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Molybdenum Versus Tungsten Based Polyoxometalates For Highly Effective Methylene Blue Removal, Roula Abi Saad, Ghassan Younes, Mohammad H. El- Dakdouki, Rami Al-Oweini

BAU Journal - Science and Technology

[SiW₁₂O₄₀]^4-(SiW₁₂) and [Mo₈O₂₆]^4- (Mo₈) were synthesized and characterized by Fourier Transform Infrared spectroscopy (FTIR). The prepared polyoxometalates were studied as potential adsorbents for the removal of methylene blue (MB) from an aqueous solution. Various operational parameters—contact time, adsorbent dose, initial dye concentration, pH, and temperature— were meticulously assessed by UV/Vis spectrophotometry to study its impact on the adsorption efficacy. An inverse relationship was observed between the percentage dye removal and the initial dye concentration, highlighting the complexes' superior adsorption capabilities under lower dye loads. The …