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Atomic Force Microscopy For Better Probing Surface Properties At Nanoscale: Calibration, Design And Application, Yu Liu Oct 2010

Atomic Force Microscopy For Better Probing Surface Properties At Nanoscale: Calibration, Design And Application, Yu Liu

Electronic Thesis and Dissertation Repository

To measure force by AFM with high resolution requires accurate calibration of optic – lever detection sensitivity and spring constant. On biological AFM force mode, the coupling effects of the liquid environment, spot size of laser beam and laser spot location on AFM cantilever backside, must be considered to correlate the static sensitivities from force curves in air and in liquid for calibration. An effective model has been developed first and experimentally elucidated to calibrate the static sensitivity in liquid. The proposed model eliminates inconvenience of static sensitivity calibration in liquid with possible contamination sources.

The static sensitivity based on …


Self-Assembly Of Colloidal Particles From Evaporating Droplets: Role Of Dlvo Interactions And Proposition Of A Phase Diagram, Rajneesh Bhardwaj, Xiaohua Fang, Ponisseril Somasundaran, Daniel Attinger Mar 2010

Self-Assembly Of Colloidal Particles From Evaporating Droplets: Role Of Dlvo Interactions And Proposition Of A Phase Diagram, Rajneesh Bhardwaj, Xiaohua Fang, Ponisseril Somasundaran, Daniel Attinger

Daniel Attinger

The shape of deposits obtained from drying drops containing colloidal particles matters for technologies such as inkjet printing, microelectronics, and bioassay manufacturing. In this work, the formation of deposits during the drying of nanoliter drops containing colloidal particles is investigated experimentally with microscopy and profilometry, and theoretically with an in-house finite-element code. The system studied involves aqueous drops containing titania nanoparticles evaporating on a glass substrate. Deposit shapes from spotted drops at different pH values are measured using a laser profilometer. Our results show that the pH of the solution influences the dried deposit pattern, which can be ring-like or …