Engineering Commons^™

A Study Of The Recrystallization And The Mechanical Properties Of Indium, Louis John Reitsma Jr.

Doctoral Dissertations

"The recrystallization temperature and the mechanical properties of tensile strength, elongation, reduction in area and hardness were determined for 99.97% indium. Metallographic techniques were developed and stress rupture data were obtained.

Single crystals of indium were grown in a horizontal furnace with a traveling temperature zone, and sectioned in a strain-free manner, with an etch-cutter. Because of the low recrystallization temperature of indium, no further work was done on the single crystals.

The effect of recrystallization on electrical resistance, thermoelectric force, hardness, bending strength, crystallographic orientation and microstructure was studied. The range of recrystallization temperature for small amounts of cold …

A Thermodynamic Study Of The Zirconium Sulfides, Andrew Hessler Larson

Doctoral Dissertations

"A hydrogen reduction technique was used to determine some thermodynamic properties of various zirconium sulfide phases. The equilibrium H₂S/H₂ ratios were determined as a function of temperature and composition of the condensed sulfide phases. The hydrogen sulfide content of the equilibrated gas mixtures was analyzed by an iodimetric titration procedure.

A detailed description is given for the method and apparatus used both in the preparation of the various sulfide phases and in their equilibration with a hydrogen-hydrogen sulfide gas mixture.

The composition ranger 59 to 67 atomic per cent sulfur was studied over a temperature range of …

Imperfections Within Ti₂O₃ And Tio₂ Phases In The Titanium-Oxygen System, Tatsuhiko Ejima

Doctoral Dissertations

“The hexagonal-rhombohedral Ti₂O₃ phase in the Ti-O system extends from 32.5 to 34.5% oxygen b.w., with the exact composition of Ti₂O₃ nearly in the middle of the phase. Seven samples of different composition within that phase were made, and the lattice constants (a and c) and the density of each sample were determined.

The plots of the constants against the composition of the samples revealed a deviation from Vegard’s rule when approaching the exact composition of Ti₂O₃. The lattice constants of this compound, obtained by graphical interpolation were; a_{25 …}