity And Alignment Via Electrothermal, Pyroelectric, Literature Xrd, And Tensile Techniques, Troy Munro, Tristan Putzeys, Michael Wubbenhorst, Christ Glorieux, Cameron G. Copeland, Randolph V. Lewis, Changhu Xing, Heng Ban
Faculty Publications
The processes used to create synthetic spider silk greatly affect the properties of the produced fibers. This paper investigates the effect of process variations during artificial spinning on the thermal and mechanical properties of the produced silk. Property values are also compared to the ones of the natural dragline silk of the N. clavipes spider, and to unprocessed (as-spun) synthetic silk. Structural characterization by scanning pyroelectric microscopy is employed to provide insight into the axial orientation of the crystalline regions of the fiber and is supported by XRD data. The results show that stretching and passage through liquid baths induce …