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Aerospace Engineering

University of Central Florida

Theses/Dissertations

2020

XRD

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Degradation From Cmas Infiltration In 7ysz Eb-Pvd Thermal Barrier Coatings, Zachary Stein Jan 2020

Degradation From Cmas Infiltration In 7ysz Eb-Pvd Thermal Barrier Coatings, Zachary Stein

Honors Undergraduate Theses

The lifetime of the high temperature ceramic coating 7 wt.% yttria-stabilized zirconia (7YSZ) is reduced when calcium-magnesium-alumino-silicate (CMAS) particulates enters aero-engines during operation in a sandy or dusty environment, melts, and infiltrates into the coating. 7YSZ undergo both chemical and mechanical degradation from CMAS infiltration during cycling. Characterization methods with synchrotron X-ray diffraction (XRD) provides a non-destructive means to measure the impact of time and temperature on coating degradation with high spatial resolution of 7YSZ coatings infiltrated and annealed by CMAS for 1 hour and 10 hours as well as at 1225 °C and 1250 °C. Additionally, qualitative results of …