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Materials Science and Engineering

Materials Engineering

Nanoparticles

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Full-Text Articles in Engineering

Life Cycle Assessment And Comparison Of Magnesium Oxide Nanoparticles Prepared By Aqueous And Microwave Synthesis Methods, Jesse Cartland Jun 2016

Life Cycle Assessment And Comparison Of Magnesium Oxide Nanoparticles Prepared By Aqueous And Microwave Synthesis Methods, Jesse Cartland

Materials Engineering

Abstract: Magnesium oxide nanoparticles are being used increasingly as catalysts for organic synthesis, fuel oil additives, and CO2 adsorbents. There are many ways to produce magnesium oxide nanoparticles, but there is little information available regarding the environmental costs of production. As demand for environmentally friendly materials increases, it is important to understand environmental impact differences between various production methods. This study will compare the differences in embodied energy and global warming potential (GWP) between two synthesis methods: microwave combustion synthesis (microwave synthesis) and oxidation of magnesium hydroxide (aqueous synthesis). The resulting nanoparticles were characterized using scanning electron microscopy (SEM), …


The Synthesis And Characterization Of Gold And Silver Nanoparticles In Formal And Informal Settings, Mathew Wynn Jun 2012

The Synthesis And Characterization Of Gold And Silver Nanoparticles In Formal And Informal Settings, Mathew Wynn

Materials Engineering

Silver nanoparticles were synthesized through the reduction of AgNO3 using NaBH4. The borohydride anions were adsorbed onto silver nanoparticles. The repelling forces of the borohydride anions prevented the aggregation of particles, but the addition of an electrolyte or agitation induced aggregation. A yellow hue was given off by the silver nanoparticle sol that, using a spectrophotometer, had plasmon resonance at 386 nm. The silver nanoparticles were estimated to be 10 to 20 nm in diameter. Gold nanoparticles were synthesized through the reduction of HAuCl4 using Na3C6H5O7. The gold nanoparticle sol gave off a red hue that had plasmon resonance at …


The Effects Of Concentration, Stir Rate, And Processing Temperature On The Iridescence Of Polymethyl Methacrylate Nanoparticles, David Baruela Jun 2012

The Effects Of Concentration, Stir Rate, And Processing Temperature On The Iridescence Of Polymethyl Methacrylate Nanoparticles, David Baruela

Materials Engineering

Synthetic opals were synthesized by creating polymethyl methacrylate (PMMA) nanospheres in order to determine which conditions would create the best iridescent samples. The factors affecting the iridescence were nanosphere concentration, stir rate, and processing temperature. PMMA solutions were made by adding 17 mg of granular azobis to a solution of 16 mL of distilled water with 3 mL of methyl methacrylate (MMA). The solution was stirred at different rates, slow and fast, and different temperatures, 70 °C and 90 °C, under a constant flow of nitrogen gas for 40 minutes until the polymerization reaction was complete. Glass substrates were prepared …