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Catalysts For The Positional Isomerization Of Internal, Long-Chain Olefins, James Edward Bruno
Catalysts For The Positional Isomerization Of Internal, Long-Chain Olefins, James Edward Bruno
LSU Doctoral Dissertations
Double-bond isomerization of internal C16-C18 olefins is a necessary step in the production of paper sizing agents. In this work, the properties that enable long-lasting solid acid catalysts (both commercial and lab-synthesized) were identified, the efficacy of regenerated solid acid catalysts was tested, and the feasibility of organometallic chain-walking catalysts (both homogeneous and polymer-supported) for olefin isomerization was evaluated. Hexadecene isomerization was investigated using perfluorinated ion exchange resins (Nafion®) supported on SiO2 or Al2O3, sulfonated poly(styrene-co-divinylbenzene) resins (PS-DVBs), tungstated zirconias, and acidic zeolites. Selected catalysts underwent lifetime studies. Oversulfonated PS-DVBs (e.g., Amberlyst 35) were reasonably selective with long lifetimes, only …
Release, Stability And Functionality Of Nanodelivered Hydrophobic (Lutein And Beta-Carotene) And Hydrophilic (Folic Acid) Antioxidants Using Zein Nanoparticles, Thanida Chuacharoen
Release, Stability And Functionality Of Nanodelivered Hydrophobic (Lutein And Beta-Carotene) And Hydrophilic (Folic Acid) Antioxidants Using Zein Nanoparticles, Thanida Chuacharoen
LSU Doctoral Dissertations
Nanodelivery systems enable innovations that can benefit foods and human health on a large scale in the coming years. The instabilities of antioxidants during food processing and during digestion are drawbacks that can be successfully addressed by nanoentrapment. This research provided technical strategies to synthesize zein nanoparticles loaded with hydrophobic/hydrophilic antioxidants, and to study the release profiles and physical stability of nanocarriers and chemical stability of entrapped bioactives under on-shelf and GI conditions. The results supported the potential of zein nanoparticles stabilized by surfactants to improve chemical stability of entrapped lutein, and to slowly release lutein under PBS conditions. Same …
Developing Co-Current And Counter-Current Spray Drying Computational Fluid Dynamics (Cfd) Simulation Studies To Predict The Quality Of Microencapsulated Fish Oil With Egg White Hydrolysates Powders, Kevin Estuardo Mis Solval
Developing Co-Current And Counter-Current Spray Drying Computational Fluid Dynamics (Cfd) Simulation Studies To Predict The Quality Of Microencapsulated Fish Oil With Egg White Hydrolysates Powders, Kevin Estuardo Mis Solval
LSU Doctoral Dissertations
Eggs are an excellent source of high quality protein containing all essential amino acids (EAA) including leucine. Food-grade protein hydrolysates can enhance the growth of lactic acid bacteria (LAB). Thermal degradation of bioactives normally occurs during microencapsulation by spray drying. Spray drying modeling using computational tools is essential to engineer new food powders and to minimize and thermal degradation of bioactives. The first chapter of this work discusses the optimization of an enzymatic process in terms of reaction temperature, pH, enzyme:substrate ratio, and reaction time using a response surface methodology (RSM) to produce food-grade protein hydrolysates from egg whites (EWH). …
On An Effective Submodeling Procedure For Stresses Determined With Finite Element Analysis, Ajay Ashok Kardak
On An Effective Submodeling Procedure For Stresses Determined With Finite Element Analysis, Ajay Ashok Kardak
LSU Doctoral Dissertations
Submodeling can enable stress analysts using finite elements to focus analysis on a subregion containing the stress concentration of interest, with consequent computational savings. Such benefits are only truly realized if the boundary conditions on the edges of the subregion that were originally contained within the global region are sufficiently accurate. These boundary conditions are drawn from initial global finite element analysis (FEA), and consequently themselves have errors that in turn lead to errors in the stresses sought. When these last boundary-condition errors are controlled, and the discretization errors incurred by the FEA of ensuing submodels are also controlled, submodeling …
Healing-On-Demand Polymer Composites Based On Shape Memory Polyurethane Fibers And Polymeric Artificial Muscles, Pengfei Zhang
Healing-On-Demand Polymer Composites Based On Shape Memory Polyurethane Fibers And Polymeric Artificial Muscles, Pengfei Zhang
LSU Doctoral Dissertations
In this dissertation, the healing-on-demand polymer composites based on shape memory polyurethane fibers and artificial muscles are investigated, for understanding and developing a novel healing-on-demand composite so that it would be used for industrial applications that could heal structural-length scale damage and leaking autonomously, repeatedly, efficiently, timely, and molecularly. Firstly, the structural relaxation behavior of shape memory polyurethane (SMPU) fiber was studied by theoretical analysis and experimental test. Then, a self-healing composite based on cold-drawn short SMPU fiber was prepared and tested for evaluating its crack-healing performance. After that, polymer artificial muscle based healing-on-demand composite was developed and characterized. Based …
Applications Of Geopolymer In Civil Engineering: Feasibility Study Of Loess Stabilization And Waste Concrete Recycling, Zhen Liu
LSU Doctoral Dissertations
The fast growing population and economic development have resulted in an increasing demand for residential and commercial buildings and infrastructures. However, there are problems identified to fulfill this demand, including that (1) problematic soils need to be treated/improved before the construction of building and infrastructures; (2) the Portland cement industry, which is used for concrete production and as the conventional soil stabilizer, is not environment friendly; (3) qualified natural aggregates for concrete production are being depleted; and (4) great amount of construction & demolition waste (C&D waste) is being produced every year. This means that green materials and recycling the …
Physics And Applications Of A Pdms Based Centrifugal Microfluidic System, Ziliang Cai
Physics And Applications Of A Pdms Based Centrifugal Microfluidic System, Ziliang Cai
LSU Doctoral Dissertations
The objective of this research work is to develop a centrifugal microfluidic system for general purposes based on microfabrication technologies including SU-8 photolithography, polydimethylsiloxane (PDMS) casting. The main contribution of this research is to integrate a flyball governor system into the polymer based centrifugal microfluidic platform. A series of function units are developed based on this unique mechanism. In the first part, three pinch valve systems were designed and tested. The first one is based on the magnetic force and the second one is on the basis of spring force and the last one is a membrane valve. All valving …
Degradation And Fatigue Involving Dissipated Processes, Md Liakat Ali
Degradation And Fatigue Involving Dissipated Processes, Md Liakat Ali
LSU Doctoral Dissertations
Irreversible material degradation due to cyclic mechanical loading is investigated utilizing the concept of thermodynamic entropy, plastic strain energy, and temperature slope measurement. Uniaxial tension-compression and fully-reversed bending fatigue tests are performed over a wide range of loading conditions with metallic and composite materials subject to both constant- and variable-amplitude loading. A methodology is developed for the estimation of the fatigue fracture entropy (FFE) and fatigue toughness of metallic specimens in a rapid fashion. It is found that the FFE and the fatigue toughness of each material tested are within a small band. The value of FFE is found to …
New Identification And Decoding Techniques For Low-Density Parity-Check Codes, Tian Xia
New Identification And Decoding Techniques For Low-Density Parity-Check Codes, Tian Xia
LSU Doctoral Dissertations
Error-correction coding schemes are indispensable for high-capacity high data-rate communication systems nowadays. Among various channel coding schemes, low-density parity-check (LDPC) codes introduced by pioneer Robert G. Gallager are prominent due to the capacity-approaching and superior error-correcting properties. There is no hard constraint on the code rate of LDPC codes. Consequently, it is ideal to incorporate LDPC codes with various code rate and codeword length in the adaptive modulation and coding (AMC) systems which change the encoder and the modulator adaptively to improve the system throughput. In conventional AMC systems, a dedicated control channel is assigned to coordinate the encoder/decoder changes. …
Development Of Satellite-Assisted Forecasting System For Oyster Norovirus Outbreaks, Jiao Wang
Development Of Satellite-Assisted Forecasting System For Oyster Norovirus Outbreaks, Jiao Wang
LSU Doctoral Dissertations
Norovirus outbreaks can cause the closure of oyster harvesting waters and acute gastroenteritis in humans associated with consumption of contaminated raw oysters. The overall goal of this study was to develop a satellite-assisted forecasting system for oyster norovirus outbreaks. The forecasting system is comprised of three components: (1) satellite algorithms for retrieval of environmental variables, including salinity, temperature, and gage height, (2) an Artificial Neural Network (ANN) based model, called NORF model, for predicting relative risk levels of oyster norovirus outbreaks, and (3) a mapping method for visualizing spatial distributions of norovirus outbreak risks in oyster harvest areas along Louisiana …
Interorganizational Collaboration And Systemic Change Framework For Building Information Modeling (Bim) Adoption, Rehema Joseph Monko
Interorganizational Collaboration And Systemic Change Framework For Building Information Modeling (Bim) Adoption, Rehema Joseph Monko
LSU Doctoral Dissertations
It was found that an integrated framework needs to be developed for the construction industry that allows optimized interorganizational collaboration and systemic change while using Building Information Modeling (BIM) technologies. The framework needs to be effective so the industry can adopt BIM through a set of interdependent activities beyond their organizational boundaries. The adoption has been proven difficult because of industry competitiveness and a fragmented work environment. Meanwhile, existing frameworks vary between studies. This research developed an integrated framework, identified critical factors, and provided an evaluation guide for interorganizational collaboration and set of coordinated changes necessary to adopt BIM. This …
Field Instrumentation And Testing To Study Set-Up Phenomenon Of Driven Piles And Its Implementation In Lrfd Design Methodology, Md Nafiul Haque
Field Instrumentation And Testing To Study Set-Up Phenomenon Of Driven Piles And Its Implementation In Lrfd Design Methodology, Md Nafiul Haque
LSU Doctoral Dissertations
This research study investigates the pile set-up phenomenon for clayey soils and develops the models to predict pile set-up resistance at a certain time after the end of driving (EOD). The increase of pile resistance after EOD is known as “pile set-up”. To fulfill this objective, a total number of twelve prestressed concrete (PSC) test piles were driven in different soil conditions of Louisiana. In addition, dynamic load tests (DLT) and static load tests (SLT) were usually performed to verify the axial resistances of piles at specific times after EOD, as well as to quantify the amount of increase in …
Uncertainty Analyses Of Climate Change Impact On Hydrologic Projections, Ehsan Beigi
Uncertainty Analyses Of Climate Change Impact On Hydrologic Projections, Ehsan Beigi
LSU Doctoral Dissertations
This study conducts uncertainty analysis on future region-scale hydrologic projections under the uncertain climate change projections of the IPCC Fifth and Forth Assessment Reports. The hierarchical Bayesian model averaging (HBMA) method is adopted to segregate and prioritize sources of climate projection uncertainty, obtain ensemble mean of hydrologic projection, and quantify the hydrologic projection uncertainty arising from individual uncertainty sources. This study deals with the choices of greenhouse gas (GHG) concentration trajectories, global climate models (GCMs), and GCM initial conditions as three major uncertainty sources in downscaled precipitation and temperature projections. The method is applied to investigate future hydrologic projections in …
Study Of Active Vibration Control Using The Method Of Receptances, Amit Maha
Study Of Active Vibration Control Using The Method Of Receptances, Amit Maha
LSU Doctoral Dissertations
Using the Method of Receptance, it is possible in general to assign 2_x0002_ poles (i.e. n conjugate pairs) of an axially vibrating rod of variable cross section by sensing the state at _x0002_ points along the rod. Using the sensor data, closed loop feedback control gains can be calculated by solving a simple set of linear equations. The feedback gains can be applied to generate the required control force using an actuator. This partial pole assignment can be done without continuous or discrete analytical modeling. Therefore, the physical parameters such as the rigidity, the density, and the variable cross-sectional area …
Analyses Of The Mec1 Dna Damage Pathway In Saccharomyces Cerevisiae, William Barrett Ainsworth
Analyses Of The Mec1 Dna Damage Pathway In Saccharomyces Cerevisiae, William Barrett Ainsworth
LSU Doctoral Dissertations
Eukaryotic organisms implement conserved surveillance machinery to sense and respond to DNA damage. Fundamental to the repair process is coordinated regulation of repair genes and initiation of cell cycle arrest protocols. Failure to preserve these checkpoints results in accumulation of mutated DNA and aberrant cell phenotypes that are characteristic of human disease. The yeast, Saccharomyces cerevisiae, utilizes the MEC1 checkpoint pathway to regulate the DNA damage response. This study addressed two overarching themes of transcriptional and post-translational regulation within the MEC1 pathway. We first applied our understanding of the MEC1 DNA damage transcriptional response to develop advanced luciferase whole cell …
Context Aware Textual Entailment, Soha Arab-Khazaeli
Context Aware Textual Entailment, Soha Arab-Khazaeli
LSU Doctoral Dissertations
In conversations, stories, news reporting, and other forms of natural language, understanding requires participants to make assumptions (hypothesis) based on background knowledge, a process called entailment. These assumptions may then be supported, contradicted, or refined as a conversation or story progresses and additional facts become known and context changes. It is often the case that we do not know an aspect of the story with certainty but rather believe it to be the case; i.e., what we know is associated with uncertainty or ambiguity. In this research a method has been developed to identify different contexts of the input raw …
Aqueous Atmospheric Species, A Dual Study: 1. Comparison Of The Effects Of Temperature, Oxygen Level, Ionic Strength, And Ph On The Reaction Of Benzene With Hydroxyl Radicals At The Air-Water Interface To The Bulk Aqueous Phase. 2. Determination Of Carbonyl Compounds In Fog Water Samples Via Online Concentration And Hplc, Aubrey Anne Heath
LSU Doctoral Dissertations
The air-water interface is the largest interface in the environment. Atmospheric droplets, such as fog, which can have an exceptionally high surface area-to-volume ratio, also have a large range of physical and chemical properties (e.g. temperature, pH, ionic strength, and chemical composition) based on location, time of day, and emission source. Unlike larger atmospheric droplets, which are predominately characterized by bulk aqueous phase conditions, reactions that take place in fog droplets are determined by both the bulk-aqueous phase and the air-water interface due to a high surface area-to-volume ratio. In order to have a greater understanding of atmospheric processes and …
Risk-Based Wind Loss And Mitigation For Residential Wood Framed Construction, Fatemeh Orooji
Risk-Based Wind Loss And Mitigation For Residential Wood Framed Construction, Fatemeh Orooji
LSU Doctoral Dissertations
As a result of increasing windstorm losses in the United States over the past 50 years, a variety of residential wind hazard mitigation methods have been suggested. Mitigation undoubtedly reduces windstorm losses; however, the expected economic risk reduction of mitigation practices over the life of the building depends on the building characteristics (i.e., capacity) and the intensity and occurrence of wind speeds (i.e., demand). Effective decision making requires estimation of potential future losses based on many variables. Many models, primarily mechanics-based simulation models, have been developed to predict building damage from wind events; however; fewer models of economic loss have …
Image-Based Modeling Of Porous Media Using Fem And Lagrangian Particle Tracking, Paula Cysneiros Sanematsu
Image-Based Modeling Of Porous Media Using Fem And Lagrangian Particle Tracking, Paula Cysneiros Sanematsu
LSU Doctoral Dissertations
The study of fundamental flow and transport processes at the pore scale is essential to understanding how the mechanisms affect larger, field-scale, processes that occur in oil and gas recovery, groundwater flow, contaminant transport, and CO2 sequestration. Pore-scale imaging and modeling is one of the techniques used to investigate these fundamental mechanisms. Although extensive development of pore-scale imaging and modeling has occurred recently, some areas still need further advances. In this work, we address two areas: (1) imaging of bulk proppants and proppant-filled fractures under varying loading stress and flow simulation in these systems and (2) nanoparticle (NP) transport modeling …
Design And Optimization Of Nanoplasmonic Waveguide Devices, Pouya Dastmalchi
Design And Optimization Of Nanoplasmonic Waveguide Devices, Pouya Dastmalchi
LSU Doctoral Dissertations
In this dissertation, we introduce compact absorption switches consisting of plasmonic metal-dielectric-metal (MDM) waveguides coupled to multisection cavities. The optimized multisection cavity switches lead to greatly enhanced modulation depth compared to optimized conventional Fabry-Perot cavity switches. We find that the modulation depth of the optimized multisection cavity switches is greatly enhanced compared to the optimized conventional Fabry-Perot cavity switches due to the great enhancement of the total electromagnetic field energy in the cavity region. We then investigate how to improve the computational efficiency of the design of nanoplasmonic devices. More specifically, we show that the space mapping algorithm, originally developed …
Fabrication And Characterization Of Miniaturized Components Based On Extruded Ceramic-Filled Polymer Blends, Khurshida Sharmin
Fabrication And Characterization Of Miniaturized Components Based On Extruded Ceramic-Filled Polymer Blends, Khurshida Sharmin
LSU Doctoral Dissertations
The objective of this work is to develop an improved manufacturing process for microstructured ceramic components that is based on co-extrusion. Co-extrusion of structured feedrods holds promise for development of multi-layered, functionally graded and/or textured structures. However, it requires a polymer binder that is difficult to remove before structures can be sintered to full density. A two-step debinding is introduced to eliminate debinding defects that are commonly observed in thermal debinding (TD). Cracking is a major issue due to a lack of pore spaces for outgassing of pyrolysis products in traditional TD. In two-step debinding, a soluble binder is removed …
Modeling Two-Phase Flow And Heat Transfer In Polygonal Microchannels, Sai Sashankh Rao
Modeling Two-Phase Flow And Heat Transfer In Polygonal Microchannels, Sai Sashankh Rao
LSU Doctoral Dissertations
Microfluidics is a burgeoning research area with applications ranging from microfluidic cooling to biomolecule synthesis. Here we study two problems to gain an improved understanding of two-phase flow and heat transfer in microfluidic devices. We also study a third problem on boundary layer flow out of theoretical interest. In the first problem, we study the heat and mass transfer in polygonal micro heat pipes under small imposed temperature differences. A micro heat pipe, used in electronics cooling, consists of a closed polygonal microchannel filled with a wetting liquid and a long vapor bubble. We model the evaporation, fluid flow, and …
Ambit Of Multiphase Cfd In Modelling Transport Processes Related To Oil Spill Scenario And Microfluidics, Abhijit Rao
Ambit Of Multiphase Cfd In Modelling Transport Processes Related To Oil Spill Scenario And Microfluidics, Abhijit Rao
LSU Doctoral Dissertations
During the ‘Deepwater Horizon’ accident in the deep sea in 2010, about 4.9 million barrels of oil was released into the Gulf of Mexico, making the spill one of the worst ocean spills in recent times. To mitigate the ill effects of the event on the environment, subsea injection of dispersants was carried out. Dispersant addition lowers the interfacial tension at oil/water interface and presence of local turbulence enhances the droplet disintegration process. The oil droplets contain a plethora of hydrocarbons which are soluble in water. In deep spill scenarios, droplets spend large amounts of time in water column; hence, …
Optimal Location Of Biomethane Gas Manufacturing Plants And Allocation Of Feedstock And Liquified Carbon Product, Bingqing Wu
Optimal Location Of Biomethane Gas Manufacturing Plants And Allocation Of Feedstock And Liquified Carbon Product, Bingqing Wu
LSU Doctoral Dissertations
Biomethane gas (BMG), known for its sustainability, low environmental impact, and high profitability, has received wide attention in recent years. To facilitate the process of making strategic plans for building a BMG production system, this dissertation leverages the mathematical modeling and optimization techniques to minimize the supply chain cost for such a system. Typical elements in a BMG production system consist of the local farms that produce the feedstock, the hubs that collect and store the feedstock produced by farms, the reactors that generate BMG from the feedstock transported from the hubs, the condensers that liquefy the BMG from the …
Development And Optimization Of Non-Hydrostatic Models For Water Waves And Fluid-Vegetation Interaction, Ling Zhu
LSU Doctoral Dissertations
The primary objective of this study is twofold: 1) to develop an efficient and accurate non-hydrostatic wave model for fully dispersive highly nonlinear waves, and 2) to investigate the interaction between waves and submerged flexible vegetation using a fully coupled wave-vegetation model. This research consists of three parts. Firstly, an analytical dispersion relationship is derived for waves simulated by models utilizing Keller-box scheme and central differencing for vertical discretization. The phase speed can be expressed as a rational polynomial function of the dimensionless water depth, $kh$, and the layer distribution in water column becomes an optimizable parameter in this function. …
Product Parameters Optimization For Double Purge Of C-Magma Integrated With Conventional Three-Boiling Crystallization Scheme To Improve Raw Sugar Whole Color, Luz Stella Polanco
Product Parameters Optimization For Double Purge Of C-Magma Integrated With Conventional Three-Boiling Crystallization Scheme To Improve Raw Sugar Whole Color, Luz Stella Polanco
LSU Doctoral Dissertations
Efficient crystallization in raw sugar production is the result of a combination of factors and responses that meet specific criteria. Matching a sugar quality standard, maximizing sugar yield, maximizing crystallization equipment capacity and minimizing heat requirement are all necessary optimization criteria. A double centrifugation or purge of C-magma is intended to improve raw sugar whole color by the reduction of color recirculation with the sugar crystal. Combining a three boiling crystallization scheme with a second centrifugation after the last crystallization stage required optimizing the input/output product parameters (purities) and the location of the liquid recycle component (double purge molasses) for …
Output Consensus Control For Heterogeneous Multi-Agent Systems, Abhishek Pandey
Output Consensus Control For Heterogeneous Multi-Agent Systems, Abhishek Pandey
LSU Doctoral Dissertations
We study distributed output feedback control of a heterogeneous multi-agent system (MAS), consisting of N different continuous-time linear dynamical systems. For achieving output consensus, a virtual reference model is assumed to generate the desired trajectory for which the MAS is required to track and synchronize. A full information (FI) protocol is assumed for consensus control. This protocol includes information exchange with the feed-forward signals. In this dissertation we study two different kinds of consensus problems. First, we study the consensus control over the topology involving time delays and prove that consensus is independent of delay lengths. Second, we study the …
Thermo-Catalytic Upgrading Of Pyrolysis Vapors Using Electromagnetic Heating, Pranjali Devidas Muley
Thermo-Catalytic Upgrading Of Pyrolysis Vapors Using Electromagnetic Heating, Pranjali Devidas Muley
LSU Doctoral Dissertations
Electromagnetic heating offers several advantages such as rapid heating rates, accurate temperature control and energy efficiency over conventional reactors. The goal of this study was to design an effective and energy efficient catalytic reactor for pyrolysis vapor upgrading. An induction based catalytic reactor was designed for upgrading of pyrolysis vapors. The effect of catalyst bed temperatures (290°, 330° and 370°C) and biomass to catalyst ratios of 1, 1.5 and 2 was studied. The results were compared to conventional heating reactor. Induction heating reactor performance exceeded that of conventional heater. The biomass to catalyst ratio of 2 in combination with the …
Electrochemical Study Of Ammonium Interaction With Au,Sn And Cu Electrodes In Nonaqueous Electrolytes, Guoying Qu
Electrochemical Study Of Ammonium Interaction With Au,Sn And Cu Electrodes In Nonaqueous Electrolytes, Guoying Qu
LSU Doctoral Dissertations
Nonaqueous electrolytes play an important role in electrochemical devices such as flip chip and lithium-air batteries. In this work, we examine ammonium-Cu, Sn and Li interactions in nonaqueous electrolytes to optimize the future flip chip flux and electrolyte additive of lithium-air battery. The activity of halogen-free carboxylic acid flux is considered one of the most important aspects in controlling flip chip joint quality recently. CuOx removal effectiveness of carboxylic acid solutions at Cu substrates using electrochemical methods at elevated temperatures from 100ºC to 180ºC is studied thoroughly by chronopotentiometry and gravimetric analysis. Carboxylic acid-based solutions with ethanolamine show oxide removal …
Heat Transfer And Film Cooling On A Gas Turbine Blade And Shroud, Onieluan Tamunobere
Heat Transfer And Film Cooling On A Gas Turbine Blade And Shroud, Onieluan Tamunobere
LSU Doctoral Dissertations
At a fixed pressure ratio, the thermodynamic efficiency and net power output of a gas turbine engine increases with an increase in the turbine inlet temperature. Cooling is necessary because of the thermal limits of the engine materials. This research studies through experimentation, the heat transfer and cooling of critical gas turbine components including the shroud and blade tip. In the first phase, the shroud heat transfer behavior and the effectiveness of shroud cooling under the conditions of rotation is undertaken in a single stage turbine at a design rotation speed of 550 rpm, at off-design speeds and for varying …