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Determination Of Ibuprofen Isotherm Using Supercritical Fluid Chromatography, Loi Ho
Determination Of Ibuprofen Isotherm Using Supercritical Fluid Chromatography, Loi Ho
USF Tampa Graduate Theses and Dissertations
Chromatography is widely used to determine physiochemical properties data including adsorption isotherm. In the separation of enantiomers through sorptive processes, supercritical fluids allow efficient and green alternatives to liquid solvent based systems. The isotherm information is vital in the development of operating policies and design of preparative chromatographic or moving bed separation schemes. Determination of sorption isotherms from experimental chromatographic elution data is automated and compared with different chromatogram model. Procedures were developed and validated for separation of R- and S- ibuprofen with supercritical 〖CO〗_2 and ethanol mixture as the mobile phase over a chiral stationary phase. The isotherms for …
Sub-Cooled Pool Boiling Enhancement With Nanofluids, Elliott Charles Rice
Sub-Cooled Pool Boiling Enhancement With Nanofluids, Elliott Charles Rice
USF Tampa Graduate Theses and Dissertations
Phase-change heat transfer is an important process used in many engineering thermal designs. Boiling is an important phase change phenomena as it is a common heat transfer process in many thermal systems. Phase change processes are critical to thermodynamic cycles as most closed loop systems have an evaporator, in which the phase change process occurs. There are many applications/processes in which engineers employ the advantages of boiling heat transfer, as they seek to improve heat transfer performance. Recent research efforts have experimentally shown that nanofluids can have significantly better heat transfer properties than those of the pure base fluids, such …