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Effect Of Polymer Concentration Rotational Speed And Solvent Mixture On Fiber Formation Using Forcespinning®, Nancy Obregon, Victor Agubra, Madhab Pokhrel, Howard Campos, David Flores, David De La Garza, Yuanbing Mao, Javier Macossay-Torres, Mataz Alcoutlabi

Chemistry Faculty Publications and Presentations

Polycaprolactone (PCL) fibers were produced using Forcespinning® (FS). The effects of PCL concentration, solvent mixture, and the spinneret rotational speed on fiber formation were evaluated. The concentration of the polymer in the solvents was a critical determinant of the solution viscosity. Lower PCL concentrations resulted in low solution viscosities with a correspondingly low fiber production rate with many beads. Bead-free fibers with high production rate and uniform fiber diameter distribution were obtained from the optimum PCL concentration (i.e., 12.5 wt%) with tetrahydrofuran (THF) as the solvent. The addition of N, N-dimethylformamide (DMF) to the THF solvent promoted the gradual formation …