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Diffusion In Wide Grain Boundaries, J. Mimkes, Manfred Wuttig
Diffusion In Wide Grain Boundaries, J. Mimkes, Manfred Wuttig
Materials Science and Engineering Faculty Research & Creative Works
The rigorous solution of the grain-boundary diffusion problem has been approximated by a series expansion method. The calculations show that higher-order terms may be neglected in the bulk adjacent to the grain boundary. Thus, in this region Whipple's and Suzuoka's solutions represent a close approximation to the problem. Inside the grain boundary, however, higher-order approximations have to be taken into account. These approximations gain importance in the case of wide grain boundaries. The solutions obtained for an instantaneous source have been fitted to available grain-boundary diffusion data of Ni2+ in MgO at 1200°C. Numerical calculations give for the bulk diffusion …
Thermal Expansion Of Tungsten At Low Temperatures, Jayant S. Shah, Martin E. Straumanis
Thermal Expansion Of Tungsten At Low Temperatures, Jayant S. Shah, Martin E. Straumanis
Materials Science and Engineering Faculty Research & Creative Works
No abstract provided.
Phase Equilibria And Thermodynamic Studies In The System Cao-Feo-Fe2o3-Sio2, M. Timucin, Arthur E. Morris
Phase Equilibria And Thermodynamic Studies In The System Cao-Feo-Fe2o3-Sio2, M. Timucin, Arthur E. Morris
Materials Science and Engineering Faculty Research & Creative Works
Phase equilibria and thermodynamic properties of the system CaO-FeO-Fe2O3-SiO2 were studied at 1450° and 1550°C, over a range of pO2 from 1 to about 10-11 atm. Isothermal phase diagrams and activity-composition diagrams were constructed for 0, 5, 10, 20, and 30 wt pct SiO2 sections. The data are applicable to further understanding the behavior of simple BOF steelmaking slags. © 1970 The Minerals, Metals & Materials Society - ASM International - The Materials Information Society.
The Fe-Ho Binary System, G. J. Roe, Thomas J. O'Keefe
The Fe-Ho Binary System, G. J. Roe, Thomas J. O'Keefe
Materials Science and Engineering Faculty Research & Creative Works
The Fe-Ho phase diagram was determined on the basis of data obtained by X-ray diffraction, metallographic and differential thermal analysis techniques. Since emphasis was centered in the region where intermetallic compounds predominate, neither the iron nor holmium terminal regions were included in this study. Eutectic reactions were found to occur at 16.5 wt pct Fe and 875° C, 61 wt pct Fe and 1284° C, and 79 wt pct Fe and 1338° C. The congruent melting points of the compounds Ho6Fe23 and Ho2Fe17 were found to be 1332° and 1343° C, respectively. Two other intermetallic compounds were found, HoFe2 and …
Electron Emitter Tips And Method, P. D. Ownby
Electron Emitter Tips And Method, P. D. Ownby
Materials Science and Engineering Faculty Research & Creative Works
Boron is deposited on the (110) plane facet at the center of a tungsten electron emitter tip by chemical vapor deposition of boron triiodide. The emission current density is greatest in the center of the emitting area (FIG. 2).
The Deformation Mechanisms In Sublimed Magnesium Under Cyclic Loading, Babu Narian Thakur
The Deformation Mechanisms In Sublimed Magnesium Under Cyclic Loading, Babu Narian Thakur
Doctoral Dissertations
"A detailed study of the deformation processes in sublimed magnesium under reverse bending fatigue in air at room temperature has been undertaken utilizing the light, scanning and transmission electron microscopy. The Principal deformation modes are the basal slip and {10Ī2} twinning. The proportion of twinning increases markedly with the increasing stress level and the number of cycles. The evidence for cross slip is seen on the basal slip bands. The extrusions are seen not only along the basal slip lines but also along the {10Ī2} twin boundaries. In the later stages of fatigue, the extrusions chip off producing a notch …
Voids In Neutron Irradiated Aluminum, Nicholas H. Packan
Voids In Neutron Irradiated Aluminum, Nicholas H. Packan
Doctoral Dissertations
"Void formation in high purity aluminum resulting from irradiation to fluences between 1.5 x 10¹⁹ and 1.6 x 10²² neutrons/cm² (E > 0 .1 MeV) at a temperature of 55 ± 5ºC was studied, primarily by means of transmission electron microscopy. In particular the effects of neutron fluence and flux were examined, as well as the possible influences of both preexisting and transmutation-produced impurities. A very low concentration of voids (about 10¹²/cm³) resulted from irradiation to 1.5 x 10¹⁹ neutrons/cm²; they averaged about 150 Å in diameter. Void concentrations and sizes increased with fluence, reaching values of 6 x 10¹⁴ voids/cm³ …
Cathodic Behavior Of Co, Co-Fe Alloys And Some Other Metals In Acids In A Cathodic Protection Arrangement, Ram Bajaj
Masters Theses
"During cathodic protection of a corroding metal, electrons are forced into the metal by a sacrificial anode, a battery or a rectifier. These electrons, which constitute the suppressing or external current, are discharged (by H⁺ of the corrosive liquid) on the local cathode of the corroding metal decreasing the emf of the local cells, and, thus, reducing the cell current or the rate of corrosion of the metal. This process was studied in detail by finding out the relationship existing between the cell and suppressing currents. The study was made using two circuits: the cell circuit (representing the local current) …
Fracture Surface Energy Determinations Of High Density Polycrystalline Ceramics, Gene Arthur Pahlmann
Fracture Surface Energy Determinations Of High Density Polycrystalline Ceramics, Gene Arthur Pahlmann
Masters Theses
"Values of fracture surface energy were measured for steatite, zircon, mullite and four densities of alumina. Rods of these high density materials were cut into thin rectangular specimens which were notched and broken in three-point loading. The resulting load necessary for fracture of the specimens was used to calculate the fracture surface energy of the materials. The value for the steatite was around 20,000 ergs/cm². The values for the zircon and mullite were on the order of 13,000 ergs/cm², and the values for the aluminas ranged from 17,000 to 24,000 ergs/cm²"--Abstract, page ii.
Thermal Expansion Of Orthorhombic Pbo, Charles A. Sorrell
Thermal Expansion Of Orthorhombic Pbo, Charles A. Sorrell
Materials Science and Engineering Faculty Research & Creative Works
Thermal expansion of orthorhombic PbO was investigated by high‐temperature X‐ray diffraction. The coefficients in the a0, and c0 directions are equal and Pb–O chains extended in the a0 direction and bonded into layers in the b0 direction; appreciable Pb–Pb bonding is indicated. Coordination and bond distances observed in PbSiO3 and lead silicate glasses, which are similar to those of massicot, and PbnOn polymeric units reported in PbO vapor are interpreted as additional evidence of the importance of PbO chains as structural entities. Copyright © 1970, Wiley Blackwell. All rights reserved
Diffusion And Internal Friction In Sodium-Rubidium Silicate Glasses, Gary L. Mcvay
Diffusion And Internal Friction In Sodium-Rubidium Silicate Glasses, Gary L. Mcvay
Doctoral Dissertations
"The internal friction and self diffusion coefficients of sodium and rubidium ions for (1 - X) Na₂O·X Rb₂O·3 SiO₂ glasses have been measured. The diffusion measurements employed radioactive isotopes and a thin sectioning technique and extended from 350 to 500°C. Internal friction measurements were made from -150 to 500°C and at frequencies of 0.05 to 6000 Hz. The maximum height for the mixed alkali internal friction peak occurs at the composition where the sodium and rubidium diffusion coefficients are equal. It is concluded that the mechanism responsible for the mixed alkali peak is a cooperative rearrangement of sodium-rubidium ions and …
Etch Patterns On Zone-Refined Fe, M. E. Straumonis, Chang-Soo Kim
Etch Patterns On Zone-Refined Fe, M. E. Straumonis, Chang-Soo Kim
Electrical and Computer Engineering Faculty Research & Creative Works
Upon dissolution of zone-refined Fe in strong acids, mainly three kinds of corrosion patterns were observed in the crystallites of the sections. Regardless of the acids, the {110} plane always appeared on the three patterns in the form of smooth and even steps, ledges, or facets. The {112}, {122}, and {123} planes were also developed but to a much lesser degree. The {100} and {111} planes were not observed because grains of the respective orientation were missing on the sections. Attempts were made to explain the formation of the planes by taking into consideration the reticular density of the planes …
Some Effects Of Oh Groups On Sodium Silicate Glasses, Mokhtar Sayed Maklad
Some Effects Of Oh Groups On Sodium Silicate Glasses, Mokhtar Sayed Maklad
Doctoral Dissertations
"Glasses of various compositions in the Na₂O-SiO₂ system were prepared with different levels of OH concentration. Phase separation kinetics, thermal expansion, radiation induced optical absorption, and internal friction of these glasses were studied. The increase in OH content in these glasses was found to (a) enhance the rate of phase separation; (b) increase thermal expansion above the glass temperature and change the dilatometric softening temperature in a way that depends on microstructure; (c) increase the radiation induced optical absorption bands associated with positive hole centers and decrease those associated with electron trap centers; and, (d) decrease the low temperature alkali …
Investigations Of Several Variables In The Dwight-Lloyd Mcwane Ironmaking Process, James Orlan Hood Jr.
Investigations Of Several Variables In The Dwight-Lloyd Mcwane Ironmaking Process, James Orlan Hood Jr.
Masters Theses
"The Dwight- Lloyd McWane Ironmaking Process (D-LM) is the first commercial process of its particular type and one of the few commercial processes involving prereduction of iron ore in existence today. This presentation reviews some promising ironmaking processes which involve iron ore prereduction, with special attention being given the D-LM process. Although the D-LM process is continuous from iron ore to high quality molten cast iron, the research and discussion herein is limited to principal variables involved in the production of high quality carbonized pellets in the prereduction phase of the operation. The variables of process temperature and pellet carbon …
Temperature Variation In Distribution Of Relaxation Times In Aluminosilicate Glasses, David Wayne Moore
Temperature Variation In Distribution Of Relaxation Times In Aluminosilicate Glasses, David Wayne Moore
Doctoral Dissertations
"The distribution of relaxation times for the alkali peak in a Li₂ O·A1₂O₃ ·2.0SiO₂ glass and for the mixed alkali peak in a 0.5Li₂O·0.5Na₂O·A1₂O₃·2.OSiO₂ glass was studied using the internal friction technique. A lognormal distribution of relaxation times provided the best agreement with the experimental data. The ß parameter of the lognormal distribution function, which is related to the half-height peak width, varied with temperature, indicating that the distribution of relaxation times is dependent upon the activation energy and the activation entropy of the relaxation mechanism. The major contributor to the distribution of relaxation times is a wide distribution in …
Thermal Expansion Of Tetragonal Pbo, Charles A. Sorrell
Thermal Expansion Of Tetragonal Pbo, Charles A. Sorrell
Materials Science and Engineering Faculty Research & Creative Works
Thermal expansion of tetragonal PbO, investigated by high‐temperature X‐ray diffraction in vacuum, is nearly isotropic, with the coefficient in the c0 direction only slightly greater than that in the a0 direction. Volume thermal expansion is only slightly greater than in massicot. Retardation of the litharge‐massicot transformation is tentatively interpreted as the result of very low oxygen partial pressures caused by catastrophic oxidation of the stainless‐steel sample holder and resulting oxygen scavenging by lead vapor. Copyright © 1970, Wiley Blackwell. All rights reserved
Carburization Of Type 316l Stainless Steel In Static Sodium, F. B. Litton, Arthur E. Morris
Carburization Of Type 316l Stainless Steel In Static Sodium, F. B. Litton, Arthur E. Morris
Materials Science and Engineering Faculty Research & Creative Works
The transport of carbon from an iron-87 wt.% carbon alloy through static sodium to Type 316L stainless steel was investigated at temperatures of interest to the liquid-metal fast-breeder reactor (LMFBR) program. The rate-controlling step for the experimental geometry employed was the diffusion of carbon in the source. © 1970.
Exact Solution For A Model Of Dislocation Pipe Diffusion, J. Mimkes, Manfred Wuttig
Exact Solution For A Model Of Dislocation Pipe Diffusion, J. Mimkes, Manfred Wuttig
Materials Science and Engineering Faculty Research & Creative Works
The dislocations are treated as an ideal array of parallel pipes of radius and diffusivity Dp embedded in the bulk material of the diffusivity Db. The exact solution of this problem of diffusion along semi-infinite edge dislocations is presented for cubic, tetragonal, and hexagonal crystals. The solution makes it possible to evaluate the dislocation pipe radius a and the ratio of diffusivities from one experiment. It is applied to experimental data for self-diffusion in tellurium available in the literature. The results of the calculations are a dislocation pipe radius a=(1.5 0.5)x10-4 cm and an activation energy for the pipe diffusion …
Electrode Reactions In Zinc Electrolysis, Ernest R. Cole
Electrode Reactions In Zinc Electrolysis, Ernest R. Cole
Doctoral Dissertations
"The effects of temperatures from 0°C to 50°C and current densities from 10 asf to 200 asf on the current efficiency in the electrolysis of pure zinc sulfate solutions (65 gpl Zn⁺⁺ - 200 gpl H₂SO₄) were determined. Pure platinum and platinum coated titanium anodes were used with an aluminum cathode. Platinum anodes were not inert at certain combinations of temperature and current density, and platinum acted as a low overvoltage impurity causing resolution of the cathode deposit. Orientation of the zinc deposits was found to vary with temperature and to have a distinct relationship to current efficiency. Preconditioning of …
The Oxidation Kinetics Of Liquid Lead And Lead Alloys, Thomas Edward Weyand
The Oxidation Kinetics Of Liquid Lead And Lead Alloys, Thomas Edward Weyand
Doctoral Dissertations
"Liquid lead and lead-silver alloys were investigated to determine the rates and products of oxidation in pure oxygen at temperatures of 350 to 600°C. The kinetic data were determined using a Cahn electro-balance. Liquid lead was found to follow a cubic rate of oxidation between 350 and 400°C. A parabolic rate was found at temperatures above 400°C. 0.496% silver and 2.258% silver alloys followed a cubic rate of oxidation from 350 to 550°C and tended to approach a parabolic rate of oxidation above this temperature. Silver additions were found to increase the rate of oxidation as compared to the pure …
Spheroidization In Tool Steels, Sharad Gajanan Bankar
Spheroidization In Tool Steels, Sharad Gajanan Bankar
Masters Theses
"A carbon steel, W1, and four other alloy tool steels, namely, A2, H13, D3, and M2, were spheroidized by five different procedures. Any modification made in the treatments for an individual steel were suggested by the results obtained with these five procedures. The hardnesses and microstructures obtained were compared with steel samples annealed at a tool steel mill. The response given by different steels to various methods of spheroidization was studied. It was found that A2, W1, and D3 steels responded the best to the cycling method whereas the best response to the isothermal annealing was given by H13 and …
The Smelting Of Lead Drosses, Humberto Adolfo Arzabe
The Smelting Of Lead Drosses, Humberto Adolfo Arzabe
Masters Theses
"The constitution of the matte and bullion obtained by the smelting of lead drosses coming from the cooling of lead blast furnace bullion was investigated by metallographic, chemical, electron-microprobe, and X-ray means. At smelting temperatures (1200°C to 1300°C) two liquid phases are in equilibrium. A liquid lead phase with low concentrations of copper and sulfur, and a lighter liquid matte phase containing a high concentration of copper and sulfur with some dissolved lead. On cooling to room temperature the matte precipitates cuprous sulfide, a eutectic mixture of cuprous sulfide and lead sulfide with a deficiency of sulfur, and metallic lead …
Investigation Of The System Al₂O₃-Teo₂-O₂, Vera Zelenkova Sestak
Investigation Of The System Al₂O₃-Teo₂-O₂, Vera Zelenkova Sestak
Masters Theses
"The system Al₂O₃-TeO₂-O₂ has been investigated by X-ray diffraction and differential thermal analysis in air and in sealed silica ampoules. The tellurate, Al₂TeO₆, with tellurium in the +6 valence state, forms in air but not in vacuum at 1 mm pressure. A second phase, a tellurite, possibly Al₂Te₂O₇, forms in air or vacuum by devitrification. The glass-forming region is wider than previously stated and is more extensive in vacuum--from 50% to 98% TeO₂. Tentative phase boundaries have been placed for the system in air and vacuum"--Abstract, page ii.
Imperfections In The Ag-In System (Alpha-Phase) And Lattice Parameters Of Cadmium Oxide, Prafulla Maganlal Vora
Imperfections In The Ag-In System (Alpha-Phase) And Lattice Parameters Of Cadmium Oxide, Prafulla Maganlal Vora
Masters Theses
"This thesis has been divided into two parts, namely, "Imperfections in the Ag-In System (Alpha-Phase)" and "Lattice Parameters of Cadmium Oxide." Imperfections in the Ag-In System (Alpha-Phase): It can be shown -- as in the case of the Cu-In α solid solutions -- that during quenching from the liquid state, strains are produced by the quenching process and, in addition, vacancies are quenched-in, in the Ag-In α-solid solutions. The number of vacancies present, measured by the decreased density of the alloys, is proportional to the indium content up to the solid-solubility limit. Upon heat treatment of the alloys, the thermal …
A Systematic Study Of Instrument Variables Upon The Accuracy Of Microprobe Analysis, R. A. Parr
A Systematic Study Of Instrument Variables Upon The Accuracy Of Microprobe Analysis, R. A. Parr
Masters Theses
"The purpose of this investigation was to study the effect of instrument parameter changes upon X-ray intensity measurements of the copper-manganese system. The parameters utilized in this study included: (1) polished, contaminated, and 600 grit surfaces ; (2) constant sample current and constant beam current modes; and (3) 15 KV, 20 KV, and 25 KV accelerating potentials. Inspection of the data disclosed three interesting points: (1) copper and manganese X-ray intensity measurements appear to be a linear function of composition in the 15 KV through 25 KV accelerating potential range; (2) electron backscatter measurements consistently show in a limited range …
Metallographic Study Of Phase Changes In Heat Treated Ductile Iron, Mahendra Vadilal Desai
Metallographic Study Of Phase Changes In Heat Treated Ductile Iron, Mahendra Vadilal Desai
Masters Theses
"Continuous cast ductile iron samples were hardened. It was found that carbide dissolved in the austenite faster than graphite and that this material requires higher austenitizing temperatures and longer austenitizing time than steels. Tempered microstructures were affected by the prior austenitizing treatment and it appeared that the amount of carbon dissolved in the austenite determined the tempered microstructure. Several attempts to determine the austenite grain size indicated that it is not as easy to determine in ductile iron as in steels. Two techniques, heat etching and an isothermal transformation method, were found to reveal prior austenite grain size. It was …