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Synthesis Of High-Temperature Stable Anatase Tio2 Photocatalyst, Suresh Pillai, Declan Mccormack, Michael Seery, Pradeepan Periyat, Steven Hinder, John Colreavy, Reenamol George, Hugh Hayden
Synthesis Of High-Temperature Stable Anatase Tio2 Photocatalyst, Suresh Pillai, Declan Mccormack, Michael Seery, Pradeepan Periyat, Steven Hinder, John Colreavy, Reenamol George, Hugh Hayden
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In the absence of a dopant or precursor odification, anatase to rutile transformation in synthetic TiO2 sually ccurs at a temperature of 600 700 °C. Conventionally, metal oxide dopants (e.g., Al2O3 nd SiO2 are used o tune the anatase to rutile transformation. A simple methodology is reported here to extend the anatase utile transformation by employing various concentrations of urea. XRD and Raman spectroscopy were used uring thermal treatment. A significantly higher anatase phase (97%) as been obtained at 800 C with use of a 1:1 Ti(OPr)4 urea composition and 11% anatase composition is etained even after calcining …