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Full-Text Articles in Engineering
Effect Of Synthesis Time And Treatment On Porosity Of Mesoporous Silica Materials, Asli Ertan, Pradeep Kodumuri, Orhan Talu, Surendra N. Tewari
Effect Of Synthesis Time And Treatment On Porosity Of Mesoporous Silica Materials, Asli Ertan, Pradeep Kodumuri, Orhan Talu, Surendra N. Tewari
Chemical & Biomedical Engineering Faculty Publications
Nitrogen adsorption at 77 K on mesoporous silica materials (MPS) with varying synthesis time and treatment conditions was investigated. Scanning electron microscope (SEM) and X-ray diffraction (XRD) were also used to characterize the mesoporous materials. This study was performed at 6, 24 and 72-h synthesis times. It is shown that 6-h is not enough for complete formation of the MPS material and at least 24-h is necessary. The pore structure starts decaying for the 72-h synthesis time. The three-after-synthesis treatment conditions used were 1) washed, 2) washed and calcined and 3) directly calcined after synthesis. Ethanol/HCl …
On Stresses Induced In A Thermal Barrier Coating Due To Indentation Testing, Jin Yan, Anette M. Karlsson, Marion Bartsch, Xi Chen
On Stresses Induced In A Thermal Barrier Coating Due To Indentation Testing, Jin Yan, Anette M. Karlsson, Marion Bartsch, Xi Chen
Mechanical Engineering Faculty Publications
Instrumented indentation has been suggested as a method to determine interfacial fracture toughness of thermal barrier coatings. However, in a previous experimental study we showed that the results are ambiguous. In this work, we investigate the experimental results by numerical simulations incorporating the material microstructure. In the numerical simulations, based on finite element analyses, the stress fields that are associated with the loading and unloading of the indenter are investigated. By comparing these stress fields to the damage observed in the experimental study, including crack path and interfacial delaminations, we explain key findings from the experimental observations. Our results suggest …