Open Access. Powered by Scholars. Published by Universities.®

Engineering Commons

Open Access. Powered by Scholars. Published by Universities.®

Materials Science and Engineering

Missouri University of Science and Technology

2019

XRD

Articles 1 - 2 of 2

Full-Text Articles in Engineering

Characterization Of Mgal₂O₄ Sintered Ceramics, Nina Obradovic, William Fahrenholtz, Suzana Filipovic, Cole Corlett, Pavle Dordevic, Jelena Rogan, Predrag J. Vulic, Vladimir Buljak, Vladimir Pavlovic Apr 2019

Characterization Of Mgal₂O₄ Sintered Ceramics, Nina Obradovic, William Fahrenholtz, Suzana Filipovic, Cole Corlett, Pavle Dordevic, Jelena Rogan, Predrag J. Vulic, Vladimir Buljak, Vladimir Pavlovic

Materials Science and Engineering Faculty Research & Creative Works

Single phase MgAl2O4 was made from a one-to-one molar ratio of MgO and Al2O3 powders mixed using ball-milling. Mixtures of MgO and Al2O3 were subsequently treated in planetary ball mill for 30, 60, 90 and 120 minutes in air. The aim of this study was to examine phase composition, microstructure, and densification behavior of sintered specimens. After sintering in dilatometer at 1500 °C, the powder was converted to single phase MgAl2O4. The results show that mechanical activation improved the densification behavior of MgAl2O4 sintered …


Microstructural Evolution Of Zirconium Carbide (Zrcₓ) Ceramics Under Irradiation Conditions, Raul Florez Jan 2019

Microstructural Evolution Of Zirconium Carbide (Zrcₓ) Ceramics Under Irradiation Conditions, Raul Florez

Doctoral Dissertations

A comprehensive understanding of the microstructural evolution of Zirconium Carbide (ZrC2) ceramics under irradiation conditions is required for their successful implementation in advanced Gen-IV gas-cooled nuclear reactors. The research presented in this dissertation focusses on elucidating the ion and electron irradiation response of ZrC2 ceramics. In the first part of the research, the microstructural evolution was characterized for ZrC2 ceramics irradiated with 10 MeV Au3+ ions up to doses of 30 displacement per atom (dpa) at 800 ºC. Coarsening of the defective microstructure, as a function of dose, was revealed by transmission electron microscopy analysis. …