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Full-Text Articles in Engineering

Carbon Nanotubes And Tungsten Oxide Nanorods: Synthesis And Applications, Bing Xiao Apr 2005

Carbon Nanotubes And Tungsten Oxide Nanorods: Synthesis And Applications, Bing Xiao

Electrical & Computer Engineering Theses & Dissertations

Synthesis and applications of two types of one-dimensional nanomaterials, carbon nanotubes (CNTs) and tungsten oxide nanorods, are investigated in this dissertation. Multi-walled CNTs have been successfully synthesized using two types of chemical vapor deposition (CVD) methods: microwave plasma enhanced CVD and atmospheric pressure thermal CVD. CNTs and their synthesis processes are characterized with various analysis techniques including scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy, and optical emission spectroscopy. Ultra-thin and high quality multi-walled CNTs are discovered in CNT films produced by MPCVD, which exhibit good field emission performance that is found to be dependent on the synthesis …


Melting And Solidification Study Of Indium And Bismuth Nanocrystals Using Reflection High-Energy Electron Diffraction, Mohamed K. Zayed Jan 2005

Melting And Solidification Study Of Indium And Bismuth Nanocrystals Using Reflection High-Energy Electron Diffraction, Mohamed K. Zayed

Electrical & Computer Engineering Theses & Dissertations

As technology begins to utilize nanocrystals for many chemical, biological, medical, electrical, and optoelectrical applications, there is a growing need for an understanding of their fundamental properties. The study of melting and solidification of nanocrystals is of interest to fundamental understanding of the effect of reduced size and crystal shape on the solid-liquid phase transition. Melting and solidification of as-deposited and recrystallized indium and bismuth nanocrystals were studied using reflection high-energy electron diffraction (RHEED). The nanocrystals were thermally deposited on highly oriented 002-graphite substrate at different deposition temperatures. The growth dynamics of the nanocrystals was studied using in situ RHEED …